• Title/Summary/Keyword: surface aging

Search Result 650, Processing Time 0.028 seconds

Effects of Oxygen Plasma Treatment on the Wettability of Polypropylene Fabrics

  • Kwon, Young Ah
    • Fashion & Textile Research Journal
    • /
    • v.16 no.3
    • /
    • pp.456-461
    • /
    • 2014
  • The objective of this study is to give PP(polypropylene) fabric a good affinity for water. Oxygen plasma was treated to PP fabrics in a commercial glow discharge reactor with different RF power, discharge pressure, and reaction time. The PP fiber surfaces were characterized by the measurement of contact angle and ESCA. A JEOL scanning electron microscope was used to observe the surface morphology of fibers. The spontaneous water uptake amount of PP fabrics was determined by the demand wettability test. To determine the effect of aging on the surface properties of $O_2$ plasma treated PP, all the above measurements of the samples were carried out after 1, 7, 30, 60, and 150 days. The results are as follows. The PP fiber surfaces treated by $O_2$ plasma treatment have a chemical composition that consisted of various oxygen containing polar groups. Consequently, the contact angles of the treated PP fibers decreased, which improved the water uptake rate of PP fabrics. Surface roughness of the treated PP affected the fabric wettabiity as well. Wettability of the treated PP decreased and leveled off with aging. The $O_2$ plasma treatment is a simple and effective method to increase the water uptake rate of PP fabrics.

A Study on the Improvement of Physical Properties for Titanium Alloy by the Grinding Conditions (연삭가공조건에 따른 티타늄 합금의 물성치 향상에 관한 연구)

  • Kim, Won Il;Lee, Yun Kyung;Wang, Duck Hyun;Heo, Soon
    • Journal of the Korean Society of Industry Convergence
    • /
    • v.4 no.3
    • /
    • pp.237-242
    • /
    • 2001
  • Ti-6Al-4V alloy can be obtained the stability of organization and product treasure, the evaluation of the cutting ability and the mechanical characteristics after the heat treatment of annealing, solution and aging. The difficulty in machining titanium alloy is how treat the heat generated during the process. Because the heat conductivity of titanium alloy is regardfully low, the heat generated during grinding is accumulated in workpiece. and it causes the increasing of grinding wheel grits' wear and makes the ground surface rough. So, these characteristics in grinding of titanium alloy will change the mechanical properties of the titanium alloy. From this study. the mechanical characteristics of annealed one and solution and aging one treated Ti-6Al-4V alloy after grinding was concerned with checking out the bending strength and hardness. For the result, both of bending strength and hardness were increased at the burned area on the surface. Roughness value was remarkably high at the table speed of 10m/min.

  • PDF

Evaluation of intaglio surface trueness, wear, and fracture resistance of zirconia crown under simulated mastication: a comparative analysis between subtractive and additive manufacturing

  • Kim, Yong-Kyu;Han, Jung-Suk;Yoon, Hyung-In
    • The Journal of Advanced Prosthodontics
    • /
    • v.14 no.2
    • /
    • pp.122-132
    • /
    • 2022
  • PURPOSE. This in-vitro analysis aimed to compare the intaglio trueness, the antagonist's wear volume loss, and fracture load of various single-unit zirconia prostheses fabricated by different manufacturing techniques. MATERIALS AND METHODS. Zirconia crowns were prepared into four different groups (n = 14 per group) according to the manufacturing techniques and generations of the materials. The intaglio surface trueness (root-mean-square estimates, RMS) of the crown was measured at the marginal, axial, occlusal, and inner surface areas. Half of the specimens were artificially aged in the chewing simulator with 120,000 cycles, and the antagonist's volume loss after aging was calculated. The fracture load for each crown group was measured before and after hydrothermal aging. The intaglio trueness was evaluated with Welch's ANOVA and the antagonist's volume loss was assessed by the Kruskal-Wallis tests. The effects of manufacturing and aging on the fracture resistance of the tested zirconia crowns were determined by two-way ANOVA. RESULTS. The trueness analysis of the crown intaglio surfaces showed surface deviation (RMS) within 50 ㎛, regardless of the manufacturing methods (P = .053). After simulated mastication, no significant differences in the volume loss of the antagonists were observed among the zirconia groups (P = .946). The manufacturing methods and simulated chewing had statistically significant effects on the fracture resistance (P < .001). CONCLUSION. The intaglio surface trueness, fracture resistance, and antagonist's wear volume of the additively manufactured 3Y-TZP crown were clinically acceptable, as compared with those of the 4Y- or 5Y-PSZ crowns produced by subtractive milling.

