• 제목/요약/키워드: surface aging

검색결과 650건 처리시간 0.025초

제V급 복합레진 수복물의 표면전색이 미세변연누출에 미치는 효과 (The Effect of Surface Sealing on the Microleakage of Class V Composite Resin Restorations)

  • 윤연희;현홍근;김영재;김정욱;장기택;이상훈;김종철;한세현
    • 대한소아치과학회지
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    • 제34권3호
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    • pp.359-369
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    • 2007
  • 본 연구는 다양한 순환 및 시효 조건 하에서 제V급 복합레진 수복물의 표면전색이 미세변연누출에 미치는 효과에 대해 알아보고자 하였다. 100개의 건전한 소구치의 협면에 제V급 와동을 형성하고 제조사의 지시대로 광중합형 복합레진으로 수복하였다. 무작위로 나누어 표면전색을 시행하지 않는 I군과 표면을 산부식 후 표면전색을 시행한 II군으로 설정한 후 열순환(thermocycling)을 하였다. 각 군에서 하위군(A군= 열순환 외 다른 시효조건이 없는 군, B군=칫솔질군, C군=부하순환군, D군=칫솔질과 부하순환을 모두 시행한 군, E군=6개월간 증류수에 보관한 군)으로 나누어 각각에 맞는 시효조건을 시행하였다. 2% methylene blue 용액에 침윤시켜 변연의 미세누출정도를 평가하여 다음과 같은 결과를 얻었다. 1. 표면전색을 시행하지 않은 군의 교합변연과 치은변연에서 시효조건에 따른 미세누출의 유의한 차이는 보이지 않았다(p>0.05). 2. 표면전색을 시행한 군의 교합변연에서는 시효조건에 따른 미세누출의 유의한 차이가 없었다(p>0.05). 3. 표면전색을 시행한 군의 치은변연에서는 부하순환이나 6개월간 증류수에서 보관하는 시효과정을 거친 군에서 미세누출이 유의하게 크게 나타났다(p<0.05). 4. 시효조건이 없는 군과 칫솔질군의 경우, 표면전색을 시행한 군이 표면전색을 시행하지 않은 군에 비해 유의하게 적은 미세누출결과를 보였다(p<0.05). 5. 부하순환을 시행한 군과 6개월간 증류수에서 보관한 경우에는 표면전색을 시행한 군과 표면전색을 시행하지 않은 군 사이에 미세누출의 차이가 있었지만 유의차가 없었다(p>0.05). 따라서 이 연구의 결과는 변연부분의 미세간격으로 침투한 표면전색제가 처음에는 미세누출을 감소하는데 효과를 보여주었으나, 교합시 교두가 휘어져서 생기는 응력과 장기간의 수분흡수로 인한 변화를 견디기에 불충분함을 보여주었다.

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SALT FOG시 EPDM고분자애자의 누설전류파형과 스펙트럼분석 (Leakage Current Waveforms and Spectrum Analysis on Polymer Insulator of EPDM under Salt fog)

  • 박재준;양태규
    • 한국정보통신학회:학술대회논문집
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    • 한국해양정보통신학회 2004년도 춘계종합학술대회
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    • pp.500-504
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    • 2004
  • 본 연구에서는 EPDM 고분자애자의 염무량 변화(salt:l0g, 25g, 50g, deionized water: 1000g)에 따른 표면방전과 환경적인 변화(salt fog 및 clean fog 그리고 raim)에 대한 누설전류 파형의 결과를 알아보았다. 기본파 및 3고조파 그리고 5고조파의 변화양상을 과전초기로부터 섬락시에 이르기까지 나타내었다. 표면열화의 진단기법을 개발하기위해서 누설전류파형의 주파수 스펙트럼을 이용하였고, 고분자애자의 표면열화에대한 환경적인 영향(clean fog, salt fog, rain)을 연구 하였다. 염분량의 변화시 기본파에 대한 저주파 고조파인 3고조파 및 5고조파에 대한 백분율(왜곡도)의 변화를 이용하여 표면 열화상태 및 정도를 정량화(a standard capacity)하여 나타내었다. 기본파에 대한 고조파 백분율인 왜곡율은 고분자 애자의 표면조건을 평가하는데 필요한 지시자라는 사실을 알 수 있었다.

