• 분석과학
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• 제23권1호
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• pp.54-59
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• 2010

액체크로마토그래피/질량분석법(LC/MS)을 이용하여 화장품에 들어있는 파라벤류등을 동시 분석하였다. 화장품 시료를 메탄올에 직접 용해시키고 $0.45\;{\mu}m$ 필터로 여과하여 메탄올/물을 이동상으로 하여 Extend $C_{18}$의 비극성 컬럼을 사용하여 기울기 용리 조건에서 12분 안에 분리하여 SIM(selected ion monitoring)방법으로 정량하였다. LC/MS 분석결과 검량선은 $0.05-10\;{\mu}g$/mL 농도범위에서 $r^2$=0.9993의 상관계수를 갖는 좋은 직선성을 나타내었으며, 검출한계는 $0.01\;{\mu}g$/mL 이었다.

• 분석과학
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• 제8권3호
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• pp.237-248
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• 1995

미국 환경청이 지정한 129종의 priority pollutants 중 16종의 유기살충제를 포함한 토양시료를 제조하여 표준분석방법인 기체크로마토그래프-전자포획법과 기체크로마토그래프/질량분석기-SIM (selected ion monitoring)법을 이용하여 동시분석의 효율성을 실험하였다. 토양시료의 추출 및 농축방법으로는 EPA의 SW-846 방법을 조금 수정한 초음파추출법(sonication extraction)과 Soxhlet 추출법(Soxhlet extraction)을 비교 연구하였다. 각 화합물의 회수율, 상대표준편차 및 method detection limit를 측정하여 그 결과들을 보고하였다.

• 한국안전학회지
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• 제27권6호
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• pp.48-53
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• 2012

This paper is purposed to develop portable electric instrument to select NI-9223(National instrument comp.) and clamp meter(HIOKI comp.), which can be used in developing electric instrument, to detect leakage current(ZCT) and current(CT) signals. In this paper, The electric instrument that can interface with current and leakage current instrument(HIOKI 9283), is developed by NI-9223 of NI comp.. HIOKI clamp meter can measure current signals certainly by high-sensitivity of 10 ${\mu}A$ resolution(leakage current : at 10 mA range) and current 1~200A range. The NI-9223 use four 16-bit analog-to-digital converters(ADCs) for true simultaneous sampling at up to 1 MS/s per channel. NI-9223 can synchronize all analog input modules installed in the same chassis to share the same start clock and/or sample clocks. The monitoring program is developed by SignalExpress of LabVIEW. The monitoring program are developed to analyze at simultaneous sampling on electrical signals such as leakage current(ZCT) and current(CT). The developed system verification tests were conducted, and portable electric instrument can be used in place which requires analysis of the actual electrical signal.

• 천문학회보
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• 제46권2호
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• pp.49.2-49.2
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• 2021

We present the results of long-term simultaneous monitoring observations (~ 12 years) of H²O (22 GHz) maser and several vibrationally excited lines of SiO J = 1-0, 2-1, 3-2 masers (43, 86, 129 GHz) carried out with the 21-m antennas of the Korean VLBI Network (KVN) toward a sample of three AGB stars (RT Vir, RR Aql, IRC-10151) that are believed to be semiregular variable star, Mira variable star, and OH/IR star, respectively, according to a sequential evolutionary phase of AGB star. A total 10 transitions were observed, of which we detected H²O, SiO 𝝊 = 1 and 2, J = 1-0, SiO 𝝊 = 1, J = 2-1 and J = 3-2 maser lines in all three target objects, depending on the observational epochs. In this study, we scrutinize the evolutionary traits of each target object based on the maser line profiles, flux/velocity variations, and phase lags with the optical light curves. The IRAS two color diagram and the infrared spectral energy distributions (SEDs) in the wavelength range from 1.2 to 240 ㎛ of three observed sources were also analyzed.

• 생약학회지
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• 제43권2호
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• pp.137-146
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• 2012

Dipsaci Radix (Dipsacaceae) has been used as a tonic, an analgesic, anti-inflammatory and anti-complement agents in traditional herbal medicine for the therapy of low back pain, knee pain, rheumatic arthritis, traumatic hematoma, and bone fractures. A high-performance liquid chromatography-electrospray ionization-mass spectrometric method (HPLC-ESI-MS) was developed for the simultaneous quantitation method of the five compounds from the herbal drug: asperosaponin VI and asperosaponin XII (terpene glycosides), sweroside, loganin and dipsacus A(iridoid glycosides). HPLC separation of the analytes was achieved on a C18 column ($150{\times}2.0$ mm i.d., 5 ${\mu}m$) using the aqueous methanol containing 5 mM ammonium acetate with gradient flow of the mobile phase. Detection of the analytes was performed by positive ion electrospray ionization, and selected ion monitoring was used for data acquisition using m/z corresponding molecular adduct ion, $[M+NH_4]^+$ and $[M+H]^+$. Calibration graphs showed good linearity ($r^2$=0.9997) over the wide range of the analytes; intra- and inter-day precisions (RSD, %) were within 9.1% and the accuracy between 94.0-111.0%. Recoveries of the analytes through the assay procedure were in the range of 93.7-110.8%. Analytical results of the herbal drugs of Dipsaci Radix (17 samples) show wide distribution of the five marker compounds and clear difference of the species from Phlomidis Radix (4 samples). The developed method would provide a practical guide for the quality control of the herbal drug.

