• Journal of the Optical Society of Korea
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• 제15권1호
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• pp.96-102
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• 2011

Simultaneous measurements using a scanning spectrograph system and transmissometer were performed for the first time over an urban site in Gwangju, Korea, to derive the ambient $NO_2$ volume mixing ratio. The differential slant column densities retrieved from the scanning spectrograph system were converted to volume mixing ratios using the light traveling distance along the scanning line of sight derived from the transmissometer light extinction coefficients. To assess the performance of this system, we compared the derived $NO_2$ volume mixing ratios with those measured by an in situ chemiluminescence monitor under various atmospheric conditions. For a cloudless atmosphere, the linear correlation coefficient (R) between the two data sets (i.e., data derived from the scanning spectrograph and from the in situ monitor) was 0.81; the value for a cloudy atmosphere was 0.69. The two sets of $NO_2$ volume mixing ratios were also compared for various wind speeds. We also consider the measurement errors, as estimated from an error propagation analysis.

• Mass Spectrometry Letters
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• 제7권3호
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• pp.64-68
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• 2016

Scanning electron microscopy combined with thermal ionization mass spectrometry (SEM-TIMS) was used to determine the precise isotope ratios of ultra-trace levels of uranium contained in individual microparticles. An advanced multiple ion counter system consisting of three secondary ion multipliers and two compact discrete dynodes was used for complete simultaneous ion detection. For verification purposes, using TIMS with complete simultaneous measurement, isotopes were analyzed in 5 pg of uranium of a certified reference material. A microprobe in the SEM was used to transfer individual particles from a NUSIMEP-7 sample to TIMS filaments, which were then subjected to SEM-TIMS and complete simultaneous measurement. The excellent agreement in the resulting uranium isotope ratios with the certified NUSIMEP-7 values shows the validity of SEM-TIMS with complete simultaneous measurement for the analysis of uranium isotopes in individual particles. Further experimental study required for investigation of simultaneous measurement using the advanced multiple ion counter system is presented.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1998년도 추계학술대회 논문집
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• pp.133-136
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• 1998

The scanning Maxwell-stress microscopy (SMM) is a dynamic noncontact electric force microscopy that allows simultaneous access to the electrical properties of molecular system such as surface potential, surface charge, dielectric constant and conductivity along with the topography. Here we report our recent results of its application to nanoscopic study of domain structures and electrical functionality in organic thin films prepared by the Langmuir-Blodgett technique.

• Journal of Ceramic Processing Research
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• 제13권spc1호
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• pp.154-157
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• 2012

We present the simultaneous growth of single-walled carbon nanotubes and graphene with the optimal conditions of the synthesizing parameters. The dense and vertically aligned SWNTs having the length of over 100 ㎛ was grown by 2 nm-thick Fe catalytic layer. From 650 ℃, the vertically well-grown SWNTs were obtained by increasing the temperature. The severallayered graphene was synthesized with the gas mixing ratio of 15 : 1(H2 : C2H2) at 650 ℃ and higher temperatures. With these optimal conditions, the vertically well-grown SWNTs and the several-layered graphene were synthesized simultaneously. The presence of SWNTs and the layer of graphene were verified by field emission scanning electron microscopy and high resolution transmission electron microscopy. From the result of this simultaneous synthesizing approach, the possibility of one step growth process of CNTs and grapheme could be verified.

• 한국세라믹학회지
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• 제53권2호
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• pp.222-226
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• 2016

The synthesis of pure calcium carbonate nanocrystals was achieved using a simultaneous injection method to produce nano particles of uniform size. These were characterized using scanning electron microscopy and powder X-ray diffraction. The nano particles were needle-shaped aragonite polymorphs, approximately 100-200 nm in length. The aragonite polymorph of calcium carbonate was prepared using aqueous solutions of $CaCl_2$ and $Na_2CO_3$, which were injected simultaneously into double distilled water at $50^{\circ}C$ and then allowed to react for 1.5 h. The resulting whisker-type nano aragonite with high aspect ratio (30) is biocompatible and potentially suitable for applications in light weight plastics, as well as in the medical, pharmaceutical, cosmetic and paint industries.

• E2M - 전기 전자와 첨단 소재
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• 제9권7호
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• pp.702-707
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• 1996

In this paper, in order to improve the withstand voltage properties of epoxy resin, IPN(interpenetrating polymer network) method was introduced and the influence was investigated. The single network structure specimen(E series), simultaneous interpenetrating polymer network specimen(EM series) and pseudo interpenetrating polymer network(EMP series) specimen were manufactured. In order to understand the internal structure properties, scanning electron microscopy method was utilized, and glass transition temperature was measured. Also, AC voltage dielectric breakdown strength, tensile strength and impact strength were measured to investigate the influence upon electrical and mechanical properties. As a result, it was confirmed that simultaneous interpenetrating polymer network specimen was the most execellent.

