• Title/Summary/Keyword: tape casting method

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The Fabrication and Electrical Properties of PMS-PZT Ceramics using a Tape Casting Method (Tape Casting법에 의한 PMS-PZT계 세라믹스 제조 및 전기적 특성)

  • Jung, Hyun-Jae;Na, Eun-Sang;Choi, Sung-Churl
    • Journal of the Korean Ceramic Society
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    • v.38 no.9
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    • pp.860-865
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    • 2001
  • After manufacturing 2mol% CdO substitute $0.05Pb(Mn_{1/3}Sb_{2/3})O_3-0.95Pb(Zr_{0.52}Ti_{0.48})O_3$ piezoelectric ceramics powder as starting material, to manufacture green sheets using Doctor Blade method. The optimum composition of slurry was studied. Moreover, the sintering properties and the dielectric and piezoelectric properties with variation a thickness of the manufactured sheets were investigated. The optimum of slurry was investigated by the rheology with addition of additives, the sintering condition was decided by TGA. And the properties of sheet were investigated through SEM. XRD. The optimum of slurry was the stablest at dispersant 3.0 wt% to solid loading 30vol%. After, at addition of binder/plasticizer(0.75/0.25) 3.0wt%, viscosity was 7.55Pa${\cdot}$s. The dielectric and piezoelectric properties of the sheet were increased a little with the increasing of sintering temperature but were not variable with variation of sheet thickness.

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Effect of Preparation Methods of a Matrix Retaining Electrolyte on the Characteristics of a Phosphoric Acid Fuel Cell (인산형 연료전지(PAFC)용 전해질 매트릭스의 제조방법이 전극/매트릭스 계면특성에 미치는 영향)

  • 윤기현;최재열;장재혁;김창수
    • Journal of the Korean Ceramic Society
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    • v.34 no.12
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    • pp.1205-1212
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    • 1997
  • The matrices which consisted of SiC whisker, PES(polyesterasulfone) as a binder, span 80(sorbitan monooleate) as a surfactant, TPP(triphenyl phosphate) as a plasticizer and dichloromethane as a solvent, have been prepared by the various methods such as tape casting, rolling, tape cast-coating and roll-coating method. The fuel cells of single stack type using these matrices are characterized by ac impedance spectroscopy and cyclic voltammetry technique. A fuel cell using a matrix prepared by the tape cast-coating method shows the best performance of 466.34 mA/$\textrm{cm}^2$ at 0.6V because it has the lowest polarization resistance at the interface between electrodes and a matrix due to the largest three phase contact region of gases, catalyst and electrolyte.

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The Fabrication and Properties of Lead-tree Transparent Dielectric Thick Films for PDP (PDP 무연 투명유전체 후막의 형성 및 특성)

  • Heo, Sung-Cheol;Choi, Duck-Kyun;Oh, Young-Jei
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.17 no.10
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    • pp.1107-1113
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    • 2004
  • Dry film method for large size of PDP(Plasma Display Panel) module has been actively investigated. This method for lead-free transparent dielectric formation depends on green sheet technology. By adjusting the composition of transparent dielectric powders and organics, uniformly dispersed slurry was fabricated, Viscosity of the slurry exhibited pseudoplastic behavior for tape casting, Cast green sheets were tested under tensile condition at room temperature. It was found that the increase in transparent dielectric powder and binder ratio leads to decrease in strain to failure of green sheets from 120 % to 34 % and from 255 % to 4 %, respectively. Tensile strength of green sheets decreased abruptly with increase of transparent dielectric powder ratio, with minimum at 0.13 MPa. On the other hand, tensile strength increased continuously from 0.1 MPa to 2.4 MPa with increase of binder ratio. The green sheets were attached on the glass substrate and heated by following firing schedule. As a result, the best result was obtained when fired at 580 $^{\circ}C$ for 15 min and had transmittance of 78 % in visible range 550 nm.

