• Title/Summary/Keyword: softening temperature

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Effect of Local Softening for Spring-back Reduction of Ultra High Strength Steel on Microstructure and Mechanical Properties (스프링백 저감을 위한 초고강도강의 국부적 연화 열처리에 따른 미세조직과 기계적 특성 변화에 관한 연구)

  • Park, S.E.;Park, B.H.;Oh, M.H.;Kang, B.S.;Ku, T.W.
    • Transactions of Materials Processing
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    • v.30 no.3
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    • pp.134-141
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    • 2021
  • In order to improve excessive spring-back behavior as a result of the roll forming process using ultra high strength steel (UHSS) sheet, local softening in region of a partial area expected to be deformed on an initial blank is considered in this study. With SPFC1470 UHSS sheet with initial blank thickness of 1.20mm, the local softening is performed with the following conditions: temperatures of 500℃, 550℃, 600℃ and 650℃, and holding time of 20s, 40s, 80s and 160s. Mechanical properties, such as yield stress and tensile strength, as well as elongation, are evaluated through uniaxial tensile tests, while the microstructural characteristics as a result of local softening are also investigated using the heat-treated specimens. As a result, it is shown that the spring-back behavior of the roll-formed prototype was reduced about by 78.9%, when the local softening at about 500℃ was performed for 160s considering the practical manufacturing condition.

Optimization to Prepare SIS-SBS Modified Asphalt for Waterproof-sheet (SIS-SBS 개질아스팔트 방수시트재 물성 최적화)

  • Lim, Kwang-Hee
    • Korean Chemical Engineering Research
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    • v.55 no.5
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    • pp.690-697
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    • 2017
  • In this study, styrene-isoprene-styrene (SIS)-styrene-butadiene-styrene (SBS) modified asphalt was prepared for waterproof-sheet to measure its properties including softening point, penetration, low temperature flexibility, viscosity and adhesion. Then the properties of SIS-SBS modified asphalt imparted with self-healing were optimized to seek for optimal compositions of SIS and SBS versus asphalt according to response surface methodology (RSM). As the content of SBS or SIS was increased, both properties of softening point and viscosity, measured at high temperature, were increased with a statistical significance. However, the increments of softening point and viscosity per unit content of SBS added, were observed to be greater than those per unit content of SIS added, respectively. It was due to the difference of thermal properties of SBS and SIS at high temperature that the cross-linking degree of SBS was increased by gelation accompanied with the increase of viscosity, while chain-entanglement of SIS was relatively reduced owing to a chain scission of poly(isoprene) blocks causing the decrease of viscosity. To the contrary, SIS-SBS modified asphalt showed a behavior of the least elasticity resulting in both the maximum of penetration and adhesion, measured at room temperature, as well as the lowest low temperature flexibility at the composition of SIS, 4 g and SBS, 8.5 g based on asphalt, 63 g.

Determination of the Temperature Coefficient of the Constitutive Equation using the Response-Surface Method to Predict the Cutting Force (반응표면법을 이용한 구성방정식의 온도계수 결정과 절삭력 예측)

  • Ku, Byeung-Mun;Kim, Tae-Ho;Park, Jung-Su
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.20 no.10
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    • pp.9-18
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    • 2021
  • The cutting force in a cutting simulation is determined by the cutting conditions, such as cutting speed, feed rate, and depth of cut. The cutting force changes, depending on the material and cutting conditions, and is affected by the heat generated during cutting. The physical properties for predicting the cutting force use constitutive equations as functions of the hardening term, rate-hardening term, and thermal-softening term. To accurately predict the thermal properties, it is necessary to accurately predict the thermal-softening coefficient. In this study, the thermal-softening coefficient was determined, and the cutting force was predicted, using the response-surface method with the cutting conditions and the thermal-softening coefficient as factors.

