• Journal of the Korean Society for Heat Treatment
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• v.20 no.2
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• pp.84-93
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• 2007

Microstructural changes during tempering at the temperature range of $300^{\circ}C{\sim}700^{\circ}C$ for the nitrogen-permeated STS 410 and 410L martensitic stainless steels has been investigated. After nitrogen permeation at temperature between 1050 and $1150^{\circ}C$, the surface layer appeared fine $Cr_2N$ of square and rod types in the martensite matrices. Hardness of the nitrogen-permeated surface layer represented 680Hv and 625Hv, respectively, for 410 and 410L steels. It is considered that the fine homogeneously dispersive effect of precipitates by nitrogen caused the increased hardness. Due to the counter current effect of carbon from interior to surface during nitrogen diffusion from surface to interior, the 0.1%C alloyed 410 steel showed the low nitrogen content of 0.025% compared with 0.045% of 410L steel at the distance of $100{\mu}m$ from the surface. Tempering of nitrogen-alloyed 410 and 410L showed the maximum hardness at $450^{\circ}C$. This maximum hardness was considered to be the secondary hardening effect of very fine carbide and nitride. The decrease in hardness at $700^{\circ}C$ was the softening effect of the matrix due to the precipitation of many needle-shaped $Cr_2N$ for 410 steel and the precipitation of coarse nitride of $Cr_2N$ in line with the spherical precipitates with directionality for 410L steel. For 410 steel, the corrosion resistance of nitrogen permeated surface in the solution of 1 N $H_2SO_4$ were nearly unchanged, however the superior corrosion resistance was obtained for nitrogen permeated 410L steel compared to the solution annealed condition.

• Proceedings of the KSME Conference
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• 2004.11a
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• pp.365-371
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• 2004

Generally, fracture of a material is influenced by plastic zone size developed near the crack tip. Hence, according to the relative size of plastic zone in the material, the mechanics as a tool for analyzing the fracture process are classified into three kinds, that is, Linear Elastic Fracture Mechanics, Elastic Plastic Fracture Mechanics, Large Deformation Fracture Mechanics. Even though the plastic zone size is such an important parameter, the practical measurement techniques are very limited and the one for in-situ measurement is not virtually available. Therefore, elastic-plastic FEA has been performed to estimate the plastic zone size. In this study, it is noticed that side necking at the surface is a consequence of plastic deformation and lateral contraction and the relation between the plastic zone and side necking is investigated. FEA for modified boundary layer models with finite thickness, various mode mixities $0^{\circ}$, $30^{\circ}$, $60^{\circ}$, $90^{\circ}$ and strain hardening exponent n=3, 10 are performed. The results are presented and the implication regarding to application to experiment is discussed.

• Tribology and Lubricants
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• v.32 no.1
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• pp.18-23
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• 2016

The effective case depth for case-hardened rolling bearing has been discussed. For this purpose, rolling contact fatigue tests for ball bearings built with inner race of various hardness values were conducted until L₁₀ calculating rating life using a bearing life test machine under radial loading. Then, the distribution of residual stress below the inner raceway, which depended on the hardness value, was measured by X-ray diffraction. As a result, the linear relationship was established between the hardness value of the inner race and the theoretical shear stress evaluated at the depth where the residual stress disappeared below the inner raceway. Based on the relationship, it could be found that the factor of safety in bearing manufacturer’s rules for the effective case depth of case hardened rolling bearings was set higher. However, it could be also found that the hardness values at the depth where the maximum shearing stress acted below the raceway surface in a tapered roller bearing hardened by the carburizing process, were not sufficient for preventing plastic deformation under the basic dynamic load rating. Consequently, further efforts were still required to reduce or to disperse the contact load on the material design of a rolling bearing in order to prolong its life.

• 보존과학연구
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• s.29
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• pp.255-278
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• 2008

Considering the physical quality of the wall body in this study we tried to select a replenishing that is proper for filling the cracked part of the painting wall layer and apply the natural adhesives that have traditionally been used, investigating whether it is possible to substitute those for the chemical adhesive which is used at present time. The result of this study showed the red algae adhesive was, in a weathering environment, as safe as the synthetic resin originated from the polyvinyl acetate which is used generally on the present spot, and it was concluded that although the starch adhesive displayed its superiority in enhancing the strength of the earth mortar and its work disposition, it seemed proper for it to be used as a filling adhesive for the first or midterm layer because it showed a surface hardening phenomenon. And also the glue and fish glue were judged they were not qualified as a filling adhesive due to mold occurring in a environment of high moisture that is a biological problem, showing at same time a weak physical feature in a weathering environment. Therefore it would be possible to use the red algae adhesive or starch one substituting them for the original one sold on the present market, if among natural adhesives the weak points of the them were to be corrected.

• Korean Journal of Materials Research
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• v.12 no.8
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• pp.608-612
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• 2002

The sliding wear behavior of an iron-base NOREM 02 hardfacing alloy was investigated in the temperature range of $25～250^{\circ}C$ under a contact stress of 103MPa (15ksi). With increasing temperature, the wear loss of Norem 02 in water increased slightly up to $180^{\circ}C$ at which Norem 02 showed the wear loss of 2.1mg. The wear resistance of Norem 02 resulted from the surface hardening due to the strain-induced phase transformation from austenite to $\alpha$'martensite during sliding wear. The wear loss of Norem 02 was smaller in water compared to air at same temperature because the water could be served as a sort of lubricant. The wear mode of NOREM 02 changed abruptly to severe adhesive wear at $190^{\circ}C$ and galling occurred above $200^{\circ}C$. It was caused that the strain- induced phase transformation took place below $180^{\circ}C$ while not above $190^{\circ}C$. Therefore, Norem 02 was considered to be inadequate at high temperature service area.

