• 한국염색가공학회지
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• 제27권2호
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• pp.113-118
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• 2015

Poly(vinyl butyral), PVB was photooxidized by UV/ozone irradiation and the effect of UV energy on the surface properties of the UV-irradiated PVB film were investigated by the measurement of reflectance, surface roughness, contact angles, elemental composition, and zeta potential. With increasing UV energy, reflectance decreased in the visible and ultraviolet regions particularly at the wavelength of 400nm. The irradiation produced nano-scale surface roughness including the maximum peak-to-valley roughness increased from 274nm for the unirradiated PVB to 370nm at the UV energy of $5.3J/cm^2$. The improved hydrophilicity was due to the higher $O_{1s}/C_{1s}$ resulting from the introduction of polar groups such as C=O bonds. The surface energy of the PVB film increased from $35.3mJ/m^2$ to $39.3mJ/m^2$ at the irradiation of $15.9J/cm^2$. While the zeta potentials decreased proportionally with increasing UV energy, the cationic dyeability of the PVB increased accordingly resulting from the improved affinity of the irradiated PVB surfaces containing the photochemically introduced anionic and dipolar dyeing sites.

• 대한기계학회논문집
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• 제14권6호
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• pp.1495-1508
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• 1990

본 연구에서는 전류밀도와 가공시간을 변화시켰을 때의 가공량, 가공상태를 검토해 보았으며, 촉침홀더의 가공각도를 달리하거나 재부착문제를 해결하기 위한 마 스크의 사용여부에 따른 촉침의 가공상태를 알아보기 위해 초기선단반경 2$\mu\textrm{m}$, 선단각 90˚의 다이아몬드 촉침을 이온스파터 가공기를 사용하고, 가공조건을 변화시켜서 초 정밀 가공품의 표면거칠기 측정에 적합한 0.5$\mu\textrm{m}$ 이하의 미세한 선단반경을 갖는 촉침 을 가공하기 위한 가공조건에 대한 실험을 하였다.

• Design & Manufacturing
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• 제14권1호
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• pp.36-41
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• 2020

Recently, due to the development of MEMS technology, researches for the production of effective micro structures and shapes have been actively conducted. However, the process technology based on chemical etching has a number of problems such as environmental pollution and time problems due to multi-process. Various processes to cope with this process are being studied, and one of the mechanical etching processes is the powder blasting process. This process is a method of spraying fine particles, which has the advantage of being an effective process in manufacturing hard brittle materials. However, it is also a process that adversely affects the material surface roughness and material properties due to the impact of the injection of fine particles. In this study, after fabricating micro-channels in fused silica glass with excellent optical properties among the hard brittle materials, we used the nano indentation system to analyze the micro parts using nano-particles as well as machinability and surface roughness analysis of the processed surface. The analysis was performed for the effective processing of powder blasting.

• 한국염색가공학회지
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• 제26권3호
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• pp.159-164
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• 2014

Biodegradable Poly(butylene succinate), PBS, was photooxidized by UV/ozone irradiation and the effect of UV energy on the surface properties of the UV-irradiated PBS film were investigated by the measurement of reflectance, surface roughness, contact angles, chemical composition, and zeta potential. With increasing UV energy, reflectance decreased in the visible and ultraviolet regions particularly at the wavelength of 380nm. The irradiation produced nano-scale surface roughness including the maximum peak-to-valley roughness increased from 106nm for the unirradiated sample to 221nm at the UV energy of $10.6J/cm^2$. The improved hydrophilicity was due to the higher $O_{1s}/C_{1s}$ resulting from the introduction of polar groups such as C-O and C=O bonds. The surface energy of the PBS increased from $42.1mJ/m^2$ for the unirradiated PBS to $56.8mJ/m^2$ at the irradiation of $21.2J/cm^2$. The zeta potentials of the UV-irradiated PBS also decreased proportionally with increasing UV energy. The cationic dyeability of the PBS increased accordingly resulting from the improved affinity of the irradiated PBS surfaces containing photochemically introduced anionic and dipolar dyeing sites.

