• 한국분말재료학회지
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• 제8권2호
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• pp.98-103
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• 2001

Metallic tin powder with diameter less than 50 nm was synthesized by inert gas condensation method and subsequently oxidized to tin oxide ($SnO_2$) along the two heat-treatment routes. The $SnO_2$ powder of single phase with a tetragonal structure was obtained by the heat-treatment route with intermediate annealing step-wise oxidation, whereas the $SnO_2$ powder with mixture of orthorhombic and tetragonal phases was obtained by the heat-treatment route without intermediate annealing (direct oxidation). $SnO_2$ gas sensors fabricated from the nano-phase $SnO_2$ powders were investigated by structural observations as well as measurement of electrical resistance. The $SnO_2$ gas sensors fabricated from the mixed-phase powder exhibited much lower sensitivity against $H_2$ gas than those fabricated from the powder of tetragonal phase. Reduced sensitivity of gas sensors with the new orthorhombic phase was attributed to detrimental effects of phase boundaries between orthorhombic and tetragonal phases and many twin boundaries on the charge mobility.

• 한국산업융합학회 논문집
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• 제23권4_1호
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• pp.531-539
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• 2020

When injection mold is repeatedly used for mass production, fatigue phenomenon due to cyclic stress may occur. The surface and interior of structure might be damaged due to cyclic stress or strain. The objective of this study was to analyze failure of SCM435 high-tension bolts connecting upper and lower parts of a three-stage injection molding machine. These bolts have to undergo an accurate heat treatment to prevent the formation of chromium carbide and the action of dynamic stresses. Bolts were fractured by cyclic bending stress in the observation of ratchet marks and beach marks. Damaged specimen showed an acicular microstructure. Impurity was observed. Chromium carbide was observed near the crack origin. Both shape parameters of the Vickers hardness were similar. However, the scale parameter of the damaged specimen was about 20% smaller than that of the as-received specimen. Much degradation occurred in the damaged specimen. Bolts should undergo an accurate heat treatment to prevent the formation of chromium carbide. They must prevent the action of dynamic stresses. Bolts need accurate tightening and accuracy of heat treatment and screws need compression residual stress due to peening.

• 한국재료학회지
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• 제19권4호
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• pp.207-211
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• 2009

In this study, we attempted to develop a convenient aluminizing process, using Al-Ti mixed slurry as an aluminum source, to control the Al content of the aluminized layer as a result of a one-step process and can be widely adopted for coating complex-shaped components. The aluminizing process was carried out by the heat treatment on disc and rod shaped S45C steel substrates with Al-Ti mixed slurries that were composed of various mixed ratios (wt%) of Al and Ti powders. The surface of the resultant aluminized layer was relatively smooth with no obvious cracks. The aluminized layers mainly contain an Fe-Al compound as the bulk phase. However, the Al concentration and the thickness of the aluminized layer gradually decrease as the Ti proportion among Al-Ti mixed slurries increases. It has also been shown that the Al-Ti compound layer, which formed on the substrate during heat treatment, easily separates from the substrate. In addition, the incorporation of Ti into the substrate surface during heat treatment was not observed.

• 한국분말재료학회지
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• 제26권2호
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• pp.126-131
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• 2019

In the present work, a new hydrogen added argon heat treatment process that prevents the formation of hydrides and eliminates the dehydrogenation step, is developed. Dissolved hydrogen has a good effect on sintering properties such as oxidation resistance and density of greens. This process can also reduce costs and processing time. In the experiment, commercially available Ti-6Al-4V powders are used. The powders are annealed using tube furnace in an argon atmosphere at $700^{\circ}C$ and $900^{\circ}C$ for 120 min. Hydrogen was injected temporarily during argon annealing to dissolve hydrogen, and a dehydrogenation process was performed simultaneously under an argon-only atmosphere. Without hydride formation, hydrogen was dissolved in the Ti-6Al-4V powder by X-ray diffraction and gas analysis. Hydrogen is first solubilized on the beta phase and expanded the beta phases' cell volume. TGA analysis was carried out to evaluate the oxidation resistance, and it is confirmed that hydrogen-dissolved Ti-6Al-4V powders improves oxidation resistance more than raw materials.

• 비파괴검사학회지
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• 제25권1호
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• pp.1-8
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• 2005

본 연구에서는 TV 유리패널의 등색프린지 분포를 광탄성 4단계 위상이동법에 의하여 측정한 실험결과를 제시하였다. 재래식 광탄성법에서는 등색 프린지 차수를 각각의 점에 대해서 수작업으로 측정한다. 4단계 위상이동법을 이용하기 위하여, 원형편광기 요소들은 등색프린지분포가 측정되는 지점 혹은 선상을 따라 등경각 방향에 일치시켜야 한다. 4단계 위상이동법은 원형편광기의 검광판을 $0^{\circ},\;45^{\circ},\;90^{\circ}$ 및 $135^{\circ}$ 회전시켜 얻은 4개의 영상을 이용한다. 4단계 위상이동법을 적용하기 위해서는 등경각이 측정하고자 하는 지점이나 선상에 일치하도록 편광기 요소를 정렬시켜야 한다. 4단계 위상이동법으로부터 얻은 실험결과는 세나르몽보간법에 의해 측정한 값과 비교한 결과 서로 잘 일치하였다. 또한, TV 유리패널의 열처리 전 후에 등색프린지 분포를 비교하였다. 측정 결과, TV 유리패널의 열처리 전 후의 등색프린지 차수는 약 2배정도 차이가 나타났다.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2001년도 추계학술대회 논문집 전기물성,응용부문
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• pp.3-5
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• 2001