• Journal of Forest and Environmental Science
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• v.34 no.5
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• pp.388-394
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• 2018

An efficient and reproducible protocol for in vitro germination of seeds of Couroupita guianensis has been developed in the present study. Couroupita guianensis is a medicinally important tree and categorized as threatened plant species by the IUCN. The seeds were surface sterilized using 0.1% $HgCl_2$ and inoculated on MS (Murashige and Skoog) and Woody Plants (Llyod and McCown) medium. The seeds with partially removed seed coat responded better (100%) on half strength MS medium as compared to the full (51%), one-fourth strength MS (79%) and the WP medium. Half strength MS medium conjunct with $2.0mg{\cdot}L^{-1}$ indole-3 butyric acid (IBA) was found best among the different types of auxins and cytokinins tested for seed germination, as all the seeds germinated on this medium combination. The seedlings were successfully hardened in the greenhouse and restored in the field with 83% survival rate. The protocol can be used as conservation measure for large scale multiplication of this threatened forest tree species.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.08a
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• pp.403-411
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• 1999

The steel plate for shadow mask is used in a Cathode-ray tube of TV monitor and is the strictest product in surface quality because hundreds thousand of holes are perforated in a plane of 25 ${\times}$25 inches. To mass-produce this product, a reversible cold rolling mill for silicon steel was used and the rolling technology and the activity for quality improvement are described in this work. Because the steel plate is a mild steel, which is very sensitive to strip-breakage even in a low tension, we reset the minimum tension values matching to the operating conditions. The roll mark due to the multi-segmented araangement of shape controlling roll was prevented by hardening the intermediate shape controlling roll and by changing the existing working-roll into a HSS (Hig Speed Steel) roll. The scratch caused by the speed difference between a idle roll and a strip was prevented by increasing the roll roughness. With these activities, the steel plate for shadow mask can be stable. The continuous improvement of quality is, however, required for the customer satisfaction both of domestic and overseas market.

• Transactions of Materials Processing
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• v.18 no.8
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• pp.640-645
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• 2009

Recently, boss and rib test based on backward extrusion process was proposed to quantitatively evaluate the interfacial friction condition in bulk forming process. In this test, the tube-shaped punch with hole pressurizes the workpiece so that the boss and rib are formed along the hole and outer surface of the punch. It was experimentally and numerically revealed that the height of boss is higher than that of the rib under the severe friction condition. This work is focused on the effect of the punch design and flow stress on deformation pattern in boss and rib test. From the boss and rib test simulations, it was found that there is slight variation in both the heights of boss and rib according to the length of punch land, nose radius, and face angle. However the hole diameter of the punch and the clearance between the punch and die have a significant influence on the calibration curves showing the heights of the boss and rib. In addition, the effect of flow stress on the calibration curves was investigated through FE simulations. It was found that there is no effect of strength coefficient of the workpiece on the calibration curves for estimation of friction condition. On the other hand, the strain-hardening exponent of the workpiece has a significant influence on the calibration curve.

• Proceedings of the KSME Conference
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• 2008.11a
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• pp.1806-1809
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• 2008

Study that form micro pattern by direct ink jet printing method is getting attention recently. Direct ink jet printing spout fine droplet including nano metal particle by force or air pressure. There is reason which ink jet printing method is profitable especially in a various micro-patterning technology. It can embody patterns directly without complex process such as mask manufacture or screen-printing for existent lithography. In this study, research of a technology that ejects fine droplet form of Pico liter and forms metal micro pattern was carried with inkjet head of piezoelectricity drive system. Droplet established pattern while ejecting consecutively and move on the surface at the fixed speed. Patterns formed in ink are mixed with organic solvent and polymer that act as binder. So added thermal hardening process after evaporate organic solvent at isothermal after printing. I executed high frequency special quality estimation of CPW transmission line to confirm electrical property of manufactured circuit board. We tried a large area printing to confirm application possibility of an ink jet technology.

• Journal of the Korean Society for Advanced Composite Structures
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• v.5 no.4
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• pp.1-10
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• 2014

A progressive failure analysis procedure for composite laminates is developed in here and in the companion paper. An anisotropic plastic constitutive model for fiber-reinforced composite material, is developed, which is simple and efficient to be implemented into computer program for a predictive analysis procedure of composites. In current development of the constitutive model, an incremental elastic-plastic constitutive model is adopted to represent progressively the nonlinear material behavior of composite materials until a material failure is predicted. An anisotropic initial yield criterion is established that includes the effects of different yield strengths in each material direction, and between tension and compression. Anisotropic work-hardening model and subsequent yield surface are developed to describe material behavior beyond the initial yield under the general loading condition. The current model is implemented into a computer code, which is Predictive Analysis for Composite Structures (PACS), and is presented in the companion paper. The accuracy and efficiency of the anisotropic plastic constitutive model are verified by solving a number of various fiber-reinforced composite laminates with and without geometric discontinuity. The comparisons of the numerical results to the experimental and other numerical results available in the literature indicate the validity and efficiency of the developed model.