An experimental study on hydrothermal degradation of cubic-containing translucent zirconia

  • Kengtanyakich, Santiphab;Peampring, Chaimongkon
    • The Journal of Advanced Prosthodontics
    • /
    • v.12 no.5
    • /
    • pp.265-272
    • /
    • 2020
  • PURPOSE. The aims of this study were to investigate mechanical properties and hydrothermal degradation behaviour of the cubic-containing translucent yttrium oxide stabilized tetragonal zirconia polycrystal (Y-TZP). MATERIALS AND METHODS. Four groups of Y-TZP (T, ST, XT, and P), containing different amount of cubic crystal, were examined. Specimens were aged by autoclaving at 122℃ under 2 bar pressure for 8 h. Phase transformation was analyzed using X-ray diffraction (XRD) to measure phase transformation (t→m). Kruskal-Wallis test was used to determine the difference. Surface hardness, biaxial flexural strength, and fracture toughness in values among the experimental groups and verified with Wilcoxon matched pairs test for hardness values and Mann Whitney U for flexural strength and fracture toughness. RESULTS. XRD analysis showed no monoclinic phase in XT and P after aging. Only Group T showed statistically significant decreases in hardness after aging. Hydrothermal aging showed a significant decrease in flexural strength and fracture toughness in group T and ST, while group XT and P showed no effect of aging on fractural strength and fracture toughness with P<.05. CONCLUSION. Hydrothermal aging caused reduction in mechanical properties such as surface hardness, biaxial flexural strength, and fracture toughness of Y-TZP zirconia. However, cubic-containing zirconia (more than 30% by volume of cubic crystal) was assumed to have high resistance to hydrothermal degradation. Clinical significance: Cubic-containing zirconia could withstand the intraoral aging condition. It could be suggested to use as a material for fabrication of esthetic dental restoration.

Effect of Aging Treatment on Fracture Characteristics of High Strength Al-Alloy (고력 알루미늄 합금의 파괴특성에 관한 시효처리의 영향)

  • Moon, Chang-Kweon;Oh , Sae-Kyoo
    • Journal of the Korean Society of Fisheries and Ocean Technology
    • /
    • v.20 no.1
    • /
    • pp.23-29
    • /
    • 1984
  • Nowdays, the high strength aluminum alloys are broadly used for structural purpose, but the practical strengthening method by aging treatment are not much available. So that, in this study, in order to investigate the effect of aging treatment for strengthening on the fracture characteristics of the domestic high strength Al alloy (A2024BE), the variations of the aging temperature and time were taken after solution treatment. By microstructural examination, and by SEM fractographs of the fractures, the effects of aging temperature and time were investigated, considering on the fracture behaviour. The results obtained are as follows: 1) It was confirmed by microstructural investigation that the aging temperature of $190^{\circ}C$ and the aging time of 12hours were optimal to get more sound microstructure with distribution of uniform precipitation. 2) By step aging treatment, the proper aging time for obtaining the similar microstructure without any microstructural defects could be shortened in half the normal aging time. 3)By examining the SEM fractographs of the fracture surface, it was found that, regardless of the aging treatment time and temperature, all were intergranular ductile fractures, but the aging treatment at $190^{\circ}C$ for 12 hours resulted in dimple-type-transgranular and intergranular-ductile-frature.

  • PDF

Tracking Performance Test of Polymer Insulator with Salt Solution which is added Surface Active Agent (계면활성제가 첨가된 염수용액에 따른 폴리머 애자의 트래킹 성능 평가)

  • Cho, Han-Goo;Han, Dong-Hee;Lee, Un-Yong;Lim, Kee-Joe;Choi, In-Hyuk
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2004.07b
    • /
    • pp.1121-1124
    • /
    • 2004
  • Aging test to estimate life property of polymer insulator is executed through several international standard such as IEC 61109 and CEA tracking wheel test, but is not getting clear conclusion yet. There are two methods in the diagnosis method of polymer insulator such as off-line and on-line. The diagnosis methods in off-line are external condition analysis by the eye, contaminant analysis on surface, surface analysis, pollution withstand voltage test, power frequency flashover voltage test, lightning impulse flashover test, tensile fracture load test and flexural load test. The diagnosis methods in off-line most are the method for virgin and last aged sample. However, the diagnosis method in on-line is method that can be evaluate sample state as progressing continuously aging test in beginning, The diagnosis method in on-line is arranged as following: leakage current measurement, electric field, surface state investigation, thermal image, emitting light measurement and then so. In this paper, the tracking performance of polymer insulator with salt solution which is added surface active agent. The diagnosis of insulator sample has been analyzed by leakage current and visual examination.

  • PDF

A Study on the Surface Properties of Epoxy Insulator by Water Degradation (수분열화에 의한 에폭시절연재료의 표면특성에 관한 연구)

  • 임경범;이백수;김종택;정무영;황명환;이덕출
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 1998.06a
    • /
    • pp.199-202
    • /
    • 1998
  • In examining application of polymer as electrical insulators, it is very important to perform accelerated aging test substituted the process which polymer insulator is degraded for long-time by the process of short-time. The purpose of this paper is to examine the properties of water degradation which affect on the efficiency of epoxy insulator. To do this, the surface properties on epoxy insulating material have been investigated after long-time accelerated degradation in boiling water condition. The experimental results showed the contact angle and surface resistivity after treatment to decrease the sample of water treatment. In dielectric properties, dielectric constant was increased by the aging development with water treatments.