Prediction on Flow Stress Curves and Microstructure of 304 Stainless Steel (304 스테인리스강이 고온 유동응력곡선과 미세 조직의 예측)

  • 한형기;유연철;김성일
    • Transactions of Materials Processing
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    • v.9 no.1
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    • pp.72-79
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    • 2000
  • Dynamic recrystallization (DRX), which may occur during hot deformation, is important for the microsturctural evolution of 304 stainless steel. Especially, the current interest in modelling hot rolling demands quantitative relationships among the thermomechanical process variables, such as strain, temperature, strain rate, and etc. Thus, this paper individually presents the relationships for flow stress and volume fraction of DRX as a function of processing variables using torsion tests. The hot torsion tests of 304 stainless steel were performed at the temperature range of 900~110$0^{\circ}C$ and the strain rate range of 5x10-2~5s-1 to study the high temperature softening behavior. For the exact prediction of flow stress, the equation was divided into two regions, the work hardening (WH) and dynamic recovery (DRV) region and the DRX region. Especially, The flow stress of DRX region could be expressed by using the volume fraction of DRX (XDRX). Since XDRX was consisted of the critical strain($\varepsilon$c) for initiation of dynamic recrystallization (DRX) and the strain for maximum softening rate ($\varepsilon$*), that were related with the evolution of microstructure. The calculated results predicted the flow stress and the microstructure of the alloy at any deformation conditions well.

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Recrystallization Behavior of 304 Stainless Steel during Hot Multistage Deformation (304 스테인레스강의 고온다단변형시 재결정 거동)

  • 조상현;김성일;유연철;노광섭
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1997.03a
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    • pp.77-80
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    • 1997
  • The torsion tests in the range of 900~110$0^{\circ}C$, 5.0$\times$10-2~5.0$\times$100/sec were performed to study the recry stallization behavior of 304 stainless steel in the high temperature multistage deformation. The no-recrystallization temperature(Tnr) and fractional softening(FS) were determined by the change of flow curves. The inflection points of stress slope were moved to lower temperature area as the strain rate and the interrupt time were increased. From the multipass flow curve, the intersection between pass stress and FS curve was corresponding to the pass which the FS dropped abruptly and it was shown that the recrystallization area could be determined by the FS measurement in multipass deformation.

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Comparison of Temperatures of the Resin Cement in Polycrystalline Ceramic Brackets Irradiated Using a Diode Laser

  • Son, Young-Tak;Son, KeunBaDa;Kim, Kyung-Min;Lee, Jae-Mok;Kim, Jin-Wook;Yu, Wonjae;Lee, Kyu-Bok
    • Journal of Korean Dental Science
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    • v.14 no.2
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    • pp.69-78
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    • 2021
  • Purpose: The primary objective of this study was to evaluate the change in the temperature of the adhesive resin in polycrystalline ceramic brackets irradiated using a diode laser at different irradiation energy levels and times. Materials and Methods: For the measurement of the temperature of the adhesive resin, it was applied at the base of the ceramic bracket, a thermocouple was placed at the center of the base surface, the bracket was placed on prepared resin specimens for light curing, and a laser was irradiated to the center of the bracket slot at 5, 7, and 10 W. For the measurement of the temperatures of the enamel under the bracket and pulp cavity, extracted premolar was fixed to a prepared mold and the ceramic bracket was bonded to the buccal surface of the premolar. The Kruskal-Wallis H test and Friedman test were used for statistical analysis. Result: At 5 W, the temperature of the adhesive resin did not reach the resin softening temperature of 200℃ within 30 seconds. At 7 W, it reached 200℃ when the ceramic bracket was irradiated continuously for 28 seconds. At 10 W, it reached 200℃ when the ceramic bracket was irradiated continuously for 15 seconds. During laser irradiation, the temperature of the enamel under the bracket increased by over 5℃ within 15 seconds. Conclusion: The use of diode laser irradiation for bracket debonding should be carefully considered because the pulp cavity temperature increases by over 5℃ within the irradiation time for resin thermal softening.

The effect of decylcyclopropene derivative on the softening of 'Fuyu' persimmon fruits (Decylcyclopropene 유도체가 부유 단감 과실의 연화에 미치는 영향)

  • Choi, Seong-Jin;Ahn, Gwang-Hwan
    • Food Science and Preservation
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    • v.23 no.1
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    • pp.7-11
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    • 2016
  • In order to develop a sprayable ethylene antagonist, unlike 1-methylcyclopropene (MCP), we synthesized 2-decylcyclopropene-1-carboxylic acid ethyl ester (DCPE) as a derivative of cyclopropene and tested its effect on the flesh softening of 'Fuyu' persimmon fruits. The fruits on trees were sprayed with $4{\cdot}10^{-4}$ M DCPE solution before harvest. After harvest, the persimmon fruits were stored at a low temperature for 1.5 months. The ripening progress of the fruits was then evaluated during storage at ambient temperature ($20^{\circ}C$). Flesh softening, a measure of ethylene response, was considerably delayed up to 7 days after DCPE treatment. However control fruits was rapidly softened after 3-day storage. The treatment effect of DCPE at $4{\cdot}10^{-4}$ M was also compared to that of 1-MCP at 1 ppm. DCPE was storable at refrigerated conditions for at least one month without any loss. The results show that DCPE could be a potential sprayable agent for the prevention of flesh softening of persimmon fruit.

