• 제목/요약/키워드: spectral peak

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CHALLENGING APPLICATIONS FOR FT-NIR SPECTROSCOPY

  • Goode, Jon G.;Londhe, Sameer;Dejesus, Steve;Wang, Qian
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.4112-4112
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    • 2001
  • The feasibility of NIR spectroscopy as a quick and nondestructive method for quality control of uniformity of coating thickness of pharmaceutical tablets was investigated. Near infrared spectra of a set of pharmaceutical tablets with varying coating thickness were measured with a diffuse reflectance fiber optic probe connected to a Broker IFS 28/N FT-NIR spectrometer. The challenging issues encountered in this study included: 1. The similarity of the formulation of the core and coating materials, 2. The lack of sufficient calibration samples and 3. The non-linear relationship between the NIR spectral intensity and coating: thickness. A peak at 7184 $cm^{-1}$ was identified that differed for the coating material and the core material when M spectra were collected at 2 $cm^{-1}$ resolution (0.4 nm at 7184 $cm^{-1}$). The study showed that the coating thickness can be analyzed by polynomial fitting of the peak area of the selected peak, while least squares calibration of the same data failed due to the lack of availability of sufficient calibration samples. Samples of coal powder and solid pieces of coal were analyzed by FT-NIR diffuse reflectance spectroscopy with the goal of predicting their ash content, percentage of volatile components, and energy content. The measurements were performed on a Broker Vector 22N spectrometer with a fiber optic probe. A partial least squares model was constructed for each of the parameters of interest for solid and powdered sample forms separately. Calibration models varied in size from 4 to 10 PLS ranks. Correlation coefficients for these models ranged from 86.6 to 95.0%, with root-mean-square errors of cross validation comparable to the corresponding reference measurement methods. The use of FT-NIR diffuse reflectance measurement techniques was found to be a significant improvement over existing measurement methodologies in terms of speed and ease of use, while maintaining the desired accuracy for all parameters and sample forms.(Figure Omitted).

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Earthquake-Induced Wall Pressure Response Analysis of a Square Steel Liquid Storage Tank (지진하중을 받는 정사각형 강재 액체저장탱크의 벽면 압력 응답 해석)

  • Yun, Jang Hyeok;Kang, Tae Won;Yang, Hyunik;Jeon, Jong-Su
    • Journal of the Earthquake Engineering Society of Korea
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    • v.22 no.5
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    • pp.261-269
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    • 2018
  • This study examines earthquake-induced sloshing effects on liquid storage tanks using computation fluid dynamics. To achieve this goal, this study selects an existing square steel tank tested by Seismic Simulation Test Center at Pusan National University as a case study. The model validation was firstly performed through the comparison of shaking table test data and simulated results for the water tank subjected to a harmonic excitation. For a realistic estimation of the wall pressure response of the water tank, three recorded earthquakes with similar peak ground acceleration are applied:1940 El Centro earthquake, 2016 Gyeongju earthquake, and 2017 Pohang earthquake. Wall pressures monitored during the dynamic analyses are examined and compared for different earthquake motions and monitoring points, using power spectrum density. Finally, the maximum dynamic pressure for three earthquakes is compared with the design pressure calculated from a seismic design code. Results indicated that the maximum pressure from the El Centro earthquake exceeds the design pressure although its peak ground acceleration is less than 0.4 g, which is the design acceleration. On the other hand, the maximum pressure due to two Korean earthquakes does not reach the design pressure. Thus, engineers should not consider only the peak ground acceleration when determining the design pressure of water tanks.

A study on the identification of type IIa natural diamonds treated by the HPHT method (HPHT(고온고압)에 의해 처리된 type IIa 천연 다이아몬드의 감별에 관한 연구)

  • 김영출;최현민
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.14 no.1
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    • pp.21-26
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    • 2004
  • Results from PL and Raman spectroscopic analyses of HPHT (high-pressure high-temperature) treated type IIa diamonds are presented, and these spectral characteristics are compared with those of untreated diamonds of similar color and type. We identify a number of significant changes by 325 nm He/Cd laser excitation. Several peaks are removed completely, including H4, H3 system in HPHT treated diamond. The N3 system, however, increased in emission. Also we can find the behaviour of the nitrogen-vacancy related center N-V centers at 575 and 637.1 nm, as observed with 514 nm Ar ion laser excitation. When these centers are present, the FWHM (full width at half maximum) of 637.1 nm luminescence intensities offers a potential means of separating HPHT-treated from untreated type IIa diamonds. The width of 637.1 nm $(N-V)^-$line measured at the position oi half the peak's height are determine to range from 19.8 to $32.1cm^{-1}$ for HPHT treated diamonds.