• 분석과학
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• 제37권5호
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• pp.295-305
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• 2024

5-Hydroxymethyl-2-furaldehyde (5-HMF) is considered one of the main quality indexes of various food products. Its metabolism in humans can potentially lead to carcinogenic compounds. Metallic ions such as Zn, Mg, Mn, and Fe have been reported to enhance 5-HMF formation. Recently, studies on adsorbents that can extract specific organic and inorganic substances with one adsorbent have been conducted. However, simultaneous analysis of organic and inorganic materials typically requires distinct pre-treatment and analytical methods, which increase a lot of labor and cost. In this study, hybrid imprinted polymer (HIP) by mixing 5-HMF imprinted polymer (FIP) and zinc ion imprinted polymer (ZIIP) were generated to extract two analytes, Zn ion and 5-HMF, simultaneously. Physicochemical characterization of HIP was conducted by Fourier-transform infrared spectroscopy, scanning electron microscopy, and sorption tests. Extraction conditions including adsorbent mixing ratio, adsorbate mixing range, and equilibrium time were optimized. Freundlich adsorption model was as the best-fitting isotherm model to elucidate the adsorption mechanism. Affinity of Zn ion and 5-HMF on HIP was superior to non-HIP. In conclusion, HIP showed reasonable feasibility that could be used as an adsorbent to be used for simultaneous extraction of organic and inorganic compounds present in the sample.

• Applied Microscopy
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• 제45권4호
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• pp.214-217
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• 2015

This study introduces metal coating as an effective sample preparation method to remove charge-up caused by the shadow effect during field emission scanning electron microscope (FE-SEM) analysis of dynamic structured samples. During a FE-SEM analysis, charge-up occurs when the primary electrons (input electrons) that scan the specimens are not equal to the output electrons (secondary electrons, backscattered electrons, auger electrons, etc.) generated from the specimens. To remove charge-up, a metal layer of Pt, Au or Pd is applied on the surface of the sample. However, in some cases, charge-up still occurs due to the shadow effect. This study developed a coating method that effectively removes charge-up. By creating a converted sample stage capable of simultaneous tilt and rotation, the shadow effect was successfully removed, and image data without charge-up were obtained.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 2004년도 춘계학술대회 논문집
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• pp.445-448
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• 2004

Linear motor is very rapidly substituted for rotary motor and ball screw for precision positioning applications because of its characteristics such as high speed, no backlash and simplicities. A precision positioning system which is composed of linear motion(LM) guide and linear motor is widely used since it has easy controllable property but this system has low accuracy problem caused by friction of the LM guide. In this study, a scanning type XY stage is manufactured and some experiments is performed to improve the accuracy of the stage.

• 한국산학기술학회논문지
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• 제21권3호
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• pp.312-320
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• 2020

3D 스캐닝과 역설계 기술은 기계/제조 분야에서 먼저 시작하였다. 건설 분야에서는 BIM(Building Information Modeling) 기반 3D 모델링 활용 환경이 조성되어 3D 스캐닝 기술을 이용하여 공장 사전제작, 구조물 시공 검측, 플랜트 시설물, 교량, 터널 구조물 검측 등 건설 전반에 활용하고 있다. 스캔 방식 중 고정식 LiDAR는 이동식 LiDAR에 비해 정확도와 밀도가 높으나 정합 시간과 데이터 처리에 오랜 시간이 걸린다. 하지만, 인테리어, 건축물 관리와 같이 상대적으로 높은 정확도가 필요하지 않은 분야에서 사용자가 편리하게 이동하며 스캔할 수 있는 방법이 생산적이고 효율적이다. 이 연구는 자유롭게 이동하면서 실시간 점군 정합을 지원하는 SLAM(Simultaneous Localization and Mapping)기반 스캔백팩 시스템 개발 시 고려사항을 도출한다. 본 연구를 통해 모바일 스캔 기술을 이용한 스캔 생산성 개선을 위해, SLAM기반 스캔백팩(Scan Backpack) 장치 개발을 위한 프레임웍, 시스템 및 컴포넌트 구조를 제안하고, 프로토타입을 통해 개발 시 고려사항을 도출한다. 프로토타입 개발은 SLAM 및 스캔백팩 2단계로 수행해, 고려사항을 도출하고, 수행 결과를 분석하였다.