• Title/Summary/Keyword: soda glass

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Composition Classification of Korea Ancient Glasses by Using Raman Spectroscopy (라만분광분석법을 이용한 한국 고대 유리의 조성 분류)

  • Sim, Woo Seok;Kim, Eun A;Lim, Soo Yeong;Kim, Hyung Min;Kim, Gyu Ho
    • Journal of Conservation Science
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    • v.38 no.2
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    • pp.117-123
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    • 2022
  • In this study, investigated the possibility of quantitatively and qualitatively analyzing Korean ancient glasses via Raman Spectroscopy. We subjected four categories of Korean traditional glasses, namely, lead-BaO, lead, potash, and soda glasses (3, 3, 10, and 10 pieces, respectively), to this analytical technique. The results showed significant differences between the stretching and bending Raman vibration regions corresponding to these different Korean ancient glass types. Specifically, the stretching vibration regions corresponding to lead-BaO and lead glasses showed peaks at 1040 and 1000 cm-1, respectively; the stretching vibration region of normal glass appears at 1100 cm-1. The bending vibration regions corresponding to potash and soda glass showed Raman peaks at 490 and 560 cm-1, respectively. Furthermore, the Raman spectra of the lead and lead-BaO glasses showed red shifts, which depended on the amount of PbO present. Thus, our findings highlighted the possibility of quantitatively determining the amount of PbO, a major component of lead glasses, via Raman Spectroscopy.

The Correlation Properties between Substrate and Molybdenum Back Contacts Fabricated by DC Magnetron Sputtering (DC 반응성 스퍼터링법에 의해 제조된 몰리브덴 후면전극과 기판과의 상관특성분석)

  • Kim, Seok-Gi;Han, Sang-Ok
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.49 no.3
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    • pp.149-154
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    • 2000
  • Bi-layer Mo films were deposited on soda-lime glass substrates using DC magnetron supttering. Increasing gas pressure, the resistivity varied from $1\times10^{-5}\; to\; 8.3\times10^{-3}\; \Omega.cm$. Furthermore, stress direction yielded compressive-to-tensile transition stress curves. The micro-structure of the compressively-stressed film which had poor adhesion consists of tightly packed columns, but of the tensile-stressed films had less dense structure. Under all gas pressure conditions, Mo films exhibited distinctly increasing optical reflection with decreasing gas pressure. The expansion of (110) peak width with the gas pressure meant the worse crystalline growth. The impurity levels in the Mo film exhibited highly concentrated Na, Se and O elements due to less dense micro-structure. The degree of Na diffusion depends on the type of the glass substrate used and the nature of the Mo film.

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Effect of Impact Angle on the Etching of Glass by Powder Blasting (Powder Blasting 을 이용한 유리의 표면부식시 분사각도의 영향)

  • 김광현;박경호;박동삼
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2001.10a
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    • pp.349-354
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    • 2001
  • In this study, we investigated the effect of the impacting ang1e of particles, the scanning times and the stand-off distance on the surface roughness and the weight-loss rate of samples with no mask, and the wall profile and overetching of samples with different mask pattern in powder blasting of soda-lime glass. The varying parameters were the different impact angles between 50$^{\circ}$ and 90$^{\circ}$, scanning times of nozz1e up to 40 and the stand-off distances 70mm and 100mm. The widths of mask pattern were 0.2mm, 0.5mm and 1mm. The powder was alumina sharp particles, WA#600. The mass flow rate of powder during the erosion test was fixed constant at 175g/min and the blasting pressure of powder at 0.2MPa

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Photocatalytic Reactivity of Titanium Dioxide in the Removal of Benzene from Air (공기중의 벤젠제거에 대한 산화티타늄 광촉매 반응특성)

  • 박달근
    • Journal of Korean Society for Atmospheric Environment
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    • v.16 no.4
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    • pp.389-398
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    • 2000
  • Photocatalytic removal of benzene from air was examined using titanium dioxide photocatalyst films prepared on soda lime glass(50$\times$50$\times$2 mm) by spin coating and chemical vapor deposition. For the measurement of photocatalytic reactivity titanium dioxide coated glass was placed into a batch reactor and concentration of benzene in the reactor was set to abuot 100 ppm, and then illuminated with UV. It was found that catalytic reactivity of titanium dioxide films increased with the increase of titanium dioxide film thickness and then level off beyond a certain film thickness. UV absorption by the films showed the similar trend. The formation of stoichiometric amount of carbon dioxide was confirmed by measurement of carbon dioxide concentration in the reactor. In general spin coated films revealed better photocatalytic reactivity than chemically deposited one within the experimental ranges covered in this study. Morphology and crystal structure of prepared films were investigated by XRD and SEM and they showed significant difference between spin coated films and CVD films. Highest quantum efficiency of prepared titanium dioxide photocatalyst was close to 50%.

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Transparent carbon nanotube field emission devices for field emission display and lamp

  • Cho, You-Suk;Lee, Se-Min;Park, Hee-Yong;Lee, Sun-Hee;An, Myung-Chan;Jeong, Se-Young;Kim, Do-Jin
    • 한국정보디스플레이학회:학술대회논문집
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    • 2006.08a
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    • pp.1233-1234
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    • 2006
  • A simple new method to fabricate transparent carbon nanotube field emission devices was developed. The highly graphitized single wall carbon nanotubes were attached on Sn/ITO glass by arc discharge method. Post heat treatments below the deformation temperature of soda-lime glass guaranteed a good mechanical adhesion and electrical contact of the nanotubes. The Sn layer was oxidized below $400^{\circ}C$ and became transparent. As increasing the oxidation temperatures, the emission properties became stable and life time of emitter has been increased.