Effect of Shoe Size on Foot Pressure, Ground Reaction Force, and Fatigue During Walking and Running (보행과 달리기 시 신발의 크기가 족저압과 지면반발력, 하지의 근피로에 미치는 영향)

  • Kim, Tack-Hoon
    • Physical Therapy Korea
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    • v.15 no.1
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    • pp.1-11
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    • 2008
  • The purpose of this study was to assess the influence of two shoe size conditions on foot pressure, ground reaction force (GRF), and lower extremity muscle fatigue. Seven healthy men participated. They randomly performed walking and running in two different conditions: proper shoe size and 10 mm greater than proper shoe size. Peak foot pressure, and vertical, anterior and mediolateral force components were recorded with the Parotec system and Kisler force platform. To assess fatigue, the participants performed treadmill running for twenty-five minutes twice, each time wearing a different shoe size. Surface electromyography was used to confirm localized muscle fatigue using power spectral analysis of four muscles (tibialis anterior, gastrocnemius medialis, rectus femoris, and biceps femoris). The results were as follows: 1) In walking conditions, there was a significantly higher peak pressure in the 10 mm greater than proper shoe size insole sensor 1, 2, 14, and 18 (p<.05). 2) In running conditions, there was a significantly higher peak pressure in the 10 mm greater than proper shoe size insole sensor 5, 14, and 15 (p<.05). 3) In walking conditions, there was a significantly higher first maximal vertical GRF in the 10 mm greater than proper shoe size (p<.05). 4) In running conditions, no GRF components were significantly different between each shoe size condition (p>.05). 5) Muscle fatigue indexes of the tibialis anterior and rectus femoris were significantly increased in the 10 mm greater than proper shoe size condition. These results indicate that wearing shoes that are too large could further exacerbate the problems of increased foot pressure, vertical GRF, and muscle fatigue.

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Design of Wideband Speech Coder Using the MLT Residual Signal (MLT 여기신호를 이용한 광대역 음성 부호화기 설계)

  • Oh Yeon-Seon;Shin Jae-Hyun;Lee In-Sung
    • The Journal of the Acoustical Society of Korea
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    • v.24 no.5
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    • pp.248-254
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    • 2005
  • In this Paper, the structure of a split bandwidth wideband speech coder and its highband coder for tone qualify elevation are Proposed. The lowband and highband by the split bandwidth method are encoded independently applying the G.729E and MLT (Modulated Lapped Transform) residual model. In the highband structure which is encoded by low bit rate of 4kbps, the MLT residual signals are distinguished to voice and unvoice signal . The voice signals are applied to MLT peak picking method by lowband pitch period. Because transformed MLT residual signals are represented by periodic signal that have periodic peak. The unvoice signals are applied to MLT which linear prediction spectral response is added and do vector quantization. Performance for proposed 15.8kbps wideband speech coder was verified through subjective listening test.

A search-based high resolution frequency estimation providing improved convergence characteristics in power system (전력계통에서 수렴성 향상을 위한 탐색기반 고분해능 주파수 추정기법)

  • An, Gi-Sung;Seo, Young-Duk;Chang, Tae-Gyu;Kang, Sang-Hee
    • Journal of IKEEE
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    • v.22 no.4
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    • pp.999-1005
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    • 2018
  • This paper proposed a search-based high resolution frequency estimation method in power systme. The proposed frequency estimation method adopts a slope-based adaptive search as a base of adaptive estimation structure. The architectural and operational parameters in this adaptive algorithm are changed using the information from context layer analysis of the signals including a localized full-search of spectral peak. The convergence rate of the proposed algorithm becomes much faster than those of other conventional slope-based adaptive algorithms by effectively reducing search range with the application of the localized full-search of spectrum peak. The improvements in accuracy and convergence rate of the proposed algorithm are confirmed through the performance comparison with other representative frequency estimation methods, such as, DFT(discrete Fourier transform) method, ECKF(extended complex Kalman filter), and MV(minimum variable) method.

Simulation method of ground motion matching for multiple targets and effects of fitting parameter variation on the distribution of PGD