Material model optimization for dynamic recrystallization of Mg alloy under elevated forming temperature (마그네슘 합금의 온간 동적재결정 구성방정식 최적화)

  • Cho, Yooney;Yoon, Jonghun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.6
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    • pp.263-268
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    • 2017
  • A hot forming process is required for Mg alloys to enhance the formability and plastic workability due to the insufficient formability at room temperature. Mg alloy undergoes dynamic recrystallization (DRX) during the hot working process, which is a restoration or softening mechanism that reduces the dislocation density and releases the accumulated energy to facilitate plastic deformation. The flow stress curve shows three stages of complicated strain hardening and softening phenomena. As the strain increases, the stress also increases due to work hardening, and it abruptly decreases work softening by dynamic recrystallization. It then maintains a steady-state region due to the equilibrium between the work hardening and softening. In this paper, an efficient optimization process is proposed for the material model of the dynamic recrystallization to improve the accuracy of the flow curve. A total of 18 variables of the constitutive equation of AZ80 alloy were systematically optimized at an elevated forming temperature($300^{\circ}C$) with various strain rates(0.001, 0.1, 1, 10/sec). The proposed method was validated by applying it to the constitutive equation of AZ61 alloy.

The Association of Post-Storage Physiological Disorder Incidence with Respiration and Ethylene Production in 'Fuyu' Persimmon Fruits ('부유' 단감 과실에서 저장 후 생리적 장해 발생과 호흡 및 에틸렌 생성의 상호 관계)

  • Ahn, Gwang-Hwan;Song, Won-Doo;Choi, Seong-Jin;Lee, Dong-Sun
    • Korean Journal of Food Science and Technology
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    • v.36 no.2
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    • pp.283-287
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    • 2004
  • Persimmons suffer from such physiological disorders as flesh softening, peel blackening, and flesh browning, which occur rapidly particularly when exposed to ambient temperature after storage at low temperature, In this study causes of these disorders were examined in terms of respiration and ethylene production of the fruits. Jelly-like flesh softening, considered as symptom of chilling injury, rapidly developed within 3 days of exposure to ambient temperature without modified atmosphere (MA) packaging after low temperature storage. Disorder development was more suppressed at $30^{\circ}C$ than at $20^{\circ}C$; such temperature dependence is closely connected to ethylene production rate of fruits at both temperatures. Inhibition of ethylene production through MA packaging effectively reduced disorder development, which indicates ethylene production is closely related to jelly-like flesh softening disorder. Development of black-staining on peels occurs in fruits exposed directly to ambient temperature, but not in those packaged with thick PE-film. Flesh browning developed only under anaerobic respiration condition of high temperature and MA packaging with thick PE film, and occurred at quick reduction of available oxygen inside MA package at high temperature.

Effect of Static Softening on Hot Plastic Deformation Behaviour for 304Stainless Steel (304 스테인레스강의 고온소성변형특성에 미치는 정적연화 효과)

  • 조상현;김유승;유연철
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1997.10a
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    • pp.185-188
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    • 1997
  • Static restoration during hot interrupted deformation of 304 stainless steel was studied in the temperature range from 900 to 1100$^{\circ}C$ under various strain rate of 0.05∼ 5/sec and pass strain of 1/4∼3 times peak strain. The static restoration was dependent on the pass strain, deformation temperature and strain rate. Fractional softening(FS) values increased with increasing strain rate, deformation temperature and pass strain. Recystallization kinetics was well explained by the Avrami equation and the time for 50% recrystallization was evaluated using equation of t0.5=2.01${\times}$10-10$\varepsilon$-.156$\varepsilon$ -0.81Dexp(196.66/RT)

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