• Tribology and Lubricants
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• 제11권5호
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• pp.71-77
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• 1995

The capacitance technique was used to measure the minimum oil film thickness in engine bearing and the central oil film thickness between cam and tappet. This method is based on the measurement of total capacitance of oil film. For the measurement of the oil film thickness between cam and tappet, two surfaces were assumed to be flat and parallel within the Hertzian region and all the measured capacitance originated from this region. Shear rates from the measured minimum oil film thickness are over 10$^{6}$ sec$^{-1}$ in the greater part in both two cases. The minimum oil film thickness in engine bearing is larger than the surface roughness. Between cam and tappet it is mostly smaller than the surface roughness. In spite of the awkward restriction of the reliability of measured oil film thickness, it was known that the capacitance technique makes it possible to measure the oil film thickness in elastohydrodynamic and mixed lubrication regimes as well as in hydrodynamic regime. Therefore, it is also possible to classify the lubrication regimes based on the oil film thickness.

• 한국산학기술학회논문지
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• 제16권10호
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• pp.6551-6557
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• 2015

철근부식에 의해 발생된 녹은 철근 주변의 콘크리트에 팽창 압력을 유발하여 콘크리트의 균열, 피복콘크리트의 박리나 탈락, 철근의 단면적 감소 등 구조물의 내구성에 부정적인 영향을 끼친다. 본 논문에서는 코일철근을 대상으로 3차원 스캐너를 이용하여 철근이 부식됨에 따른 표면적을 측정하여 철근의 부식률과 표면 거칠기와의 관계를 프랙탈 이론을 이용하여 규명하였다. 코일 철근은 현장 적재일이 길수록 부식률이 증가하였으며, 부식률이 증가할수록 표면 거칠기는 거칠게 평가되었다. 프랙탈 차원의 증가량은 적재일 3일, 7일, 14일, 21일 경우 각각 0.0235, 0.0280, 0.0319, 그리고 0.0455로 나타났다. 이때의 부식률은 각각 0.3367%, 0.6127%, 0.7898%, 그리고 1.1965%로 나타나 프랙탈 차원을 이용한 부식된 코일철근의 표면 물리량 평가는 실제 부식률과 유사한 결과를 나타냈다.

• Tribology and Lubricants
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• 제11권5호
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• pp.99-107
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• 1995

This paper reported research results to develop an algorithm of on-lin evaluation of surface profiles and roughness generated by turning. The developed module consisted of computer simulation of surface profiles using mechanism of cutting mark formation and cutting vibrations, and online measurement of cutting vibrations. The relative cutting vibrations between tool and worpkiece were measured through an inductance pickup at the rate of one sample per rotation of the workpiece. The sampling process was monitored using an encoder to avoid conceling out the phase lag between waves. The digital cutting signals from the Analog-to-Digital converter were transferred to the simulation module of surface profile where the surface profiles were generated. The developed algorithm or surface generation in a hard turning was analyzed through computer simulations to consider the stochastic and dynamic nature of cutting process. Cutting tests were performed using AISI 304 Stainless Steel and carbide inserts in practical range of cutting conditions. Experimental results showed good correlation between the surface profiles and roughness obtained using the developed algorithm and the surface texture measured using a surface profilemeter. The research provided the feasibility to monitor surface characteristics during tribelogical tests considering wear effect on surface texture in machining.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2000년도 하계학술대회 논문집 D
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• pp.2854-2855
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• 2000

In industry and engineering. the tensile measurement of single crystal metal material such as the uniform change. surface structure and the tensile torque of the material is not easy to obtain by current the tensile measurement methods. In this paper. we have implemented a tensile system which can acquire tensile information in real time.