• KSBB Journal
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• 제24권1호
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• pp.106-112
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• 2009

An optical sensing membrane has been fabricated to measure the concentration of dissolved oxygen(DO) and pH value simultaneously. It has employed HPTS as a pH sensitive dye and a ruthenium(II) complex as a DO sensitive dye. The sensing membrane has been applied to wells in a 24-well microtiter plate. Using the 24-well microtiter plate the concentrations of dissolved oxygen and pH values have been on-line monitored during the cultivations of E.coli DH5${\alpha}$, B.cereus 318 and P.pastoris X-33. On-line monitoring of DO and pH in microorganism cultivation processes showed good performance of the sensing membrane containing 5 mM HPTS and 2 or 5 mg/mL Rudpp.

• Journal of the Korean Data and Information Science Society
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• 제26권6호
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• pp.1593-1600
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• 2015

A control chart is very useful in monitoring various production process. There are many situations in which the simultaneous control of two or more related quality variables is necessary. We construct bivariate Shewhart control charts based on the trace of the product of the estimated variance-covariance matrix and the inverse of the in-control matrix and investigate the properties of bivariate Shewart control charts with VSI procedure for monitoring covariance matrix in term of ATS (Average time to signal) and ANSW (Average number of switch) and probability of switch, ASI (Average sampling interval). Numerical results show that ATS is smaller than ARL. From examining the properties of switching in changing covariances and variances in ${\Sigma}$, ANSW values show that it does not switch frequently and does not matter to use VSI procedure.

• Structural Monitoring and Maintenance
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• 제6권3호
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• pp.237-254
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• 2019

This paper presents an improved time series based damage detection approach with experimental verifications for detection, localization, and quantification of damage in shear-type structures under varying mass effects using output-only vibration data. The proposed method can be very effective for automated monitoring of buildings to develop proactive maintenance strategies. In this method, Auto-Regressive Moving Average models with eXogenous inputs (ARMAX) are built to represent the dynamic relationship of different sensor clusters. The damage features are extracted based on the relative difference of the ARMAX model coefficients to identify the existence, location and severity of damage of stiffness and mass separately. The results from a laboratory-scale shear type structure show that different damage scenarios are revealed successfully using the approach. At the end of this paper, the methodology limitations are also discussed, especially when simultaneous occurrence of mass and stiffness damage at multiple locations.

• 한국대기환경학회:학술대회논문집
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• 한국대기환경학회 2003년도 추계학술대회 논문집
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• pp.400-401
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• 2003

Atmospheric fine aerosol particles play an important role in controlling a number of atmospheric processes, such as the deposition of different compounds, the optical properties etc. (Molnar et al., 1999). In this report, water-soluble species of PM$_{2.5}$ obtained from simultaneous measurements at four Asia sites (Beijng (39.56$^{\circ}$N, 116.17$^{\circ}$E), China; Gwangju (35.10$^{\circ}$N, 126.53$^{\circ}$E), South Korea; Kyoto (35.01$^{\circ}$N, 135.44$^{\circ}$E), Japan; and Ulan-Bator (47.55$^{\circ}$N, 106.52$^{\circ}$E), Mongolia) during the periods of 14-22 August, 30 October-06 November 2000, 14-21 January 2001, 23 July-02 August and 05-16 November 2002, within the framework of an APN (The Asia-Pacific Network for Global Change Research) project are reported. Ion components in 23 July-02 August 2002 were not obtained because of the technical problem of equipments.s.

• Journal of Chest Surgery
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• 제57권2호
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• pp.205-212
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• 2024

Background: Postoperative atrial fibrillation (A-fib) is a serious complication of cardiac surgery that is associated with increased mortality and morbidity. Traditional 24-hour Holter monitors have limitations, which have prompted the development of innovative wearable electrocardiogram (ECG) monitoring devices. This study assessed a patch-type wearable ECG device (MobiCARE-MC100) for monitoring A-fib in patients undergoing cardiac surgery and compared it with 24-hour Holter ECG monitoring. Methods: This was a single-center, prospective, investigator-initiated cohort study that included 39 patients who underwent cardiac surgery between July 2021 and June 2022. Patients underwent simultaneous monitoring with both conventional Holter and patchtype ECG devices for 24 hours. The Holter device was then removed, and patch-type monitoring continued for an additional 48 hours, to determine whether extended monitoring provided benefits in the detection of A-fib. Results: This 72-hour ECG monitoring study included 39 patients, with an average age of 62.2 years, comprising 29 men (74.4%) and 10 women (25.6%). In the initial 24 hours, both monitoring techniques identified the same number of paroxysmal A-fib in 7 out of 39 patients. After 24 hours of monitoring, during the additional 48-hour assessment using the patch-type ECG device, an increase in A-fib burden (9%→38%) was observed in 1 patient. Most patients reported no significant discomfort while using the MobiCARE device. Conclusion: In patients who underwent cardiac surgery, the mobiCARE device demonstrated diagnostic accuracy comparable to that of the conventional Holter monitoring system.