• Title/Summary/Keyword: standard amount used

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Establishment of HPLC-UV Analysis Method Validation for Simultaneous Analysis of Standard Compounds of Oplopanax elatus Nakai Stem (HPLC-UV를 이용한 땃두릅나무 줄기의 지표 성분 동시 분석법 확립)

  • Yoo, Nam Ho;Kwon, Yongsoo;Kim, Myong Jo
    • Korean Journal of Pharmacognosy
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    • v.50 no.2
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    • pp.133-140
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    • 2019
  • In our previous study, we found uracil, adenosine, protocatechuic acid, syringin (eleutheroside B) and scoparone (6, 7-dimethoxycoumarin) in the Oplopanax elatus Nakai Stem. High-performance liquid chromatography (HPLC) -UV was used to quality and quantify the internal marker compounds in the O. elatus extract after validation of method with linearity, limit of detection (LOD), limit of quantitation (LOQ), accuracy and precision. The specificity assessment visually confirmed that the substance was detected without the introduction of other substances. The established method showed high linearity of the calibration curve and coefficient of correlation ($R^2$) of over the 0.999. HPLC was reported as five standard compounds equivalent using the following linear equation based on the calibration curve. The accuracy of measurement was 84.34 ~ 119.74% and the relative standard deviation (RSD) value was 0.28 ~ 1.60%. In addition, our established method showed high repeatability. The RSD value was 1.10 ~ 6.81%. So, we found the amount of the internal marker compounds in the O. elatus extract. These results demonstrated that can be used to quality evaluation of the O. elatus.

A Study on the Seismic Protection Performance of Press Fittings for Light Gauge Stainless Steel Pipes (일반배관용 스테인리스강관에 대한 프레스식 관이음쇠의 내진성능에 관한 연구)

  • Baek, Yeal-Sun;Nam, Jun-Seok
    • Fire Science and Engineering
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    • v.31 no.4
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    • pp.65-70
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    • 2017
  • The seismic performance of press fittings is studied, which is one of the weldless joints of stainless steel pipe used in the water piping of recent fire protection system. The piping of this study was constructed based on the piping connection reference of NFPA 13. The permissible displacement of the piping was set as the allowed amount which is given in the Building Structure Standard, and the measurements were repeated 10 times. The Von-mises stress of the piping was 2.48 and 1.25 times of the allowed amount of stress, which was less than the standard, noted three times on the NPPs Allowable Stress for Level D service loading. Therefore, the press fittings shows enough seismic performance.

A study on the Phase Noise Performance of CATV Transmission System (CATV 전송시스템 위상잡음성능에 관한 연구)

  • Lee, Yong-Woo;Oh, Seung-Hyeub
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.10 no.4
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    • pp.199-204
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    • 2010
  • Recently, the transmission amount of information that each single person requires is growing by development of electron information communication technology. So in this paper we analysis the phase noise characteristics to obtain a most suitable of SNR performance request characteristic by BER on CATV transmission system that satisfy performance request DOCSIS 2.0 standard. Especially we get the parameter value of PLL that satisfy phase noise characteristic request standard using developed simulator. Presented method can be used to obtain a performance request standard connection performance request standard of high speed CATV transmission system in the future.

A study on Actual Quantity of Shotcrete Sprayed in a NATM tunnel (NATM 산악터널의 숏크리트 투입율에 관한 연구)

  • Lee, Cheol-Ju;Kim, Sung-Yun;Kim, Dong-Gun;Yoo, Nam-Jae
    • Journal of Industrial Technology
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    • v.29 no.B
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    • pp.57-64
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    • 2009
  • This study has analysed actual overbreak, shotcrete rebound and the ratio between the actual quantity of shotcrete to designed shotcrete measured during a NATM tunnel construction. The measured shotcrete rebound was about 7.2% in average which was about half the allowable rebound (15%), showing shotcrete spraying was performed well. Based on the measurement of excavated tunnel shape, average overbreak was about 28.5cm after tunnel excavation by drill and blasting method. This was about 260% of allowable overbreak. In addition, due to the rebound and overbreak actual amount of shotcrete used in the tunnelling work was about 116.5 % of the designed value. According to the field measurement the ratio of actual shotcrete to designed value showed some relation with standard support pattern, but the size of overbreak did not show the correlation with standard support pattern. Hence current design specifications stating the size of overbreak based entirely on standard support pattern should perhaps be reestablished. The insight into the design guideline regarding overbreak and shotcrete.

