• Title/Summary/Keyword: silver techniques

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THE EFFECT OF PROCESS CONDITIONS ON THE PHYSICAL PROPERTIES OF SILVER FILMS PREPARED BY USING SPUTTERING ON POLYESTER SUBSTRATE

  • Hoang, Tae-Su;Ri, Eui-Jae
    • Journal of the Korean institute of surface engineering
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    • v.32 no.3
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    • pp.401-405
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    • 1999
  • Reflective silver films with high quality were prepared on polyester substrate by using sputter deposit on techniques. Best reflectivity thin films of silver were produced with process parameters of $10^{-6}$ Torr as base pressure, 50 W as R.F. power, 5 mTorr as working pressure, and 10 sccm as Ar flow rate. Being deposited with an R.F. power of 50 W, Ag films revealed the highest 96.3 % reflectance as illuminated with a light of 700 nm wavelength. The adhesion of sample films showed as high as 14 to $20{\;}kg/\textrm{cm}^2$, which is suitable for industrial purposes. Their film crystallinity and orientation resulted in the planes of (111) and (200) for the growth with a preferred orientation of <111>, in general. The cross-sections of thin film specimens showed columnar structures. It is noted that columns became coarsened and less dense as R.F. power increased, resulting in a low reflectivity for the product film.

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Effects on the tissue reaction using compomer & Ketac Silver in the maxillary furcation in the beagle dogs (Compomer와 Ketac Silver로 성견 상악 이개부 병소 충전시 조직반응에 미치는 영향)

  • Ryu, Jea-Youn;Lim, Sung-Bin;Chung, Chin-Hyung;Lee, Chong-Heon
    • Journal of Periodontal and Implant Science
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    • v.33 no.4
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    • pp.705-715
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    • 2003
  • Procedures for treatment of molar furcation invasion defects range from open flap debridement, apically repositioned flap surgery, hemisection, tunneling or extraction, to regenerative therapies using bone grafting or guided tissue regenerative therapy, or a combination of both. Several clinical evaluations using regenerative techniques have reported the potential for osseous repair of treated furcation invasions. Regenerative treatment of maxillary molars are more difficult due to the multiple root anatomy and multiple furcation entrances therefore, purpose of this study was to evaluated histologically compomer and Ketac Silver as a barrier in the treatment of a bi-furcated maxillary premolar. Five adult beagle dogs were used in this experiment. With intrasulcular and crestal incision, mucoperiostcal flap was elevated. Following decortication with 1/2 high speed round bur, furcation defect was made on maxillary premolar. 2 month later one premolar was filled with compomer and the other premolar was filled with Ketac Silver. After 4, 8 weeks, the animals were sacrificed by vascular perfusion. Tissue block was excised including the tooth and prepared for light microscope with H-E staining. Results were as follows. 1. Compomer & Ketac Silver restoration were encapsulated fine connective tissue. 2. In 4 weeks, compomer & Ketac Silver restoration slightly infiltrated inflammatory cells but not disturb the new bone or new cementum formation. 3. In 8 weeks, compomer & Ketac Silver restoration were less infiltrated iflammatory cell and encapsulated fine connective tissue. 4. Therefore, compomer & Ketac Silver filling to the grade III maxillary furcations with multiple root anatomy and multiple furcation entrances is possible clinical method and this technique is useful method for maxillary furcation involvement but it is thought that periodic maintenance should be needed

Electrochemical Behaviors of Polycrystalline Silver Electrodes in 8M KOH Solutions Containing Bi2O3 (Bi2O3를 첨가한 8M KOH용액에서 다결정 Ag전극의 전기화학적 거동)

  • Hur, Tae-Uk;Kong, Yeong-Kyung;Chung, Won-Sub
    • Journal of the Korean Electrochemical Society
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    • v.8 no.1
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    • pp.17-23
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    • 2005
  • The electrochemical behaviors of polycrystalline silver electrodes in 8M KOH solutions containing $Bi_2O_3$ were studied under various conditions by cyclic voltammetry, potentiostatic and galvanostatic techniques as well as the morphology of the silver oxide structures by SEM. It was found that three new compounds comprising silver, bismuth, and oxygen as well as $Bi_2O_3$, $Ag_2O$ and AgO were formed during the electrochemical oxidation of silver. In addition, the potentiostatic current transients were characterized by the appearances of the first current peaks corresponding to the formation of silver oxides, and the second current peaks corresponding to the Ag-Bi-O compounds, indicating the presence of the nucleation and 3D growth mechanism, in the potential regions of $Ag_2O$ and AgO, respectively. Microscopic examinations showed that two types of silver (I) oxide morphologies are formed in the potential region of $Ag_2O$.