• 대한치과보철학회지
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• 제52권3호
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• pp.177-185
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• 2014

목적: 본 연구는 구리 합금 스케일러 팁을 비롯한 수종의 스케일러 팁이 임플란트와 수복물 재료 표면에 실제 치석제거 시와 같이 적용하였을 때 표면 거칠기에 미치는 영향을 알아보고자 하였다. 재료 및 방법: 도재, 티타늄, 지르코니아, 제3형 금합금의 지름 15 mm, 높이 1.5 mm의 원반형 시편을 준비하였고, 거칠기 형성기구로 스테인리스 스틸팁(SS), 플라스틱 수동 큐렛(PS), 구리 합금 팁(IS)을 이용하였으며, 시편의 개수는 각 재료 당 기구 별로 4개씩 총 64개를 사용하였다. 표면 거칠기는 40 g의 힘으로 초음파 스케일러는 시편의 표면과 팁이 15도, 핸드 큐렛은 시편의 표면과 큐렛의 날이 45도가 되도록 하여 1초에 1회 5 mm 수평 왕복운동을 30초 동안 시행하여 형성하였다. 각 시편을 주사전자 현미경을 이용하여 관찰하였고, 원자현미경과 표면조도 거칠기 단 차 측정기를 이용하여 표면 거칠기(Ra, ${\mu}m$)를 측정하고 분석하였다. 결과: 주사전자 현미경으로 관찰 결과 표면 거칠기의 증가는 스테인리스 스틸 팁(Group SS)에서 가장 컸으며 구리 합금 팁(Group IS)에서 가장 적게 나타났다. 원자현미경으로 표면 거칠기를 측정한 결과, 스테인리스 스틸 팁(Group SS)은 도재 군과 제3형 금합금 군에서 대조군과 플라스틱 수동 큐렛(Group PS), 구리 합금 팁(Group IS)보다 표면 거칠기가 유의성 있게 크게 나타났고, 구리 합금 팁(Group IS)은 금합금 군에서는 스테인리스 스틸 팁(Group SS)과 플라스틱 수동 큐렛(Group PS)에 비해 표면 거칠기가 유의성 있게 적게 나타났다. 표면조도 거칠기 단 차 측정기로 측정 결과, 스테인리스 스틸 팁(Group SS)은 모든 군에서 대조군 및 플라스틱 수동 큐렛(Group PS)과 구리 합금 팁(Group IS)보다 표면 거칠기가 유의성 있게 크게 나타났으며, 구리 합금 팁(Group IS)은 모든 군에서 스테인리스 스틸 팁(Group SS)에 비해 표면 거칠기가 유의성 있게 적게 나타났다. 제3형 금합금은 도재, 티타늄, 지르코니아 군에 비해 치석제거 기구에 의한 표면 거칠기의 증가가 크게 나타났다(P<.05). 결론: 이상의 연구결과 새로이 개발된 구리 합금 팁(IS)을 적용하였을 때 티타늄 및 치과 수복 재료의 표면 거칠기에 영향을 주지 않음으로써, 임플란트 및 수복치료 된 치아의 치석제거 시 전통적인 스테인리스 스틸 팁(SS)의 대용품으로 유용하게 사용될 수 있을 것으로 사료된다.

• 한국재료학회지
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• 제24권12호
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• pp.682-688
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• 2014

Physical and chemical changes in a polished wafer and in $2.5{\mu}m$ & $4{\mu}m$ epitaxially grown Si layer wafers (Epilayer wafer) after surface treatment were investigated. We characterized the influence of surface treatment on wafer properties such as surface roughness and the chemical composition and bonds. After each surface treatment, the physical change of the wafer surface was evaluated by atomic force microscopy to confirm the surface morphology and roughness. In addition, chemical changes in the wafer surface were studied by X-ray photoemission spectroscopy measurement. Changes in the chemical composition were confirmed before and after the surface treatment. By combined analysis of the physical and chemical changes, we found that diluted hydrofluoric acid treatment is more effective than buffered oxide etching for $SiO_2$ removal in both polished and Epi-Layer wafers; however, the etch rate and the surface roughness in the given treatment are different among the polished $2.5{\mu}m$ and $4{\mu}m$ Epi-layer wafers in spite of the identical bulk structural properties of these wafers. This study therefore suggests that independent surface treatment optimization is required for each wafer type, $2.5{\mu}m$ and $4{\mu}m$, due to the meaningful differences in the initial surface chemical and physical properties.