• 제목/요약/키워드: specimens size

검색결과 1,774건 처리시간 0.024초

소결시의 승온속도가 질화규소 요업체의 미세조직과 파괴인성에 미치는 영향 (Effect of the Heating Rate on the Microstructure and Fracture Toughness of Silicon Nitride Ceramics)

  • 이상훈;이재도;김도연
    • 한국세라믹학회지
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    • 제32권11호
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    • pp.1227-1232
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    • 1995
  • Effect of heating rate on the microstructure of the silicon nitride ceramics has been investigated. The specimens with composition of 92Si3N4-6Y2O3-2Al2O3 (in wt%) were sintered at 176$0^{\circ}C$ under 127 kPa for 3h in N2 atmosphere at various heating rates from 1 to 10$0^{\circ}C$/min. The grain size of larger than 2${\mu}{\textrm}{m}$ and less than 1${\mu}{\textrm}{m}$ were measured and compared for the specimens. Regardless of heating rate, grain size of all the specimens showed bimodal distributions and the fracture toughness remained in the range of 5.53~5.72 MPa.m1/2. However, the aspect ratio of the grains of diameter above 2${\mu}{\textrm}{m}$ increased with the heating rate while their grain size and volume fraction decreased.

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합금크롬주철의 탄화물형상 및 열처리가 내마모성에 미치는 영향 (Effects of Carbide Morphology and Heat Treatment on Abrasion Wear Resistance of Chromium White Cast Irons)

  • Yu, Sung-Kon;Matsubara, Yasuhiro
    • 한국재료학회지
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    • 제12권5호
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    • pp.407-413
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    • 2002
  • Eutectic high chromium cast irons containing 17%Cr and 26%Cr were produced for this research by making each of them solidify unidirectionally. Abrasion wear test against SiC or $Al_2$O$_3$bonded paper was carried out using test pieces cut cross-sectionally at several distances from the chill face of castings. The wear resistance was evaluated in connection with the parameters such as eutectic colony size($E_w$), area fraction of boundary region of the colony($S_B$) where comparatively large massive chromium carbides are crystallized and, average diameter of chromium carbides in the boundary region($D_c$). The wear rate($R_w$), which is a gradient of straight line of wear loss versus testing time, was influenced by the type and the particle size of the abrasives. The $R_w$ value against SiC was found to be larger than that against A1$_2$O$_3$under the similar abrasive particle size. In the case of SiC, the $R_w$ value increased with an increase in the particle size. The $R_w$ value also increased as the eutectic colony size decreased, and that of the 17%Cr iron was larger than that of the 26%Cr iron at the same $E_w$ value. Both of the $S_B$ and $D_c$ values were closely related to the $R_w$ value regardless of chromium content of the specimens. The $R_w$ values of the annealed specimens were greater than those of the as-cast specimens because of softened matrix structures. As for the relationship between wear rate and macro-hardness of the specimens, the hardness resulting in the minimum wear rate was found to be at 550 HV30.

SCM415강의 동적 변형거동에 미치는 페라이트 결정립크기 변화에 관한 연구 (A Study of Dynamic Deformation Behaviors of SCM415 steel with the Change of Ferritic Grain Size)

  • 김헌주;박무용
    • 열처리공학회지
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    • 제20권1호
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    • pp.22-30
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    • 2007
  • Effects of ferrite grain size on static and dynamic deformation behaviors of SCM415 stels were investigated in this study. Dynamic torsional test was conducted using torsional Kolsky bar with the strain rate of $1.6{\times}10^3/s$. Specimens with three different grain size of ferrite, $4.6{\mu}m$, $11{\mu}m$, $35.5{\mu}m$ were used. Dimple fracture mode of the dynamic test specimens showed adiabatic shear bands on the beneath of fracture surface. Increased uniform elongation and decreased non-uniform elongation appeared as grain size of ferrite decreased in dynamic torsional test. However, shear strength was independent on grain size of ferrite.