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IMPROVEMENT OF I-PICTURE CODING USING INTER-PICTURE PROCESSING

  • Arizumi, Masao;Sagara, Naoya;Sugiyama, Kenji
    • Proceedings of the Korean Society of Broadcast Engineers Conference
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    • 2009.01a
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    • pp.618-622
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    • 2009
  • An improvement of standard encoder has been saturated recently. However, new coding method does not have a compatibility with conventional standard. To solve this problem, new concept coding method that has a semicompatibility with standard may be discussed. On the other hand, cyclic Intra-picture coding is used for access and refreshment. However, I-picture spend large amount of bits. An enhancement of I-picture is desired with keeping its refreshment performance. Further, it's a problem that quality change at the border of GOP because of its independency. To respond these, we propose the coding which is applied an inter-frame processing at the border of GOP. Applied method is the reduction of quantization error using the motion compensated inter-picture processing. In this report, we check the improvement of the efficiency and the compatibility of proposed method. As a result of examination, we recognize that the total gain is maximally 1.2dB in PSNR. Generally, the degradation of performance in standard decoding is smaller than its gain. Also the refreshment performance is tested.

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A study on the phase noise performance improvement of CATV transmission system using the simulator (시뮬레이터를 이용한 CATV 전송시스템 위상잡음성능 개선에 관한 연구)

  • Lee, Yong-Woo;Oh, Seung-Hyeub;Chang, Sang-Hyun;Lee, Il-Kyoo
    • Journal of Satellite, Information and Communications
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    • v.5 no.1
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    • pp.1-5
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    • 2010
  • Recently, the transmission amount of information that each single person requires is growing by development of electron information communication technology. So in this paper we analysis the phase noise characteristics to obtain a most suitable of SNR performance request characteristic by BER on CATV transmission system that satisfy performance request DOCSIS 2.0 standard. Especially we get the parameter value of PLL that satisfy phase noise characteristic request standard using developed simulator. Presented method can be used to obtain a performance request standard connection performance request standard of high speed CATV transmission system in the future.

A Study on the Determination of Water Storage-Supply Capacity of Agricultural Reservoir (소규모 농업용 저수지의 저류량-용수공급능력 결정에 관한 연구)

  • 안승섭;정순돌;이증석;윤경덕;장인수
    • Journal of Environmental Science International
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    • v.11 no.12
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    • pp.1217-1226
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    • 2002
  • This study aims at the effective estimation of water supply capacity of small scale reservoir and the proposal of the data which is necessary to establish the water resources management plan of down stream area of the reservoir in the future by comparison and examination about reservoir operation technique for the security of agricultural water in small scale reservoir. The result of flow calculation by Tank model is used for the input data as the inflow data which is needed for the analysis of water supply capacity. Stochastic method, simulation method, and optimization method are used to examine the water supply capacity, and water security amount is compared with each method. From the analyses of water supply capacities by each method, slightly different results are shown in spite of the effort to compare them equally using input data such as inflow data under equal conditions, and the comparison of water supply capacities by each method are as follows; linear planning method, simulation method, and transition probability matrix method in the order of amount from the largest. It is thought that the simulation method in which comparatively reasonable application of the inflow data is possible and is simulated in successive time series dam operation of the three methods used in this study thus, simulation model is proper to estimate the water supply capacity of agricultural small scale reservoir. And it is judged that the heightening of efficiency of water resources utilization according to the development of downstream area of dam may be possible using the upward readjusted water supply amount of $55.18{\tiems}10^6ton$ and $63.7{\times}10^6ton$ at 95% and 90% supply reliability respectively which are above the planning water supply amount of $50.0{\times}10^6$ton when the simulation method is introduced as the standard.

