• Journal of the Korean Ceramic Society
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• v.23 no.6
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• pp.52-58
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• 1986

$Pb(Zr_{0.525} Ti_{0.475})O_3$ piezoelectric ceramics both unmodified and doped with NiO were prepared by the conventional oxide techniques using sintering temperature from 900 to to 125$0^{\circ}C$. The difference in densification process between unmodified and NiO doped PZT ceramics was studied by shrinkage vs. firing temperatures and it was caused by increasing defect concentration in calcining process of NiO doped PZT ceramics. And nickel oxide solubility limit for $Pb(Zr_{0.525} Ti_{0.475})O_3$ ceramics is shown to be at the range from 0.2wt% to 0.5wt% from this defect model micro-structures dielectric and piezolectric properties of Nio doped PZT ceramics.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.3 s.174
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• pp.769-776
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• 2000

RP(Rapid Prototyping) technology is gaining its popularity in building a prototype in all industries. SLS(Slective Laser Sintering) is one of RP technologies, which is focused on tooling processes as well as three dimension solid model. There are several factors, the length and the cross-sectional area of a part, that have an effect on build setup in SLS process. In this paper, the computation on geometrical relationship is used to slice STL file and to estimate these factors. Based on these values, the build setup parameters such as the heating temperature, the laser power, and the powder cartridge feed rate are determined by neural network approaches. The test results show that the computation time is saved and the neural network approach is able to apply to get the optimal parameters of build process within an acceptable error rate.

• Journal of the Speleological Society of Korea
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• no.71
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• pp.13-17
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• 2006

New methods of nano sized material and composite coating preparations have been considered on the base of mathematical model of abrasion reaction interaction of milling and grinding bodies in planetary centrifugal mill. The essence of the method is the abrasive and oxidative wear of the milling bodies and amorphous (better inert) additives. Interactions between them has been supplied the necessary impulse of pressure and temperature on the impact frictional contacts and promoted chemical processes. The offered method can find application for such processing as sintering and geological minerals opening.

• Transactions of the Korean Society of Automotive Engineers
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• v.5 no.3
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• pp.86-94
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• 1997

Quick aging of catalysts has done with IAE(Institute for advanced engineering) AGING MODE suggested by IAE. To estimate the effects of number of aging cycle, temperature and $H_2O$, characteristics of surfaces, mechanical properties and weibull modulus were estimated. Also, the conversion efficiency of aged catalysts was evaluated with model gas bench test. The area of surface and pore volume were decreased according to the number of aging cycle. The precious metal which is well dispersed in fresh state was sintered and agglomerated with aging. The mechanical of deactivation and sintering of catalysts are discussed on the basis of mechanical tests. The conversion efficiency was decreased with the repeats of aging. Especially, the existence of $H_2O$ in supply gas had a main role in catalyst deactivation withy high temperature.

• Journal of the Korean Ceramic Society
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• v.40 no.10
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• pp.931-935
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• 2003

A complex-shaped part was successfully fabricated by Laminate Object Manufacturing (LOM) technique using silicon nitride tape with aligned silicon nitride whisker seeds. The ceramic tape was cut using a commercial cutting plotter according to the cross section drafts generated by slicing a 3-D model, and then the tapes were stacked sequentially. In order to improve adhesion between the tapes, stacking was performed under vacuum. After binder burnout, the part was encapsulated using latex emulsion and was cold isostaically pressed under 250 ㎫. It was sintered to 98.5% TD at 2148 K for 4 h under 2 ㎫ nitrogen pressure.

• Proceedings of the IEEK Conference
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• 2002.07c
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• pp.1740-1743
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• 2002

This paper presents the basic concept of a Solid Freeform Fabrication System using a rapid prototyping procedure. The system can fabricate a ceramic model by laser cutting, accumulating, laminating and sintering of each slice. The system is mainly equipped with a laser apparatus, an x-y table, a material transfer system, and an electric oven. The system could fabricate a small object with smooth surface within comparatively short period of time. The system has also shown its effectiveness in terms of the direct application of the object without the secondary mechanical process. The fabricated sample could directly be applied and used to fairly wide practical areas.

• Proceedings of the KSME Conference
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• 2004.04a
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• pp.1487-1492
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• 2004

For the present study, three heat pipes with different thickness of sintered metal wick were manufactured, and their operational performances, such as capillary limit and thermal resistance were tested and compared with theoretical predictions. Experimental results showed good agreement with those by the theoretical model, and that seemed to present that the sintering process we had developed in the present study was valid.

• Proceedings of the KAIS Fall Conference
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• 2001.05a
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• pp.287-289
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• 2001

The morphology of silica supported MoO$_3$ catalysts, which was prepared by impregnation of ammonium heptamolybdate with various weight loadings up to 35 wt%, was studied using x-ray diffraction. In addition to the orthorhombic phase, the behavior of the rarely studied hexagonal phase was characterized. For high loading catalysts, excess ammonium ions present in the monoclinic and triclinic precursors are capable of occupying interstitial sites of microcrystalline MoO$_3$ during moderate temperature calcinations and in doing so enhance the MoO$_3$-SiO$_2$ interaction. This results in a "well dispersed" morphology at high loadings. Sintering at high temperature is due to loss of ammonium from the oxide framework. Ammonia reimpregnation, which leads back to the well dispersed hexagonal phase, may offer a simple regeneration process for spent Mo containing catalysts.

• Transactions on Electrical and Electronic Materials
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• v.12 no.1
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• pp.1-6
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• 2011

This paper summarized concept, manufacture and results of the micro-tubular solid oxide fuel cells (SOFCs). The cells were fabricated by co-sintering of extruded micro-tubular anode support and electrolyte coating layer, and then additional cathode coating. The cells showed quick voltage rising within 1 minute, and the electrochemical performances were closely related to the balance of fuel utilization and performance loss. And a thermal-fluid simulation model was also reported in combination with the electrochemical evaluation results on the GDC-based micro-tubular SOFCs.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.336-337
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• 2006

During sintering of cemented carbides abnormal grain growth is often observed but cannot be understood from the classical LSW-theory. A model based on 2-D nucleation of new crystalline layers and a grain-size distribution function is formulated and the equations are solved numerically. Experimental studies and computer simulations show that the initial grain size distribution has a strong effect on the grain growth behavior. For example, a fine-grained powder can grow past a coarser powder.