• 제목/요약/키워드: simple procedure

검색결과 1,836건 처리시간 0.031초

Gas Liquid Chromatography에 의한 Dienestrol Cream 중의 Dienestrol 정량 (Determination of Dienestrol in Dienestrol Cream by Gas Liquid Chromatography)

  • 백남호;박만기;염정록
    • 약학회지
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    • 제23권1호
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    • pp.7-10
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    • 1979
  • A gas chromatographic determination of dienestrol in dienestrol cream has been studied. Dienestrol cream was dissolved in pyridine and silylation was done by using N, O-bis (trimethylsilyl) trifluoroacetamide. The derivative was injected into 3% silicone OV-17 column for chromatographic estimation. The dienestrol peak was found to be well separated from the other components of the cream. The detection limit was obtained to be $5.6{\times}10^{11}$ mol of dienestrol for this method. As there is no need for prior separation procedure, this experiment is extremely simple and less time consuming as compared to the conventional methods for estimation of dienestrol in cream.

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Application of Preconditioning Method to Cavitating Flow Computation

  • Shin, Byeong-Rog
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2004년도 춘계학술대회
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    • pp.1903-1908
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    • 2004
  • A preconditioned numerical method for gas-liquid two-phase flows is applied to solve cavitating flow. The present method employs a finite-difference dual time-stepping integration procedure and the MUSCLTVD scheme. A homogeneous equilibrium cavitation model is used. The present density-based numerical method permits simple treatment of the whole gas-liquid two-phase flow field, including wave propagation, large density changes and incompressible flow characteristics at low Mach number. Some internal flows such as convergent-divergent nozzles are computed using this method. Comparisons of predicted and experimental results are provided and discussed.

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비선형 구조해석에서 부분구조를 이용한 수정 BFGS법 (A Modified BFGS Method with Substructuring for the Nonlinear Structural Analysis)

  • 류연선;윤길수
    • 대한조선학회지
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    • 제23권3호
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    • pp.39-44
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    • 1986
  • The basic BFGS procedure for the nonlinear finite element analysis is reviewed. Through a simple numerical example, promising characteristics of the method evaluated discussed. Based on the discussion of computational performance, a modified BFGS algorithm with substructuring is derived and proposed for the quasi-static analysis of large-scale nonlinear structures.

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Metal-Free Oxidation of Alcohols to Their Corresponding Carbonyl Compounds Using NH4NO3/Silica Sulfuric Acid

  • Zarei, Amin
    • Bulletin of the Korean Chemical Society
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    • 제33권7호
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    • pp.2149-2155
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    • 2012
  • A metal-free and efficient procedure for the oxidation of alcohols into the corresponding carbonyl compounds has been described using ammonium nitrate in the presence of silica sulfuric acid under mild and heterogeneous conditions. The use of non-toxic and inexpensive materials, simple and clean work-up, short reaction times and good yields of the products are among the advantages of this method.

Mutual Inductance of the Non-Coaxial Coils in Coil Gun

  • 김기봉
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1994년도 추계학술대회 논문집 학회본부
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    • pp.120-123
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    • 1994
  • The purpose of this paper is to describe the mutual inductance between two non-coaxial circular coils in coil gun. As being in many electromagnetic applications, one of them is fixed and the other one is moving and, being not supported, its axis may not coincide with the axis of the fixed coil. This paper presents a method for the calculation of the mutual inductance in case of non-coaxial coupled coils, the characteristics of this inductance and experimental results. For the computation, the complete elliptic integrals formula and mesh matrix technique were introduced. This method enables accurate results from relatively simple procedure and calculation program.

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검상돌기하절개에 의한 심방중격결손증의 교정 -2례보고- (Subxiphois Approach for The Repair of Atrial Septal Defects -A cases report-)

  • 오상기
    • Journal of Chest Surgery
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    • 제33권2호
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    • pp.183-185
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    • 2000
  • With the marked decrease in operative mortality in simple heart diseases there have been several reports on the minimally invasive and cosmetic techniques including submammary incision right parasternal approach right anterolateral thoracotomy partial sternotomy and subxiphoid approach. We report here subxiphoid approach without sternotomy for the repair of atrial septal defect as the procedure that has less invasive technique and more cosmetic effect.

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선천성 관동정맥루 -수술치험 3례- (Surgical Treatment of Congenital Coronary Arteriovenous Fistula -A report of three cases-)

  • 하현철
    • Journal of Chest Surgery
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    • 제27권8호
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    • pp.700-704
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    • 1994
  • Congenital coronary arteriovenous fistula is relatively rare congenital heart disease which has formation of fistula between coronary artery and cardiac ventricle, atrium, or pulmonary artery, but that can be repaired with simple surgical procedure. We experienced three cases of congenital coronary arteriovenous fistula, which were repaired surgically under cardiopulmonary bypass, so we report these cases with review of the literatures.

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Experimental technique for efficiency transfer along different geometries and volumes

  • Haddad, Kh;AL-Homyed, A.
    • Nuclear Engineering and Technology
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    • 제53권2호
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    • pp.695-698
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    • 2021
  • Efficiency calibration is a fundamental procedure in gamma spectrometric measurement. Experimental technique for efficiency calibration transfer in gamma spectrometer along different geometries and volumes has been developed and validated in this work. The developed technique offers simple and easy procedures to overcome several problems encountered in efficiency calibration of gamma spectrometer such as rate-related correction and different sample volumes. The validation shows that application of the developed technique has a precision of 95%.

New Analytical Method of Cyclosporine A in Human Serum by High -performance Liquid Chromatography/Diode Array Detector and Its Application to Pharmacokinetics of Cyclosporine A in Human Volunteers

  • Kim, Eun-Young;Chung, Yeon-Bok;Kwon, Oh-Seung
    • 대한약학회:학술대회논문집
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    • 대한약학회 2002년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.2
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    • pp.423.1-423.1
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    • 2002
  • A simple. specific and sensitive method for the determination of cyclosporine A (CsA) in human serum has been developed by a high performance liquid chromatography/diode array detector (DAD) and applied to pharmacokinetic study of CsA. This method involves the use of solid phase extraction procedure following rapid protein precipitation with zinc sulphate from 1 $m\ell$ of human serum, using a disposable $C_{18}$ extraction cartridge. (omitted)

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