A Study on Improvenment of Livingroom Smoke-control System using the FDS (화재 시뮬레이션(FDS)을 이용한 거실제연설비 개선에 관한 연구)

  • Kim, Mi-Seon;Baek, Eun-Seon
    • Fire Science and Engineering
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    • v.31 no.4
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    • pp.26-34
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    • 2017
  • The purpose of this study is to identify and improve the performance of the adjacent room ventilation system in living room ventilation facilities, and compare and analyze the smoke control regulations of the NFPA code and the national fire safety standard (NFSC). The analysis method was fire dynamics simulation (FDS) and was used to analyze the, variations of the air supply amount, width of the boundary, change in indoor combustion and wind velocity of the incoming air. It was found to be advantageous to secure the clean layer when the amount of air supplied is less than the amount of discharged air in the fire room. However, in the supply room, it is more effective to secure the clean layer when the amount of supplied air is larger than the amount of discharged air, as a longer boundary width gives rise to better performance. In addition, it is necessary to consider the amount of air supplied and discharged as a function of the kind of flammable material. Moreover, decreasing the air inlet wind speed and amount of incoming air is advantageous for securing the clean layer of the fire room.

A Literary Study on Bezoar Bovis (우황에 대한 문헌적 고찰)

  • Park, Seong-Kyu;Park, Jae-Seuk;Baik, Seong-Il;Kwon, Ki-Rok
    • Journal of Pharmacopuncture
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    • v.8 no.3
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    • pp.51-55
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    • 2005
  • Objectives: Literary investigation of existing data was conducted to verify effects of Bezoar Bovis and its herbal acupuncture, and determine quality management through component analysis. Results: Following results were obtained through literary investigation. 1. Bezoar Bovis is dried cystic stone from a cattle. Its characteristics are cool, no toxicity, and bitter taste. Known actions are: quells heat and detoxifies Fire Poison, extinguishes internal movement of Liver Wind and stops convulsion, vaporizes phlegm, and opens orifice. It is mainly used for treating tremor, stroke, delirium, sore throat, oral furuncle, boil, and others. 2. Bezoar Bovis is effective for eliminating liver toxicity, protecting against brain damage, and has anti-microbial activities. 3. Bezoar Bovis is mixed with bear gall bladder and deer musk to be used as herbal acupuncture, and this mixture is effective is invigorating liver functions as well as treating arthritis, headache, and etc. 4. Principal components of Bezoar Bovis are bilirubin-type pigments and cholic acids. The amount of bilirubin can be used as a standard to determine the quality of Bezoar Bovis.

Detection of Aflatoxins in Soybean Food by HPLC (고속액체 크로마토 그라피에 의한 대두식품중 아플라톡신의 검출)

  • Kim, Young-Kook;Roh, Jung-Koo
    • Korean Journal of Food Science and Technology
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    • v.17 no.4
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    • pp.295-303
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    • 1985
  • Aflatoxin $B_1$, $B_2$, $G_1$, and $G_2$were quantitatively detected by the high pressure liquid chromatography on a Micropak-CN column, with Hexane-THF-IPA-water, using a Lichrosorbpacked flowceil in the fluorometric detector. Under those conditions, the minimum detectable amount of aflatoxin $B_1$ was 0.2 ng. HPLC was used in determining amount of aflatoxins in the commercially manufactured soybean food and home-made Meju. Aflatoxin producing abilities of strains used in the industrially fermented soybean food were also studied with the HPLC technique. Although aflatoxin-like substances were detected in a few samples on TLC, they were not identified with the HPLC retention times of standard aflatoxins. The commercial fungal strains used in Korea had no aflatoxin producing abilities.

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