ELECTROLYTIC RECOVERY OF PRECIOUS METALS FROM DILUTED SOLUTIONS

  • Roland Kammel;Lieber, Hans-Wilhelm
    • Journal of the Korean institute of surface engineering
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    • v.14 no.4
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    • pp.209-214
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    • 1981
  • Electrolytic recovery of gold and silver from diluted solutions has at first been applied nearly 100 years ago. Compared with other recovery techniques electrolytic treatment offers several advantages. But to achieve high space-time yields special constructions of electrolytic cells for improved mass transfer are necessary. Ex-tended cathode surface areas and vigorous agitation are important features. Gold and silver recovery by use of newly developed electrolytic cell constructions - rotating tubular bed reactor and impact rod reactor - has been described. Calculations based on industrial application during several years are confirming that electrolytic recovery of precious metalss from diluted solutions has been operated in a very economic way.

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Effect of annealing atmosphere on the properties of chemically deposited Ag2S thin films

  • Pawar, S.M.;Shin, S.W.;Lokhande, C.D.;Kim, J.H.
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.34.2-34.2
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    • 2009
  • The silver sulphide (Ag2S) thin films have been chemically deposited from an alkaline medium (pH 8 to 10) by using a silver nitrate and thiourea as a Ag and S ion precursor sources. Ethylene Damine tetraacetic acid (EDTA) was used as a complexing agent. The effect of annealing atmosphere such as Ar, N2+H2S and O2 on the structural, morphological and optical properties of Ag2S thin films has been studied. The annealed films were characterized by using X-ray diffraction (XRD), scanning electron microscopy (SEM) and optical absorption techniques for the structural, morphological, and optical properties, respectively. XRD studies reveal that the as-deposited thin films are polycrystalline with monoclinic crystal structure, is converted in to silver oxide after air annealing. The surface morphology study shows that grains are uniformly distributed over the entire surface of the substrate. Optical absorption study shows the as-deposited Ag2S thin films with band gap energy of 0.92eV and after air annealing it is found to be 2.25 eV corresponding to silver oxide thin films.

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Antifungal Effects of Silver Phytonanoparticles from Yucca shilerifera Against Strawberry Soil-Borne Pathogens: Fusarium solani and Macrophomina phaseolina

  • Ruiz-Romero, Paola;Valdez-Salas, Benjamin;Gonzalez-Mendoza, Daniel;Mendez-Trujillo, Vianey
    • Mycobiology
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    • v.46 no.1
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    • pp.47-51
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    • 2018
  • In the present study, the characterization and properties of silver nanoparticles from Yucca shilerifera leaf extract (AgNPs) were investigated using UV-visible spectroscopic techniques, zeta potential, and dynamic light scattering. The UV-visible spectroscopic analysis showed the absorbance peaked at 460 nm, which indicated the synthesis of silver nanoparticles. The experimental results showed silver nanoparticles had Z-average diameter of 729 nm with lower stability (195.1 mV). Additionally, our dates revealed that AgNPs showed broad spectrum antagonism ($p{\leq}.05$) against Fusarium solani (83.05%) and Macrophomina phaseolina (67.05%) when compared to the control after nine days of incubation. Finally, AgNPs from leaf extracts of Y. shilerifera may be used as an agent of biocontrol of microorganism of importance. However, further studies will be needed to fully understand the agronanotechnological potentialities of AgNPs from Yucca schidigera.

The Types and Characteristics of Decorative Techniques Applied to the Korean Traditional Skirt of Contemporary Style - Focusing on 2001 to 2010 - (현대 한복치마에 사용된 장식기법의 유형과 특성 - 2001~2010년도를 중심으로 -)

  • Ok, Myung-Sun;Park, Ok-Lyun
    • The Research Journal of the Costume Culture
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    • v.19 no.4
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    • pp.712-722
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    • 2011
  • The purpose of this study is to examine the types and characteristics of decorative techniques applied to the Korean traditional skirt of contemporary style. For the purpose, this researcher selected 167 pieces of Korean traditional skirts which were shown in relevant monthly magazines published between 2001 and 2010. Then, the researcher classified the types of decorative techniques found in those selected pieces and analyzed the characteristics of decoration technique for each area of the pieces and the characteristics of patterns used in relation to those techniques. The Korean traditional skirt, otherwise called 'Hanbok chima', was classified into two types, single and composite, in accordance with which technique of decoration was used to it. The single type was characterized by so many embroideries, while the composite type, a combination of two decorative techniques, seonchigi and jatmulim. In the Korean traditional skirt, decorative techniques were applied to the knotting and entire of the skirt. Patterns used to decorate the Korean traditional skirt were usually in form of embroidery, gold or silver foil or painting. Out of the patterns, those which were embroidered or painted were shaped flowers, while those which were plated with gold or silver are shaped bosangdangchomun and flowers. There were other decorative techniques than mentioned above, for example, applying two or more different colors to the hem of the skirt, attaching pads to the knotting of the skirt and padding a decorative cloth on the front center of the skirt.