  • Wang, Shaoqing;Yu, Ruifang;Li, Xiaojun;Lv, Hongshan
    • Earthquakes and Structures
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    • v.16 no.5
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    • pp.563-573
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    • 2019
  • When generating spectrum-compatible artificial ground motion in engineering practices, the effect of the variation in fitting parameters on the distribution of the peak ground displacement (PGD) has not yet drawn enough attention. In this study, a method for simulating ground motion matching for multiple targets is developed. In this method, a frequency-dependent amplitude envelope function with statistical parameters is introduced to simulate the nonstationarity of the frequency in earthquake ground motion. Then, several groups of time-history acceleration with different temporal and spectral nonstationarities were generated to analyze the effect of nonstationary parameter variations on the distribution of PGD. The following conclusions are drawn from the results: (1) In the simulation of spectrum-compatible artificial ground motion, if the acceleration time-history is generated with random initial phases, the corresponding PGD distribution is quite discrete and an uncertain number of PGD values lower than the limit value are observed. Nevertheless, the mean values of PGD always meet the requirement in every group. (2) If the nonstationary frequencies of the ground motion are taken into account when fitting the target spectrum, the corresponding PGD values will increase. A correlation analysis shows that the change in the mean and the dispersion values, from before the frequencies are controlled to after, correlates with the modal parameters of the predominant frequencies. (3) Extending the maximum period of the target spectrum will increase the corresponding PGD value and, simultaneously, decrease the PGD dispersion. Finally, in order to control the PGD effectively, the ground motion simulation method suggested in this study was revised to target a specified PGD. This novel method can generate ground motion that satisfies not only the required precision of the target spectrum, peak ground acceleration (PGA), and nonstationarity characteristics of the ground motion but also meets the required limit of the PGD, improving engineering practices.

Spatial correlation of aerodynamic forces on 5:1 rectangular cylinder in different VIV stages

  • Lei, Yongfu;Sun, Yanguo;Zhang, Tianyi;Yang, Xiongwei;Li, Mingshui
    • Wind and Structures
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    • v.34 no.1
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    • pp.81-90
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    • 2022
  • To better understand the vortex-induced vibration (VIV) characteristics of a 5:1 rectangular cylinder, the distribution of aerodynamic force and the non-dimensional power spectral density (PSD) of fluctuating pressure on the side surface were studied in different VIV development stages, and their differences in the stationary state and vibration stages were analyzed. The spanwise and streamwise correlations of surface pressures were studied, and the flow field structure partitions on the side surface were defined based on the streamwise correlation analysis. The results show that the variation tendencies of mean and root mean square (RMS) pressure coefficients are similar in different VIV development stages. The RMS values during amplitude growth are larger than those at peak amplitude, and the smallest RMS values are observed in the stationary state. The spanwise correlation coefficients of aerodynamic lifts increase with increase of the peak amplitude. However, for the lock-in region, the maximum spanwise correlation coefficient for aerodynamic lifts occurs in the VIV rising stage rather than in the peak amplitude stage, probably due to the interaction of vortex shedding force (VSF) and self-excited force (SEF). The streamwise correlation results show that the demarcation point positions between the recirculation region and the main vortex region remain almost constant in different VIV development stages, and the reattachment points gradually move to the tailing edge with increasing amplitude. This study provides a reference to estimate the demarcation point and reattachment point positions through streamwise correlation and phase angle analysis from wind tunnel tests.

Performance Analysis of PAR Reduction Method using Combined Method in OFDM (OFDM에서 혼합방법을 이용한 PAR 경감법의 성능 해석)

  • 변건식;장은영;김성곤;전제훈
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.7 no.1
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    • pp.42-49
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    • 2003
  • OFDM should be used for the fourth generation communication for high speed communication. Because of high spectral efficiency and high tolerance to fading channel, OFDM is applied to many high speed wire and wireless communication such as DAB (Digital Audio Broadcast), DVB(Digital Video Broadcast), IMT 2000 etc. Inter-modulation, however, is derived from PAR(Peak to Average Power Ratio) of OFDM signals. The paper describes PTS(Partial Transmit Sequence) and SLM(Select Mapping) of an existing methods which can reduce PAR. And then this papers proposed the new method that is called "Combine method". The method proposed in this paper is to combine PTS and SLM. As a result of the simulation, Combine PAR method is better than the existing methods.

Wavelength-Tunable, Passively Mode-Locked Erbium-Doped Fiber Master-Oscillator Incorporating a Semiconductor Saturable Absorber Mirror

  • Vazquez-Zuniga, Luis A.;Jeong, Yoonchan
    • Journal of the Optical Society of Korea
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    • v.17 no.2
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    • pp.117-129
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    • 2013
  • We briefly review the recent progress in passively mode-locked fiber lasers (PMLFLs) based on semiconductor saturable absorber mirrors (SESAMs) and discuss the detailed characterization of a SESAM-based, passively mode-locked erbium-doped fiber (EDF) laser operating in the 1.5-${\mu}m$ spectral range for various configurations. A simple and compact design of the laser cavity enables the PMLFL to generate either femtosecond or wavelength-tunable picosecond pulses with high stability as the intra-cavity filtering method is altered. All the cavities investigated in our experiments present self-starting, continuous-wave mode-locking with no Q-switching instabilities. The excellent stability of the source eventually enables the wavelength-tunable PMLFL to be used as a master oscillator for a power-amplifier source based on a large-core EDF, generating picosecond pulses of >10-kW peak power and >100-nJ pulse energy.