Effects of Crystallization Behavior on Microwave Dielectric Properties of CaMgSi2O6 Glass-Ceramics

  • Choi, Bo Kyeong;Kim, Eung Soo
    • 한국세라믹학회지
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    • 제50권1호
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    • pp.70-74
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    • 2013
  • Dependence of microwave dielectric properties on the crystallization behaviors of $CaMgSi_2O_6$ (diopside) glass-ceramics was investigated with different heat treatment methods (one and/or two-step). The crystallization behaviors of the specimens, crystallite size and degree of crystallization, were evaluated by differential thermal analysis (DTA), scanning electron microscope (SEM) and X-ray diffraction (XRD) analysis by combined Rietveld and reference intensity ratio (RIR) methods. With an increase in heattreatment temperature, the dielectric constant (K) and the quality factor (Qf) increased due to the increase of the crystallite size and degree of crystallization. The specimens heat-treated by the two-step method had a higher degree of crystallization than the specimens heat-treated by the one-step method, which induced improvement in the quality factor (Qf) of the specimens.

철근 콘크리트 구조물의 역학적 거동에 미치는 크기효과에 관한 실험적 연구 (An Experimental Study on the Size Effect influencing to Mechanical Behavior of Reinforced Concrete Structures)

  • 박현수;정란
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1995년도 가을 학술발표회 논문집
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    • pp.366-371
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    • 1995
  • it is extremely difficult to perform the dynamic experiments with full-scale specimens. For this reason, small-scale structural models offer an attractive means to peform dynamic loading experiments. The purpose of this reserch is to estabilish the reliance for modeling techniques of small-scale specimens subjected to dynamic cyclic loading. This research focused on the similitude requirements for reinforced concrete frame structures subjected to dynamic cyclic loading. Length scale ratio of specimens were 1:2:4, and six specimens were tested at the frequencies of 0.0025Hz~2.0Hz. It was confirmed that modeling techniques based on the similitude requirements were useful method to evaluate the behavior of full-size R/C structures subjected to earthquake type loading.

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용융염 합성법에 의한 반도성 $BaTiO_3$의 PTCR 효과 (PTCR Effects in Molten Salt System Synthesized Semiconductive $BaTiO_3$)

  • 윤기현;오기영
    • 한국세라믹학회지
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    • 제22권3호
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    • pp.13-18
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    • 1985
  • Semiconductive $Ba_{0.9}Sr_{0.1}TiO_3$ was prepared by both the Calcining of mixed Oxides (C. M. O) and the Molten Salt Synthesis(M.S.S) methods to investigate the PTCR effects. In the Molten Salt Synthesis method the temperature of calcination for Synthesis of $BaTiO_3$ could be lowered from 110$0^{\circ}C$ to 80$0^{\circ}C$. The M.S.S Specimens had smaller grain size and more homogeneous size distribution at the same sintering temperature as compared with the C. M. O specimens. The M. S. S. specimens showed greater PTCR effects and current variations in the time vs. current charac-teristics than those of C. M. O Specimens.

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중형견 치과보철물 제작을 위한 교합관계 관찰 (Observation of Occlusal Relations for Production to Dental Prosthetics of Dogs)

  • 박유진;최성민
    • 대한치과기공학회지
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    • 제38권3호
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    • pp.203-208
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    • 2016
  • Purpose: This study introduces the production process of dog's dental prosthesis using an automated dental prosthetics technology. The occlusal interaction of dog's dental prosthesis was observed. Methods: This study was proceeded with dog's the mandibular first molar teeth. The 3D CAD designed to 3D model specimens was observed by CAD software. and The specimens designed to 3D model specimens was observed occlusal interaction by using articulator. Results: Occlusal contact point in prosthetic specimens were observed in buccal surface. and 98% of the size of the crown is the best occlusal relationship. Conclusion: Observation of occlusal relations result to 98% of the size of the crown is the best.

Application of RTI to Improve Image Clarity of a Trace Fossil Cochlichnus Found from the Jinju and Haman Formations