Preparation of Silver/Polystyrene Nanocomposites by Radical Polymerization Using Silver Carbamate Complex (은 카바메이트 복합체를 이용한 라디칼 중합에 의한 은/폴리스티렌 나노복합체의 제조)

  • Park, Heon-Su;Park, Hyung-Seok;Gong, Myoung-Seon
    • Polymer(Korea)
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    • v.34 no.2
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    • pp.144-149
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    • 2010
  • Ag/polystyrene(PS) nanocomposites were prepared by in situ reduction of silver 2-ethylhexylcarbamate (Ag-CB) complex and follwing radical polymerization only by heating at 110 $^{\circ}C$. In contrast to this conventional heating method, the microwave irradiation afforded well-dispersed silver nanoparticles(NPs) in styrene monomer without polymerization. The synthesis of Ag NPs proceeded uniformly throughout the reaction vessel only under microwave irradiation, completing the reaction simultaneously in the whole reaction solution. Successive polymerization of the monomer containing the resultant NPs has successfully produced a hybrid of the silver NPs dispersed in PS matrix. Ag/PS (0.1/100) nanocomposites were prepared successfully by melt-mixing process using Ag/PS(4.0/100) as a master-batch. UV-VIS spectroscopy, TEM, and X-ray diffraction techniques were used to investigate the process of formation of Ag/PS nanocomposites.

Evaluation of Contact Resistance between Carbon Fiber/Epoxy Composite Laminate and Printed Silver Electrode for Damage Monitoring (손상 감지 모니터링을 위한 탄소섬유 복합재료와 인쇄된 은 전극 사이의 접촉저항 평가)

  • Jeon, Eun-Beom;Takahashi, Kosuke;Kim, Hak-Sung
    • Journal of the Korean Society for Nondestructive Testing
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    • v.34 no.5
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    • pp.377-383
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    • 2014
  • An addressable conducting network (ACN) makes it possible to monitor the condition of a structure using the electrical resistance between electrodes on the surface of a carbon fiber reinforced plastics (CFRP) structure. To improve the damage detection reliability of the ACN, the contact resistances between the electrodes and CFRP laminates needs to be minimized. In this study, silver nanoparticle electrodes were fabricated via printed electronics techniques on a CFRP composite. The contact resistance between the silver electrodes and CFRP were measured with respect to various fabrication conditions such as the sintering temperature of the silver nano-ink and the surface roughness of the CFRP laminates. The interfaces between the silver electrode and carbon fibers were observed using a scanning electron microscope (SEM). Based on this study, it was found that the lowest contact resistance of $0.3664{\Omega}$ could be achieved when the sintering temperature of the silver nano-ink and surface roughness were $120^{\circ}C$ and 0.230 a, respectively.

A Study on Patterning Techniques by sliced unit with square woods's color bars (각목 색상 배치에 의한 문양막대의 횡절단 무늬편을 이용한 문양구성 연구)

  • Kim, Ji-Geon
    • Journal of the Korea Furniture Society
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    • v.20 no.5
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    • pp.431-439
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    • 2009
  • When we look at the pattern techniques of wooden furniture in the 19th century Joeson Dynasty, we see that furniture patterns in the main living room were showy and colorful while furniture patterns in the library room, where noble men used to study, were natural and moderate, retaining the actual color of the material without any artificial coloring. Even the serial patterns in the Hwe-Jang technique, Which were used rarely, used moderate techniques. such as weaving in patterns with colorless woods - willow and black persimmon ets. - rather than using excessive techniques. However, considering the marquetry&intarsia technique of ceramic and the silver string intarsia technique of metal then current, wood work must also have been technically advanced. Korean modern wood furniture needs remedies to improve the standard of sound wood work techniques. This study shows that pattern unit production, composition techniques, and color effects etc. Using colored patterns bars, by improving the pattern composition techniques of Marquetry&Intarsia, can be substituted for the production logic of modern manufactured furniture.

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