  • PDF

Nondestructive Evaluation for Thermally Degraded Co-base Superalloy by Scanning Acoustic Microscope (초음파현미경을 이용한 Co 기 초내열 합금 열화재의 비파괴평가)

  • Kim, Chung-Seok;Song, Jin-Hun;Kwon, Sook-In;Lim, Jea-Seang;Park, Ik-Keun
    • Proceedings of the KSME Conference
    • /
    • 2004.04a
    • /
    • pp.336-341
    • /
    • 2004
  • This research investigates the feasibility of ultrasonic microscope for nondestructive assessment of thermal degradation in artificially aged commercial Co-base superalloy, FSX414. This alloy has been used for high temperature structure applications such as stationary gas turbine blade and nozzle chamber in fossil plant. Microstructural change was found that the fine carbides became coarser and spheroidized in matrix as aging time increased. The leaky surface acoustic wave velocity gradually decreases by a maximum of 4.7% with increasing aging time up to 4,000hours. However, the longitudinal wave velocity has a little change. Also, it has a good correlation between leaky surface acoustic wave velocity and Vickers hardness. Consequently, LSAW can be used to examine the degree of degradation in thermally aged Co-base superalloy.

  • PDF

Improvement of Surface Properties of CP-Titanium by Thermo-Chemical Treatment (TCT) Process (열확산처리 공정에 의한 순수 타이타늄의 표면특성 향상 연구)

  • Jeong, Hyeon-Gyeong;Lee, Dong-Geun;Yaskiv, O.;Lee, Yong-Tai;Hur, Bo-Young
    • Korean Journal of Metals and Materials
    • /
    • v.49 no.9
    • /
    • pp.692-698
    • /
    • 2011
  • The thermo-chemical treatment (TCT) process was applied to achieve surface hardening of CP titanium. The following three different surface modification conditions were tested so that the best surface hardening process could be selected:(a) PVD, (b) TCT+PVD, and (c) TCT+Aging+PVD. These specimens were tested and analyzed in terms of surface roughness, wear, friction coefficient, and the gradient of hardening from the surface of the matrix. The three test conditions were all beneficial to improve the surface hardness of CP titanium. Moreover, the TCT treated specimens, that is, (b) and (c), showed significantly improved surface hardness and low friction coefficients through the thickness up to $100{\mu}m$. This is due to the functionally gradient hardened surface improvement by the diffused interstitial elements. The hardened surface also showed improvement in bonding between the PVD and TCT surface, and this leads to improvement in wear resistance. However, TCT after aging treatment did not show much improvement in surface properties compared to TCT only. For the best surface hardening on CP titanium, TCT+PVD has advantages in surface durability and economics.

The Investigation on Thermal Aging Characteristics of Oil-Paper Insulation in Bushing

  • Liao, Rui-jin;Hu, En-de;Yang, Li-jun;Xu, Zuo-ming
    • Journal of Electrical Engineering and Technology
    • /
    • v.10 no.3
    • /
    • pp.1114-1123
    • /
    • 2015
  • Bushing is the key link to connect outer and inner insulating systems and also the essential electric accessory in electric power system, especially in the high voltage engineering (AC 1000kV, DC 800kV). This paper presented the experimental research of thermal aging characteristic of oil-paper insulation used in bushing. A thermally accelerated aging experiment at 90℃ was performed. The bushing models containing five layers of paper were sealed into the aging vessels and further aged for 250 days. Then several important parameters associated with the aging were observed and evaluated. The results showed that the degree of polymerization (DP) of papers gradually decreased. The DP values of outermost layer and middle layer fit well into the second-order kinematic model and first-order kinematic model, respectively. Less deterioration speed of the inter-layer paper than outer layer was confirmed by the variation of DP. Hydrolysis was considered as the main cause to this phenomenon. In addition, the logarithm of the furfural concentrations in insulation oil was found to have good linear relationship with DP of papers. Interestingly, when the aging time is about 250 days and DP is 419, the aging process reaches an inflection point at which the DP approaches the leveling off degree of polymerization (LODP) value. Both tanδ and acid number of oils increased, while surface and volume resistivity of papers decreased. The obtained results demonstrated that thermal aging and moisture absorbed in papers brought great influence to the degradation of insulating paper, leading to rapid decrease of DP and increase of the tanδ. Thus, the bushing should be avoided from damp and real-time monitoring to the variation of tanδ and DP values of paper is an effective way to evaluate the insulation status of bushing.