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Characterization of Glasses by Ion-Exchange(II) : Behavior of Mechanical Properties (이온교환에 따른 비정질 고체재료의 특성화(II) : 기계적 물성 거동)

  • 이동인;이용근;이희수
    • Journal of the Korean Ceramic Society
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    • v.25 no.6
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    • pp.665-670
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    • 1988
  • The behavior of mechanical properties of ion exchanged glasses was investigated in this study. The used glasses were soda-lime-silica glasses that were produced by float process. The maximum values of the bending strength and the curvature depth are 45Kg/$\textrm{mm}^2$ and 8.6mm respectively treated at 45$0^{\circ}C$ for 6h, which are 4.4 times and 3.3 times higher than parent glass. In the case, the thermalshock resistance ΔT is 335$^{\circ}C$ that is 205$^{\circ}C$ higher than parent glass, which is the maximum values in this study. The maximum values of the surface microhardness is 490Kg/$\textrm{mm}^2$ in case of 43$0^{\circ}C$ for 4h. It is also found out that annealing points are increased linearly with increasing the amount of K+ ion exchange independent of treatment temperature. Furthermore, the present work shows that the ion exchange strengthened glasses are more effective than the physical tempering glasses ; the bending strength and the curvature depth are 1.8 times and twice higher respectively.

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Improvement of Mechanical Property by Single Ion Exchange Process in Substrate Glass

  • Lee, Hoi-Kwan;Kang, Won-Ho;Green, David J.
    • Journal of Information Display
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    • v.4 no.3
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    • pp.12-16
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    • 2003
  • In connection with the ion exchange strengthening on soda-lime-silicate, substrate glass for display use was investigated. In the processing, the temperature was varied during the ion exchange in order to make stress profile and to determine optimum condition. In the present work, we found that the maximum value of strength was 617.8 MPa after an ion exchange process at 470 $^{\circ}C$ for 1h, and then, at 450 $^{\circ}C$ for 24h. Also, the effect of residual stress placed on the near surface was measured by analyzing the number of crack branches and brittleness. This approach allowed us the residual stress profile to be engineered to improve mechanical reliability.

Field Emission Properties of Flat Lamp using Carbon Nanotubes Grownon Glass Substrate (유리기판 위에 성장된 탄소나노튜브를 이용한 평판 램프의 전계방출 특성)

  • Lee, Yang-Doo;Moon, Seung-Il;Han, Jong-Hun;Lee, Yun-Hi;Ju, Byeong-Kwon
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.17 no.6
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    • pp.647-651
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    • 2004
  • We fabricated the 1-inch diode type flat lamp using CNTs, which were grown directly on soda-lime glass substrate at 600 ∼ 650 $^{\circ}C$ by thermal chemical vapor deposition(CVD) of acetylene gas. Turn- on field was about 2.8 V/${\mu}{\textrm}{m}$. We observed that uniform and high brightness had been obtained. The brightness of CNT flat lamp was measured up to about 14 kcd/$m^2$ at 2000V in spacing of 500 ${\mu}{\textrm}{m}$. The results showed that the CNTs were very good emission source and suitable for application in the lamp.

Transparent Conductive ITO thin flims for Liquid Crystal Display (액정표시소자용 ITO 투명전극의 특성에 관한 연구)

  • Kim, H.S.;Kim, D.Y.;Choi, B.K.;Koo, K.W.;Han, S.O.
    • Proceedings of the KIEE Conference
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    • 2003.07c
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    • pp.1553-1555
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    • 2003
  • Coatings on glass with highly transparent conducting oxide films(TCOs) are performed mostly by using indium tin oxide(ITO). This Oxide material is very common for applications where both high electrical conductivity. Photovoltaic cells, transparent electrical heater, selective optical filter, and a optical transmittance are essential. In this study, ITO thin films were deposited on $SiO_2$/soda-line glass plates by a dc magnetron sputtering technique. The crystallinity and electrical properties of the films were investigated by X-ray diffraction(XRD), atomic force microscopy(AFM) scanning and 4-point probe. The optical transmittance of ITO films in the range of 300-800nm were measured with a spectrophotometer. As a result, we obtained polycrystalline structured ITO films with (222), (400), and (440) peak. Transmittance of all the films were higher than 90% in the visible range.

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Gas Typed Digital X-ray Image Sensor Using PDP Fabrication Process (PDP공정을 이용한 가스 방식의 디지털 X-ray 영상 센서)

  • Kim, Chang Man;Kim, Si Hyung;Nam, Ki Chang;Kim, Sang Hee;Song, Kwang Soup
    • Journal of the Institute of Electronics and Information Engineers
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    • v.49 no.9
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    • pp.322-327
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    • 2012
  • Parallel-plate-type scanning sensors have been commercially used for X-ray imaging sensors. In this study, we manufactured the scan typed 1D X-ray image sensor that can be used to obtain scanning images, by using the plasma display panel (PDP) fabrication process. We fabricated drift and pixel electrodes in the glass chamber and injected Xe gas at atmospheric pressure. We evaluated the intensity of a pixel signal depending on the bias voltage on the drift electrode and investigated the characteristics of shielding effect on the single pixel using lead (Pb). The adsorption rate of X-ray photon is low (4%) on the soda lime glass (1.1mm) and the electrical signal detected on the X-ray sensor was increased in the high bias voltage. We acquired digital X-ray scanning image with our DAS (data acquisition system) and sensor scanning system.