• Macromolecular Research
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• 제12권4호
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• pp.391-398
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• 2004

Thick-film photolithography is a new technology that combines lithography processes, such as exposure and development, with the conventional thick-film process applied to screen-printing. In this study, we developed a low-temperature cofireable silver paste applicable for thick-film processing to form fine lines using photolitho-graphic technologies. The optimum paste composition for forming fine lines was investigated. The effect of processing parameters, such as the exposing dose, had on the fine-line resolution was also investigated. As the result, we found that the type of polymer and monomer, the silver powder loading, and the amount of photoinitiator were the main factors affecting the resolution of the fine lines. The developed photoimageable silver paste was printed on a low-temperature cofireable green sheet, dried, exposed, developed in an aqueous process, laminated, and then fired. Our results demonstrate that thick-film fine lines having widths < 20 $\mu\textrm{m}$ can be obtained after cofiring.

• 대한금속재료학회지
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• 제48권9호
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• pp.856-860
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• 2010

Silver nanoparticles were formed on silica substrates through thin film dewetting at high temperature. The microstructural and morphological evolution of the particles were characterized as a function of processing variables such as initial film thickness, annealing time, and temperature. Silver thin films were deposited onto the silica using a pulsed laser deposition system and annealed in reducing atmosphere to induce agglomeration of the films. The film thicknesses before dewetting were in the range of 5 to 25 nm. A noticeable agglomeration occurs with annealing at temperatures higher than $300^{\circ}C$, and higher annealing temperature increases particle size uniformity for the same film thickness sample. Average particle size linearly correlates to the film thickness, but it does not strongly depend on annealing temperature and time, although threshold temperature for complete dewetting increases with an increase of film thickness. Lower annealing temperature develops faceted surface morphology of the silver particles by enhancing the growth of the low index crystal plane of the particles.

• 대한방사선기술학회지:방사선기술과학
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• 제44권3호
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• pp.219-224
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• 2021

The purpose of these experiments is often to scan infected patients with MRI. Therefore, it is to investigate whether the antibacterial film containing silver ions, which is a non-magnetic substance, affects magnetic resonance imaging. In this experiment, the ACR phantom was used, not the patient. The ACR phantom was wrapped in an antibacterial film and the SNR, CNR, sagittal localization image, and geometrical accuracy were compared before and after. The experiment was performed 10 times and the averaged values were compared. There were no significant differences in the results of all experiments. The FDA recommends removing metal and antibacterial film masks during MRI scans. The reason is that there was one case of injury with facial burns. When I touched the antibacterial film to check the fever during the 2 hour experiment, I did not feel any particular fever. In light of the experimental results, it would be helpful to use an antibacterial film when testing an infected patient. The reason is that there isn't a difference before and after the experiment of SNR, CNR, and sagittal localization images.

• 한국세라믹학회:학술대회논문집
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• 한국세라믹학회 1986년도 Priceedings Of The Third Korea-Japan Seminar On New Ceramics
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• pp.259-267
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• 1986

The sintering behavior of silver-oxide glass composite thick-film has been studied with varing glass content. It is shown that during heat treatment glass became liquid phase to deeply affect the microstructure development of the silver particles and to control the physical properties of the thick-films. As glass content increased, the initial repacking of silver particles took place rapidly but the homogeneities of the microstructure showed different features. When the glass content was over some range, the silver particles exuded glass to decrease net energy and glass formed liquid pools separated from the solid skeletons. Finally the relations between the microstructures and electrical properties of the thick-film were discussed.

• 한국환경농학회지
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• 제38권3호
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• pp.124-132
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• 2019

BACKGROUND: Silver grass (Miscanthus sinensis) No. 1 was developed for production of bio-ethanol, and for the purpose the silver grass growing sector was established in Geumgang basin, Iksan, Jeonbuk, in 2011. However, the other application potentials except for using as the bio-energy resources should be considered because of the drop in international oil prices. Therefore, there is the necessity of a scientific basis to use the silver grass instead of rice straw as the organic matter source that is used for improvement of soil quality in the plastic film house. METHODS AND RESULTS: The silver grass was applied at 5, 10, 15 and 20 Mg/ha and tilled before the watermelon was planted in the plastic film-house. The control plot was treated with 10 Mg/ha with rice straw, and watermelons have been cultivated for 3 years(2017~2019). Soil aggregation, soil chemistry, and the growth characteristics were investigated, when the watermelon was harvested every year. Soil aggregation levels at the 2nd and 3rd year of watermelon harvest were similar from the plot applied with the silver grass at 5 Mg/ha and the control plot, and increased in the silver grass treated plots with more than 10 Mg/ha. However, there was no statistically significant difference between the plots. The nitrogen mineralization of silver grass in the control plot tended to be similar to the 5 Mg/ha plot, but the silver grass treated plots with over 10 Mg/ha showed low nitrogen mineralization. Soil EC on harvest stage was proportional to the applied mass of the silver grass, but pH was in inverse with the applied mass. Soil organic matter content, available phosphate, and exchangeable cations increased with the continued use of silver grass. Watermelon weight found to be the best on more than 15 Mg/ha of silver grass, and the sugar content was highest when 10 Mg/ha was treated. CONCLUSION: The use of the silver grass at 10 Mg/ha annually as the organic source was effective in replacing rice straw while growing fruits and vegetables on the plastic film house.