Electrical properties of Low Fired Pb(Mg,Te,Mn,Nb)$O_3-Pb(Zr,Ti)O_3$ Ceramics (저온에서 소결한 Pb(Mg,Te,Mn,Nb)$O_3-Pb(Zr,Ti)O_3$세라믹스의 전기적 특성)

  • 정수태;조상희
    • Electrical & Electronic Materials
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    • v.9 no.7
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    • pp.652-659
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    • 1996
  • Sintering characteristics and electrical properties of xPb(Mg$_{1}$8/Te$_{1}$8/Mn$_{1}$4/Nb$_{1}$2/) $O_{3}$-(1-x) Pb (Zr$_{1}$2/ $Ti_{1}$2/) $O_{3}$ (x=0.075, 0.1, 0.125) ceramics are investigated. A sintering temperature of ceramics could be reduced to 950.deg. C by a reaction between PbO and B site compound material. The physical properties of 0.1Pb(Mg, Te, Mn, Nb) $O_{3}$ - 0.9Pb(Zr, Ti) $O_{3}$ bulk ceramic with 3wt% glass frit(0.857PbO-0.143W $O_{3}$) were following : den = 7.95 g/cm$^{3}$, T$_{c}$=340.deg. C, .epsilon.$_{33}$= 754, k$_{31}$=0.3 and Q.=1780. The 3-layer piezoelectric transformer by using a tape casting method showed a good monolithic structure, and its voltage setup ratio was 2.5 times higher than that of a single device by using bulk ceramics.s.s.

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Effect of Organic Additive Composition on Isostatic Thermocompression Behavior of Alumina Tapes (유기물 조성에 따른 알루미나 테이프의 열간 가압 거동)

  • 이명현;박일석;김대준;이득용
    • Journal of the Korean Ceramic Society
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    • v.37 no.8
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    • pp.824-831
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    • 2000
  • Alumina tapes, having various ratios of alumina to alumina+binder+plasticizer (a/(a+o)) and binder to binder+plasticizer(b/(b+p)), were prepared by the tape casting method. The tapes were thermocompressed varying the thermocompression parameters such as temperature, pressure, and duration time. Among the parameters, the pressure was the most influential to the tape packing density. The packing density varied in two different ways depending on the a/(a+o) ratio. For the tapes having low a/(a+o) ratio, a saturation density was reached by applying very a low pressure of 1 MPa. For tapes with high a/(a+o), on the contrary, the saturation density was obtained at a relatively high pressure. These different responses to the pressure are attributed to the fact that the rearrangement of alumina particles by the pressure becomes easy as an organic content in the tapes is high.

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Guide for Processing of Textured Piezoelectric Ceramics Through the Template Grain Growth Method

  • Temesgen Tadeyos Zate;Jeong-Woo Sun;Nu-Ri Ko;Hye-Lim Yu;Woo-Jin Choi;Jae-Ho Jeon;Wook Jo
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.36 no.4
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    • pp.341-350
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    • 2023
  • The templated grain growth (TGG) method has gained significant attention for its ability to produce highly textured piezoelectric ceramics with significantly enhanced performance, making it a promising method for transducer and actuator applications. However, the texturing process using the TGG method requires the optimization of multiple steps, which can be challenging for beginners in this field. Therefore, in this tutorial, we provide an overview of the TGG method mainly based on our previous published works, including its various processing steps such as synthesizing anisotropic-shaped templates with size and size distribution control using the molten salt synthesis technique, tape casting, and identifying key factors for proper alignment of the templates in the target matrix system. Our goal is to provide a resource that can serve as a basic reference for researchers and engineers looking to improve their understanding and utilization of the TGG method for producing textured piezoelectric ceramics.