  • Sangho Won;Dal-Yong Kong
    • 자원환경지질
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    • 제56권4호
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    • pp.397-408
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    • 2023
  • A total of 64 specimens of trace fossils were collected from the Jinju Formation of the construction site of Jinju Aviation Industrial Complex, and from the Haman Formation of Namhae Gain-ri fossil site. The fossils are continuously and regularly meandering sine-curve in shape. The fossil varies in morphology: width between 0.2 and 5.6 mm, wavelength between 1.5 and 28 mm, and amplitude between 0.9 and 7.9 mm; the Jinju specimens are commonly wider than the Haman ones. The ratio of wavelength to amplitude is more or less regular regardless of width of the specimen, and the linear correlation of the ratios shows that the Jinju specimens fit better than the Haman specimens. Taking all morphometric parameters, specimens in all size ranges are temporarily identified as ichnospecies Cochlichnus anguineus. In order to obtain more distinct and clearer images of Cochlichnus, we selected two specimens and applied a new imaging technology RTI. For photography of the trace fossils, 50 to 80 images were taken per set with photometric lighting close to the surface and horizontally. RTI technology clearly showed that the images of tiny fossils were improved: the surface contrast become sharper and messy and unnecessary information disappeared. Currently, RTI technology is used in many fields including preservation of cultural properties and archaeology. As a consequence, we hope to apply this technique to the field of paleontology, especially to the study of trace fossils of very small size.

Effects of Density, Temperature, Size, Grain Angle of Wood Materials on Nondestructive Moisture Meters

  • Pang, Sung-Jun;Jeong, Gi Young
    • Journal of the Korean Wood Science and Technology
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    • 제47권1호
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    • pp.40-50
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    • 2019
  • The aim of this study was to investigate the effects of density, temperature, size, and grain direction on measurement of moisture contents (MC) of wood materials non-destructively. The MC of different sizes of solid wood, glulam, and CLT from larch (larix kaempferi, $560kg/m^3$) and pine (pinus koraiensis, $430kg/m^3$) were measured using the dielectric type and resistance type meters. The specimens were conditioned in the environmental chamber to be equilibrium moisture content (EMC) of 12 % and 19 %. When density setting in dielectric type meter was increased from $400kg/m^3$ to $600kg/m^3$, the MCs of specimen (S-L-100-E) were decreased from 13.4 % to 11.3 %. However, when wood group (WG) setting in resistance type meter was changed from WG1 to WG4, the measured MCs were increased from 9.2 % to 12.3 %. When temperature setting in resistance type meters was changed from 0 to $35^{\circ}C$, the MC was decreased from 17.0 % to 13.0 %. The MCs measured by dielectric type meter for larger specimens (S-L-100-E_11.3 %, G-L-240-E_11.7 % and C-L-120-E_12.8 %) were higher than those of small size specimens (S-L-30-E_8.7 %, G-L-150-E_10.3 %, and C-L-90-E_9.7 %). The MCs measured by resistance type meter for larger specimens (G-L-240-E_11.6 % and C-L-120-E_13.3 %) were also higher than those of small size specimens (G-L-150-E_10.4 %, and C-L-90-E_11.8 %). The resistance type meter was not affected by the grain direction but the dielectric type meter were affected by the grain direction. The MC measured by resistance type meter for G-L-120-E perpendicular to grain direction was 11.5 % and the measured MC parallel to grain direction was 11.3 %. The MC measured by dielectric type meter parallel to grain direction (12.1 %) was higher than that measured perpendicular to grain direction (10.7 %).

Nb 첨가에 따른 저탄소강의 충격 특성에 미치는 변태 온도의 영향 (Influence Nb Addition and Transformation Temperature on Impact Properties of Low-Carbon Steels)

  • 이상인;강준영;황병철
    • 한국재료학회지
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    • 제26권11호
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    • pp.590-597
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    • 2016
  • In this study, six kinds of low-carbon steel specimens with different ferrite-pearlite microstructures were fabricated by varying the Nb content and the transformation temperature. The microstructural factors of ferrite grain size, pearlite fraction, interlamellar spacing, and cementite thickness were quantitatively measured based on optical and scanning electron micrographs; then, Charpy impact tests were conducted in order to investigate the correlation of the microstructural factors with the impact toughness and the ductile-brittle transition temperature (DBTT). The microstructural analysis results showed that the Nb4 specimens had ferrite grain size smaller than that of the Nb0 specimens due to the pinning effect resulting from the formation of carbonitrides. The pearlite interlamellar spacing and the cementite thickness also decreased as the transformation temperature decreased. The Charpy impact test results indicated that the impact-absorbed energy increased and the ductile-brittle transition temperature decreased with addition of Nb content and decreasing transformation temperature, although all specimens showed ductile-brittle transition behaviour.