• 제목/요약/키워드: specific deposit

검색결과 85건 처리시간 0.019초

Cathodic Stripping Voltammetry법에 의한 식물체 중 극미량 셀렌의 분석 (Determination of Traces of Selenium in Plant Materials by Cathodic Stripping Voltammetry)

  • 문동철;홍성화;박만기;김중기;이광우
    • 약학회지
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    • 제29권3호
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    • pp.144-151
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    • 1985
  • Cathodic stripping voltammetric determination of traces of selenium in plant samples was studied. Stripping peak of selenium (IV) from Cu-Se intermettalic deposit in acidic media containing copper (II) ion is specific, highly sensitive and well defined, is successfully used for the quantitative determination of selenuin down to the level of 1ng/ml. Sample is burnt in a calorimeter bomb under the oxygen pressure of 40atm. and the selenium is absorbed in 0.1M NaOH. After the solution is filtrated, concentrated and acidified with HCl, then passed through a column of cation exchange resin in the $H^{+}$ form(Dowex 50X-8). The column eluate is analyzed for selenium by differential pulse cathodic stripping voltammetric method. Analytical results of selenium for NBS SMR is well agreement with the certified values. Results are given for a series of plant materials.

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잉크젯 프린팅을 이용한 유기태양전지용 기능성 잉크의 적층 (Stacking of functional inks for organic solar cell using inkjet printing)

  • 김명기;황준영;이상호;강희석;강경태;김종석;조영준
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2008년도 춘계학술대회 논문집
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    • pp.398-401
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    • 2008
  • Inkjet printing is commonly used in the controlled deposition of solutions of functional materials in specific locations on a substrate, and it can provide easy and fast deposition of polymer films over a large area. which could become a way to manufacturer low cost solar cells. In the present study, inkjet printing technology is adopted to deposit functional layers of PEDOT/PSS solutions and P3HT/PCBM blends for organic solar cell. The results show that merging of separately deposited ink droplets into a continuous, pinhole-free organic thin film could be achieved by a balance between ink property and substrate treatment. As a result, a power conversion efficiency of 2.0% has been accomplished a solar cells applying inkjet technology.

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소 결핵균의 면역세포화학적 동정 (Immunocytochemical identification of Mycobacterium bovis in tissues)

  • 김순복;서정향;문운경
    • 대한수의학회지
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    • 제33권1호
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    • pp.119-123
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    • 1993
  • The present study was intended to use the avidin-biotin-peroxidase-antiperoxidase complex (ABPAP) method for the identification of Mycobacterium bovis in the tissue sections of infected cattle. Antibodies and linksera for ABPAP procedure used in incubated order were rabbit anti-Mycobacterium polyvalent antibodies, goat anti-rabbit IgG, rabbit peroxidase-antiperoxidase complex, biotinyl-horse anti-rabbit IgG, and avidin-biotin-peroxidase complex. Where the bacterial antigen was localized by ABPAP, a dark brown deposit occurred in the cytoplasms of macrophages and Langerhans' giant cells of the granulomatous lesions. The method approved to be highly specific for the identification of the bacteria and allowed a precise localization of the bacterial antigen in infected cells.

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SURFACE DEGRADATION OF GALLIUM-ALLOYS DURING TOOTH BRUSHING IN VITRO

  • Lee, Seok-Hyung
    • 구강회복응용과학지
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    • 제19권4호
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    • pp.309-315
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    • 2003
  • When the exposure surface of restoration is brushed with various toothpaste in the mouth, wear or undesirable surface deposit of restoration can occur. Surface change of gallium alloys according to brushing and toothpaste may directly affect oral hygiene. The aim of this study was to evaluate the surface alterations of Gallium alloys during tooth brushing with different prophylactic agents. Two gallium-alloys and an amalgam as a control were investigated. Without and with brushing were applied with three kinds of prophylactic agents on the sample for 0, 1, 5, 10, 60 and 360 minutes. At each time interval, surface roughness was recorded by a profilometer and some pictures were taken by a SEM. All results were analyzed by the one-way ANOVA, followed by Tukey multiple comparisons and the simple linear regression analysis. The results indicate that gallium alloys are more susceptible to surface degradation during tooth brushing than amalgam with respect to the specific prophylactic agent used.

Grafting of Casein onto Polyacrylonitrile Fiber for Surface Modification

  • Jia Zhao;Du Shanyi
    • Fibers and Polymers
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    • 제7권3호
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    • pp.235-240
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    • 2006
  • Polyacrylonitrile (PAN) fiber was grafted with casein after alkaline hydrolysis and chlorination reactions of the original fiber. The structures and morphologies of the casein grafted fiber were characterized by Fourier transform infrared spectroscopy (FTIR), X-Ray diffraction (XRD), and scanning electron microscope (SEM). Moisture absorption, specific electric resistance, water retention value, and mechanical properties were also investigated. The results showed that casein was grafted onto the surface of the PAN fiber and the grafted PAN fiber presented better hygroscopicity compared with the untreated fiber. With proper tensile strength, the modified fiber could still meet the requirement for wearing. A mechanism was proposed to explain the deposit of casein on the synthetic acrylic fiber.