Electrochemical Properties of FeS2 Thin Film Electrodes for Thermal Batteries (열전지용 FeS2 박막전극의 전기화학적 특성)

  • Im, Chae-Nam
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.30 no.5
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    • pp.318-324
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    • 2017
  • Powder compaction technology is widely used to prepare thermal battery components. This method, however, is limited by the size, thickness, and geometry of the battery components. This limitation leads to excessive cell capacity, overweight, and higher cost of the pellets, which decreases the specific capacities and delays the activation time of thermal batteries. $FeS_2$ thin-film cathodes were fabricated by tape-casting technology and analyzed by SEM and EDS in this paper. The residual organic binder of the $FeS_2$ thin-film cathodes decreased with the temperature of the heat treatment, which improved the specific capacity because of the lower resistance. Specific capacities of the $FeS_2$ thin-film cathodes decreased because of the higher residual binder and the restrictive reaction of active materials with molten salts as the thickness increased. $FeS_2$ thin-film cathodes showed much higher specific capacity (1,212.2 As/g) than pellet cathodes (860.7 As/g) at the optimal heat-treatment temperature ($230^{\circ}C$).

A Study on the Acoustic Properties of Acoustic Treansducer with PZT/Metal (PZT/Metal로 구성된 음향변환기의 음향특성에 관한 연구)

  • Kim, Jin-Soo;Kang, Dae-Ha;Kim, So-Jung;Kim, Ho-Gi;Lee, Deok-Chool
    • The Journal of the Acoustical Society of Korea
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    • v.11 no.2
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    • pp.28-37
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    • 1992
  • In the study, the Acoustic transducer of a thin circular disc-type with PZT/Metal was manufactured. The 'tape casting method' was introduced to prepare the thin disc-type of piezoelectric ceramics. The acoustic characteristics of PZT/Metal acoustic transducer for piezoelectric buzzer and piezoelectric speaker etc. have been studied and analyzed. As a result, the sound pressure level (dB), in the range from -6dB to -14dB, increased with increasing the piezoelectric coeffeicient ($d_{31}$) of ceramics. The optimal conditions of the sound pressure characteristics of acoustic transducer were that the radius ratio(${\eta}$) of ceramics and metal plate is 0.7-0.8 and the thickness ratio(${\beta}$) is 1.0, and the value were -15~-165dB.

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Low Temperature Sintering and Dielectrics Properties of $(Ba_{1-x}Sr_x)TiO_3$ Ceramics by Addition (첨가물에 따른 $(Ba_{0.6}Sr_{0.4})TiO_3$의 저온소결 및 유전특성)

  • Jeon, So-Hyun;Kim, In-Sung;Song, Jae-Sung;Min, Bok-Gi;Yoon, Jon-Do
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.202-203
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    • 2005
  • To recognize whether admixture affects some $(Ba_{0.6}Sr_{0.4})TiO_3$, powder in this research $Li_2CO_3$, MgO, $MnO_2$ adding each 3 wt % by Tape casting method thick film make. Sitering temperature lowered 1300$^{\circ}C$ adding $Li_2CO_3$, and density is 5.942g/$cm^3$, and specific inductive capacity increases about decuple and displayed 4000. Climbed sitering temperature 1400$^{\circ}C$ adding MgO, specific inductive capacity reduced 1/2 times. Lowered sintering temperature 1325$^{\circ}C$ low adding $MnO_2$.

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Characteristics of Meta-aramid Fabrics Coated with Slurry of Nanoscale SiC Particles (나노 탄화규소(SiC) 슬러리로 코팅된 메타-아라미드 직물의 특성)

  • Park, Jong Hyeon;Lee, Sun Young;Won, Jong Sung;Lee, Eung Bo;Kim, Eui Hwa;Lee, Seung Goo
    • Textile Coloration and Finishing
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    • v.29 no.3
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    • pp.131-138
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    • 2017
  • Most of high performance fabrics for the car racing protective clothing have been developed to have thermal resistance, flame retardant property, impact resistance and anti-frictional properties to protect the racer from the crucial accident. In this study, the meta-aramid fabric, which has inherent flame retardant, was coated with nanoparticles of SiC to enhance the impact resistance and anti-friction properties. Uniform coating of the nanoparticles onto the fabrics was obtained by using tape casting method. As the experimental parameters, size and content of the SiC nanoparticle were varied with the coating conditions of the fabric surface. The effects of the nanoparticle coating on the properties of meta-aramid fabric were examined with various instrumental analyses such as SEM, tensile strength and abrasion test.