• 마이크로전자및패키징학회지
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• 제29권2호
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• pp.107-112
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• 2022

본 연구에서는 용제를 전혀 사용하지않고 UV경화가 가능한 실버 페이스트를 개발하였다. 무용제(solvent-free) 타입으로 개발한 실버 페이스트의 점도 및 점탄성 측정하였다. 그리고 스크린인쇄로 패턴을 인쇄한 후에 UV경화로 전극도막을 형성시켰다. 형성된 전극도막의 전도성, 연필경도, 접착력에 대해서 평가하였다. 마지막으로 전극도막의 경화특성은 TGA 및 FT-IR로 평가하였다. 이러한 결과를 정리하면 전도성, 접착력, 경화특성에 대해서는 Paste(4), 즉 1.2 ㎛의 구형 실버 파우더와 50 nm 실버 파우더를 72:8%로 혼합한 실버 페이스트가 가장 우수한 물성이 얻어짐을 알 수 있었다.

• 한국분말재료학회지
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• 제24권6호
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• pp.464-471
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• 2017

A metal mesh TCE film is fabricated using a series of processes such as UV imprinting of a transparent trench pattern (with a width of $2-5{\mu}m$) onto a PET film, filling it with silver paste, wiping of the surface, and heat-curing the silver paste. In this work nanosized (40-50 nm) silver particles are synthesized and mixed with submicron (250-300 nm)-sized silver particles to prepare silver paste for the fabrication of metal mesh-type TCE films. The filling of these silver pastes into the patterned trench layer is examined using a specially designed filling machine and the rheological testing of the silver pastes. The wiping of the trench layer surface to remove any residual silver paste or particles is tested with various mixture solvents, and ethyl cellosolve acetate (ECA):DI water = 90:10 wt% is found to give the best result. The silver paste with 40-50 nm Ag:250-300 nm Ag in a 10:90 wt% mixture gives the highest electrical conductance. The metal mesh TCE film obtained with this silver paste in an optimized process exhibits a light transmittance of 90.4% and haze at 1.2%, which is suitable for TSP application.

• Korean Chemical Engineering Research
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• 제61권3호
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• pp.439-445
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• 2023

본 연구에서는 질산은을 PVA로 환원시켜 은 나노입자를 합성하였으며, 얻어진 은 나노입자에 Carboxymethyl cellulose (CMC)를 첨가시켜 제조된 용액을 PET 기재 위에 코팅함에 의해 항균 특성과 김서림 방지 기능을 갖는 코팅 도막을 제조하였다. 코팅 도막을 80 ℃의 수증기와 접촉 시 코팅되지 않은 PET 기재는 김서림 발생으로 인한 빛의 산란이 발생해 흐려진 결과를 보인 반면에 CMC가 첨가된 은 나노졸로 코팅된 도막은 수증기와의 접촉에도 불구하고 투명한 상태를 유지하여 김서림 방지 기능이 우수하였다. 또한 코팅 도막의 항균성을 그램 양성균인 포도상구균과 그람 음성균인 대장균에 대해 필름 밀착법으로 측정하였다. 코팅되지 않은 PET 기재에서는 많은 포도상구균과 대장균의 집락이 관찰된 반면에 은 나노졸로 코팅된 도막은 포도상구균과 대장균의 성장이 크게 억제되어 항균 효과가 우수하였다.

• E2M - 전기 전자와 첨단 소재
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• 제10권7호
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• pp.713-718
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• 1997

Polyaniline free standing films cast from N-methyl-2-pyrrolidinone(NMP) solution, camphorsulfonic acid(HCSA), dodecylbenzensulfonic acid(HDBSA), inorganic matter(carbon black, graphite) and metal(silver) were prepared by processings. The properties of these films such as crystallinity, near-infrared absorption spectra and conductivity were investigated. The HCSA and HDBSA doped polyaniline films cast from m-cresol and chloroform solvents showed the metallic property and high crystallinity, respectively. The value of conductivity in the HCSA doped polyaniline film obtained 180 S/cm. We have obtained the value of conductivity 200 S/cm in the metal(silver) doped polyaniline film, which is higher than that of the HCSA doped polyaniline film. The metal(silver) doped polyaniline film shows good properties as a electromagnetic shielding material.

• 열처리공학회지
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• 제19권4호
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• pp.219-224
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• 2006

Silver paste with low sintered temperature has been developed in order to apply electronic parts, such as bus electrode, address electrode in PDP (Plasma Display Panel) with large screen area. In this study, nano-sized silver particles with 10-30 nm were synthesized from silver nitrate ($AgNO_3$) solution by chemical reduction method and silver paste with low sintered temperature was prepared by mixing silver nanoparticles, conventional silver powder with the particle size 1.6 um and Pb-free frit. Conductive thick film from silver paste was fabricated by screen printing on alumina substrate. After firing at $540^{\circ}C$, the cross section and surface morphology of the thick films were analyzed by FE-SEM. Also, the sheet resistivity of the fired thick films was measured using the four-point technique.