용액 교반이 미세 패턴 내 무전해 구리 도금에 미치는 영향 (The Effect of Solution Agitation on the Electroless Cu Deposition Within Nano-patterns)

  • 이주열;김만;김덕진
    • 한국표면공학회지
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    • 제41권1호
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    • pp.23-27
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    • 2008
  • The effect of solution agitation on the copper electroless deposition process of ULSI (ultra large scale integration) interconnections was investigated by using physical, electrochemical and electrical techniques. It was found that proper solution agitation was effective to obtain superconformal copper configuration within the trenches of $130{\sim}80nm$ width. The transition of open potential during electroless deposition process showed that solution agitation induced compact structure of copper deposits by suppressing mass transfer of cuprous ions toward substrate. Also, the specific resistivity of copper layers was lowered by increasing agitation speed, which made the deposited copper particles smaller. Considering both copper deposit configuration and electric property, around 500 rpm of solution agitation was the most suitable for the homogeneous electroless copper filling within the ultra-fine patterns.

모래층 지반 안벽구조물의 탄성침하거동 연구 (A Study on Behavior of Elastic Settlement of Coastal Structure on Sandy Ground)

  • 유남재;전상현;전진용
    • 산업기술연구
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    • 제27권B호
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    • pp.201-208
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    • 2007
  • This paper is research results of investigating the elastic settlement behavior of the coastal caisson structure built on the sandy deposit by comparing results of centrifuge model experiments and those of existing methods of estimating elastic settlement. Basic soil property tests such as specific gravity test, grain size distribution test and organic content test with disturbed soil sampled from the site were carried out. The centrifuge experiment of model satisfying the required design criteria was performed under 50 of artificial accelerated gravitational force condition. The Centrifuge model experimental results were compared and analyzed with the current methods of estimating settlement based on the elastic modulus obtained from the results of odeometer tests and empirical methods from literature reviews.

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해안도달 거리에 따른 서해안 지역 염해 오손물의 분포특성 (The Distribution Characteristics of Salt Contaminants in West Coast Region with the Distance from Sea)

  • 최남호;한상옥
    • 대한전기학회논문지:전기물성ㆍ응용부문C
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    • 제50권6호
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    • pp.276-280
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    • 2001
  • This paper presents the result of a study on the distribution characteristics of salt contaminants in the west coast region, from Inchon to Yearsoo, of South Korea. To evaluate the distribution characteristics of salt contaminants, we had measured the equivalent salt deposit density(ESDD) with brush wiping method for thirteen month(from May 1999 to June 2000). Under the consideration on the measuring interval and method, normalization method was applied for the ESDD data. Besides the measurement, the chemical analysis (chromatography) was carried to investigate the relationship, between the electrical property and the amount of specific ingredient, such as sodium, magnesium and chloride. From the result, we could get the representative value of contamination for each site and distribution characteristics of salt contaminants with the distance from sea in the west coast.

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무전해도금(I) (Review on Electroless Plating(I))

  • 김만;권식철
    • 한국표면공학회지
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    • 제19권3호
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    • pp.121-127
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    • 1986
  • There are many plating methods already commercially employed in te surface technology. One of the plating methods is electroless (chemical) plating, which is deposited by auto-catalytic reduction of metallic ion with the reducing agent in the plating bath. And it has many advantages comparing with electrolytic plating in respect of properties of deposit, such as corrosion resistance, wear resistance, uniformity, hardness, adhesion and so on. So, electroless plating is the fatest growing process in metallization of plastic and electronic industry. The properties and numerous applications of electroless deposits are attracting more and more attention from finish specifies. Many metal finishers are considering set-up of new electroless line in their shops. This review will be beneficial to domestic metal finishers to understand the real status of present electroless plating technology. It will also provide some knowledge on the economic aspect of electroless plating for the commercial application of specific parts.

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잎 표면의 분무입자 부착특성에 따른 제초제 침투성 분석 (The Analysis of Herbicide Penetration with Spray Deposit Characteristics on Plant Leaves)

  • 장영창
    • Journal of Biosystems Engineering
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    • 제25권4호
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    • pp.287-292
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    • 2000
  • The herbicide penetration on weed leaves was spatially analyzed by using chlorophyll fluorescent emission and machine vision technique. Velvetleaf and metribuzin were used as experimental materials in the study. The herbicide spray images were obtained by a combinaton of a fluorescent dye and a UV lighting system. The herbicide penetration was analyzed by means of detecting chlorophyll fluorescent emission under blue-green lighting. According to the experiment results, the number and the size of spray droplets decreased with coverage increasing. The herbicide penetrated mainly along leaf veins and the time for complete penetration over the whole leaf was approximately 100 minutes after herbicide spraying. When the coverage of herbicide droplets on the surface of leaves increased, the speed of herbicide penetration also increased. This study suggested a way of characerizing herbicide spatial penetration and distribution in leaves.

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