ZnO thin films are deposited on $SiO_2$/Si (111) substrate by RF magnetron sputtering. The two-step deposition method is proposed to enhance both the c-axis orientation and the resistivity of ZnO films. This method consists of the following two procedures: the 1 st-deposition for 30 min without oxygen at l00W and the 2nd-deposition with oxygen added in the range of $O_2/(Ar+O_2)=10{\sim}50%$. Effects of thermal treatment on the properties of ZnO films are systematically investigated.

• 한국재료학회지
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• 제21권1호
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• pp.39-45
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• 2011

In this study, the heat flow of the plant scale aluminum extrusion process was investigated to establish optimum continuous heat treatment conditions. During the extrusion of 6061 aluminum alloy, processing parameters such as the extrusion pressure, speed and temperature histories of billets were logged as a function of time. The surface temperature of the billets increased at constant ram speed, while it decreased with decreases of the ram speed. In order to maintain the billet temperature within a solutionizing temperature range prior to the succeeding water quenching step, the ram speed or the temperature of the blower should be controlled. The temperature histories of the billets during the extrusion and hot air blowing processes were successfully simulated by using the velocity boundary model in ANSYS CFX. The methodology to design an optimum process by using a commercial simulation program is described in this study on the basis of the metallurgical validation results of the microstructural observation of the extrudates. The developed model allowed the advantages of taking into account the motion of the extrudate coupled with the temperature change based on empirical data. Calculations were made for the extrudate passing through the isothermal chamber maintained at appropriate temperature. It was confirmed that the continuous heat treatment system is beneficial to the productivity enhancement of the commercial aluminum extrusion industry.

• 한국식품영양과학회지
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• 제39권1호
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• pp.154-158
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• 2010

본 연구에서는 현미 발아 시 침지 및 발아 조건에 따른 GABA 함량의 변화를 분석하고 효과적으로 GABA 함량을 증가시키기 위한 처리조건을 살펴보았다. 발아 현미의 GABA 함량 증가를 위해 침지 전 열처리를 실시하였으며, 한약재로 널리 쓰이는 오미자와 용안육, 구릿대, 천마를 침지수와 발아수로 이용하였을 때의 GABA 함량의 변화를 확인하였다. 실험 결과 $45^{\circ}C$에서의 열처리군이 3977.3 nmol/g로 무처리군에 비해 약 1.4배 정도의 증가 효과를 나타내었다. 또한 한약재를 침지 및 발아수로 이용한 결과 용안육은 3% 추출물을 발아수로 이용하였을 경우가 가장 높은 증가율을 보여주었으며, 오미자는 5% 추출물을 발아수로 이용한 경우가 대조군보다 2.1배로 가장 높은 GABA 함량을 나타내었다. 천마 추출물의 경우는 5% 추출물을 침지수와 발아수로 이용했을 경우 약 2.5배의 증가율을 보여 실험한 한약재 중 가장 높은 효과를 보여주었다. 본 연구 결과는 점차 관심이 높아지고 있는 발아현미 연구에 있어서 기초자료가 될 것으로 예상되며, 쌀 소비촉진에 영향을 미칠 것으로 기대된다.

• 열처리공학회지
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• 제22권1호
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• pp.23-26
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• 2009

Pt nanotubes with diameter of 200 nm were fabricated by simple and convenient method of Template-Wetting Process. Porous alumina membranes were prepared by 2 step anodic oxidation as the template. To improve wetting properties and lower surface energy, pt solution was mixed with polymer. Polymer was removed completely during annealing. Grain growth process of pt nanotubes during baking and furnace annealing was examined by FE-SEM and XRD.

• 한국산학기술학회논문지
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• 제2권2호
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• pp.91-94
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• 2001

Glass ceramics composed of (5-X)$Li_2O$ㆍ$XAg_2O$ㆍ36CaOㆍ$20TiO_2$.27$P_2O_5$(X=1 to 5) were prepared by melting process and 2 step heat treatment for nucleation at$610^{\circ}C$ and crystallization at $730^{\circ}C$, Fabricated crystal phases were $LiTi_2(PO_4)_3$(LTP),$AgTi_2(PO_4)_3$(AgTP)와 $\beta-Ca_3(PO_4)$. Antibacterial effects and characterizations of the glass ceramics as $Ag_2$O content were investigated. Staphylococcus aureus and Salmonella typhi were used in this study. Staphylococcus aureus and Salmonella typhi bacteria were removed 5 hours added after glass ceramics.