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Stochastic Estimation of Acoustic Impedance of Glass-Reinforced Epoxy Coating

  • Kim, Nohyu;Nah, Hwan-Seon
    • 비파괴검사학회지
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    • 제34권2호
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    • pp.119-127
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    • 2014
  • An epoxy coating applied to the concrete surface of a containment building deteriorates in hazardous environments such as those containing radiation, heat, and moisture. Unlike metals, the epoxy coating on a concrete liner absorbs and discharges moisture during the degradations process, so it has a different density and volume during service. In this study, acoustic impedance was adopted for characterizing the degradation of a glass-reinforced epoxy coating using the acoustic reflection coefficient (reflectance) on a rough epoxy coating. For estimating the acoustic reflectance on a wavy epoxy coating surface, a probabilistic model was developed to represent the multiple irregular reflections of the acoustic wave from the wavy surface on the basis of the simulated annealing technique. A number of epoxy-coated concrete specimens were prepared and exposed to accelerated aging conditions to induce an artificial aging degradation in them. The acoustic impedance of the degraded epoxy coating was estimated successfully by minimizing the error between a waveform calculated from the mathematical model and a waveform measured from the surface of the rough coating.

15$0^{\circ}C$에서 시효처리한 80Sn-20Pb 합금 도금층의 파괴특성에 전착조건이 미치는 영향 (Effects of Electrodeposition condition on the fracture characteristics of 80Sn-20Pb electrodeposits aged at 15$0^{\circ}C$)

  • 김정한;서민석;권혁상
    • 한국표면공학회지
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    • 제27권5호
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    • pp.292-302
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    • 1994
  • Alloy deposits of 80Sn-20Pb, electroplated on Cu-based leadframe alloy from an organic sulfonate bath were aged at $150^{\circ}C$ to form intermetallic phases between substrate and deposit, and effects of the deposit morphology, influenced by deposition conditions, on the fracture resistance of the 80Sn-20Pb deposit aged at $150^{\circ}C$ were examined. The growth rate of intermetallic compound layer on aging depended on the microstructure of deposit ; it was fastest in deposit formed using pulse current in bath without grain refining additive, but slowest in deposit formed using dc current in bath containing grain refining additive in spite of similar structure with equivalent grain size. The grain refining additive incorporated in electrodeposit appears to inhibit diffusion of atoms on aging, resulting in slow growth of intermetallic layer in the thickness direction but substantial growth in the lateral one. Density of surface cracks that were occurring when samples were subjected to the $90^{\circ}$-bending test increased with increasing the thickness of intermatallic layer on aging. For the same aged samples, the surface crack density of the sample electrodeposited from a bath containing the grain refining additive was the least due to the inhibiting effect of the additive incorporated into the deposit during electrolysis on atomic diffusion.

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코너 특정점 기반의 영상분석을 활용한 진공단열재 결함 검출 (Defect detection of vacuum insulation panel using image analysis based on corner feature detection)

  • 김범수;양정현;김연원
    • 한국표면공학회지
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    • 제55권6호
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    • pp.398-402
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    • 2022
  • Vacuum Insulation Panel (VIP) is an high energy efficient insulation system that facilitate slim but high insulation performance, based on based on a porous core material evacuated and encapsulated in a multi-barrier envelope. Although VIP has been on the market for decades now, it wasn't until recently that efforts have been initiated to propose a standard on aging testing. One of the issues regarding VIP is its durability and aging due to pressure and moisture dependent increase of the initial low thermal conductivity with time. It is hard to visually determine at an early stage. Recently, a method of analyzing the damage on the a material surface by applying image processing technology has been widely used. These techniques provide fast and accurate data with a non-destructive way. In this study, the surface VIP images were analyzed using the Harris corner detection algorithm. As a result, 171,333 corner points in the normal packaging were detected, whereas 32,895 of the defective packaging, which were less than the normal packaging. were detected. These results are considered to provide meaningful information for the determination of VIP condition.

금 합금 도금층의 접촉저항에 미치는 합금원소의 영향 (Effect of alloying elements on the contact resistance of electrodeposited gold films)

  • 이지웅;손인준
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2013년도 춘계학술대회 논문집
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    • pp.184-184
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    • 2013
  • 본 연구에서는 금 합금 도금층의 접촉저항에 미치는 첨가 합금원소의 영향을 조사하였다. 또한 표면실장을 위한 솔더링 공정에서 도금층에 가해지는 열이력이 접촉저항 값에 미치는 영향을 조사하기 위해서, $260^{\circ}C$에서 thermal aging을 실시한 후, 접촉저항을 측정하였다. 합금원소의 종류에 따라서 thermal aging후의 접촉저항 값이 변하는 요인을 조사하기 위해서 XPS를 이용하여 표면분석을 실시하였다.

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오손액에 의한 EPDM rubber의 표면열화 현상 (Surface Aging Phenomena of EPDM rubber by Contaminant)

  • 이철호;김상욱
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1997년도 추계학술대회 논문집
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    • pp.317-320
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    • 1997
  • The paper reports on a study of the influence of the size of the particles of alumina trihydrate(ATH) filler on the surface aging characteristics of ehylene propylene diene terpolymer(EPDM). A fixed 100pph concentration of the filler of ATH was used (or all particle sizes from 0.7 to 20$\mu\textrm{m}$, It is show that hysteresis of contact angle and leakage current increase with increasing particle size, whereas tracking resistance decrease with increasing particle size.

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트래킹 휠과 복합열화시험에 의한 폴리머 애자의 성능 평가 (Performance Evaluation of Polymer Insulator using Tracking Wheel and Multi-Aging Test)

  • 조한구;안명상;한세원;허종철;이운용
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 하계학술대회 논문집
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    • pp.119-122
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    • 2000
  • Recently polymer insulators are being used for outdoor high voltage applications. Polymer insulators for transmission line have significant advantages over porcelain and glass insulators, especially for ultra-high voltage transmission lines. Their advantages are light weight, vandalism resistance and hydrophobicity. Polymer insulators are a relatively new technology, but their expected life is still unknown. Therefore these estimating technique are very important. Their life time is related to weathering and operating condition. Multi-aging test is requested because aging factor is occurred by multi-aging than unique aging. The aging test about polymer insulators have mainly carried out by IEC 61109. This paper presents multi-stress chamber experiments and tracking wheel test to examine the tracking and erosion performance of polymer insulator for transmission. Multi-stress testing is able to demonstrate deficiencies of polymer insulator materials and designs, including the nature of interfaces in insulation design. We have investigated IEC 61109 Annex C (5000h aging test) and CEA tracking wheel test as test methods of artificial accelerated aging. The aging degree of polymer insulator is estimated by leakage current, measurement of hydrophobicity degree, damage conditions of insulator surface, withstand voltage test etc.

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티타늄합금의 와이어 방전가공시 방전가공 조건의 영향 (Effect of EDM Conditions when wire-EDM for Titanium Alloy)

  • 김종업;왕덕현;이윤경;김원일
    • 한국공작기계학회:학술대회논문집
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    • 한국공작기계학회 2001년도 춘계학술대회 논문집(한국공작기계학회)
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    • pp.281-286
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    • 2001
  • Titanium alloy conducted in this experimental study has superior corrosive resistant and is mainly used in aerospace, automotive and petro-chemical industries. It is also treated with important materials of domestic goods due to improvement of the standard of living. In this study specimens were processed in the wire EDM after annealing, solution treatment and aging. Results were obtained through repeated experments of main rough process and finish process with the change of process parameters. Processing characteristics such as surface hardness, surfaces roughness, shape of processed surface and components were measured. The results confirmed that the above mentioned elements were improved in accordance with the number of process. Therefore, the optimal wire EDM condition in accord with processing characteristics is proposed in this experiment.

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Effect of artificial aging on mechanical and physical properties of CAD-CAM PMMA resins for occlusal splints

  • Julia Correa Raffaini;Eduardo Jose Soares;Rebeca Franco de Lima Oliveira;Rocio Geng Vivanco;Ayodele Alves Amorim;Ana Lucia Caetano Pereira;Fernanda Carvalho Panzeri Pires-de-Souza
    • The Journal of Advanced Prosthodontics
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    • 제15권5호
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    • pp.227-237
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    • 2023
  • PURPOSE. This study aimed to assess and compare the color stability, flexural strength (FS), and surface roughness of occlusal splints fabricated from heat-cured acrylic resin, milled polymethyl methacrylate (PMMA)-based resin, and 3D-printed (PMMA) based-resin. MATERIALS AND METHODS. Samples of each type of resin were obtained, and baseline measurements of color and surface roughness were recorded. The specimens were divided into three groups (n = 10) and subjected to distinct aging protocols: thermomechanical cycling (TMC), simulated brushing (SB), and control (without aging). Final assessments of color and surface roughness and three-point bending test (ODM100; Odeme) were conducted, and data were statistically analyzed (2-way ANOVA, Tukey, P <.05). RESULTS. Across all resin types, the most significant increase in surface roughness (Ra) was observed after TMC (P < .05), with the 3D-printed resin exhibiting the lowest Ra (P < .05). After brushing, milled resin displayed the highest Ra (P < .05) and greater color alteration (∆E00) compared to 3D-printed resin. The most substantial ∆E00 was recorded after brushing for all resins, except for heat-cured resin subjected to TMC. Regardless of aging, milled resin exhibited the highest FS (P < .05), except when compared to 3D-printed resin subjected to TMC. Heat-cured resin exposed to TMC demonstrated the lowest FS, different (P < .05) from the control. Under control conditions, milled resin exhibited the highest FS, different (P < .05) from the brushed group. 3D-printed resin subjected to TMC displayed the highest FS (P < .05). CONCLUSION. Among the tested resins, 3D-printed resin demonstrated superior longevity, characterized by minimal surface roughness and color alterations. Aging had a negligible impact on its mechanical properties.