• Title/Summary/Keyword: second phases

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The Effects of Second Phases on the Photocatalytic Characteristics of the TiO2 base Nano Composite (TiO2계 나노 복합촉매 특성에 미치는 생성상의 영향)

  • 안인섭;고봉석;배승열
    • Journal of Powder Materials
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    • v.11 no.2
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    • pp.143-148
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    • 2004
  • In the present study, $TiO_2$ imbedded composite powders have been successfully prepared from the (Cu. Zn)/$TiO_2$ composite salt solution. The composite (Cu, Zn)/$TiO_2$ powders were formed by drying the solution at 200~$600^{\circ}C$ in the hydrogen atmosphere. Photocatalytic characteristics was evaluated by detecting the decomposition ratio of aniline blue with UV-visible spectrophotometer(Shimazu Co., UV-1601). Phase analysis of (Cu, Zn)/$TiO_2$ composite powders was carried out by XRD and DSC, and powder size was measured with TEM. The mean particle size of composite powders was about 100mm. As the reduction temperature increases, a few zinc sulfide and oxide phases was formed and copper oxide phase was reduced. The decomposition ratio of aniline blue was about 80% under the UV irradiation by the TiO$_2$ phase in the composite (Cu, Zn)/$TiO_2$ powders and similar decomposition ratio of 80% was obtained at the UV lightless condition by virtue of Cu and Zn compounds.

Phase transformation of $REBa_2Cu_3O_{7-x}$ (RE=Nd, Gd, Dy) Superconductor during Continuous Cooling and Isothermal Heat Treatment (등온열처리와 냉각에 따른 $REBa_2Cu_3O_{7-x}$ (RE=Nd, Gd, Dy) 초전도체의 상변화)

  • O, Yong-Taek;Shin, Dong-Chan;Han, Young-Hee;Sung, Tae-Hyun;Jeong, Nyeon-Ho
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.05a
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    • pp.42-45
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    • 2003
  • The phase transformation of $REBa_2Cu_3O_{7-x}$ (RE=Nd, Gd, Dy) was investigated using isothermal heat-treatment and continuous cooling in air. During continuous cooling, the $REBa_2Cu_3O_{7-x}$ (RE=123) superconducting phase with well-distributed $REBa_2Cu_3O_{7-x}$ (RE-211) was obtainde at a cooling rate of $0.001^{\circ}C$/s. Single phase RE-123 (Nd, Gd, Dy) was stable at $1050^{\circ}C$, $1050^{\circ}C$, and $950^{\circ}C$ during isothermal heat-treatment, respectively. Above these temperatures the RE-211 phase existed within the RE-123 grains. The RE-123, RE-211, $BaCu_2Od_2$, and CuO phases coexisted at $50^{\circ}C$ below the partial melting temperature for each respective rare-earth RE-123.

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New Liquid Crystalline Methacrylate Polymers Containing 4-Methacryloyloxyphenoxy Group and 4'-((S)-(+)-2-Methylbutoxy)biphenyl-4-carboxyl Mesogenic Group: 1. Synthesis and Characterization of the Monomers (4-Methacryloyloxyphenoxy기와 4'-((S)-(+)-2-methylbutoxy)biphenyl-4-carboxyl 메소겐기를 갖는 새로운 메타크릴레이트 액정화합물: 1. 단량체의 합성 및 특성)

  • So, Bong-Keun;Lee, Sang-Ho;Lee, Soo-Min
    • Journal of the Korean Chemical Society
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    • v.48 no.6
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    • pp.599-608
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    • 2004
  • New two kinds of methacrylate monomers having a benzene ring inserted between spacer and methacryloyl group and the chiral center connected to the terminal of the mesogenic structures were synthesized. In these two series the effects for the formation of the liquid crystals in regard to the length changes of the spacers and mesogenic groups were investigated. The first series did not show any liquid crystalline phases in the intermediate compounds nor in the end products. However, the methacrylates of second series showed the liquid crystalline phases in the intermediate compounds as well as in the final products regardless of the length of the spacers.

Spray Combustion Simulation in Transverse Injecting Configurations

  • Yi, Yoon-Yong;Roh, Tae-Seong
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2004.03a
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    • pp.186-191
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    • 2004
  • The reactive flowfield of the transverse injecting combustor has been studied using Euler-Lagrange method in order to develop an efficient solution procedure for the understanding of liquid spray combustion in the transverse injecting combustor which has been widely used in ramjets and turbojet afterburners. The unsteady two-dimensional gas-phase equations have been represented in Eulerian coordinates and the liquid-phase equations have been formulated in Lagrangian coordinates. The gas-phase equations based on the conservation of mass, momentum, and energy have been supplemented by combustion. The vaporization model takes into account the transient effects associated with the droplet heating and the liquid-phase internal circulation. The droplet trajectories have been determined by the integration of the Lagrangian equation in the flow field obtained from the separate calculation without considering the iterative effect between liquid and gas phases. The reported droplet trajectories had been found to deviate from the initial conical path toward the flow direction in the very end of its lifetime when the droplet size had become small due to evaporation. The integration scheme has been based on the TEACH algorithm for gas-phase equation, the second order Runge-Kutta method for liquid-phase equations and the linear interpolation between the two coordinate systems. The calculation results has shown that the characteristics of the droplet penetration and recirculation have been strongly influenced by the interaction between gas and liquid phases in such a way that most of the vaporization process has been confined to the wake region of the injector, thereby improving the flame stabilization properties of the flowfield.

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Effect of Calcination Temperature and Sintering Additives on the Sintering Behaviors and Microwave Dielectric Properties of $(Zn_{0.8}Mg_{0.2})TiO_3$ (하소온도와 소결조제가 $(Zn_{0.8}Mg_{0.2})TiO_3$계의 소결거동과 마이크로파 유전특성에 미치는 영향)

  • Sim, Woo-Sung;Bang, Jae-Cheol
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.05c
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    • pp.282-286
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    • 2003
  • We investigated the effects of calcination temperature and sintering additives on the sintering behaviors and microwave dielectric properties of $(Zn_{0.8}Mg_{0.2})TiO_3$. Highly densified samples were obtained at the sintering temperatures below $1000^{\circ}C$ with additions of 0.45 wt.% $Bi_2O_3$ and 0.55 wt.% $V_2O_5$. From the examination of the existing phases and microstructures before and after sintering of $(Zn_{0.8}Mg_{0.2})TiO_3$ system calcined at the various temperatures ranging from $800^{\circ}C$ to $1000^{\circ}C$, it was found that high $Q{\times}f_o$ values were obtained when unreacted or second phases in calcined body were reduced. When calcined at $1000^{\circ}C$ and sintered at $900^{\circ}C$, it consists of hexagonal as a main phase with uniform microstructure and exhibits $Q{\times}f_o$ value of 42,000 GHz and dielectric constant of 22.

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A Method of Lane Marker Detection Robust to Environmental Variation Using Lane Tracking (차선 추적을 이용한 환경변화에 강인한 차선 검출 방법)

  • Lee, Jihye;Yi, Kang
    • Journal of Korea Multimedia Society
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    • v.21 no.12
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    • pp.1396-1406
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    • 2018
  • Lane detection is a key function in developing autonomous vehicle technology. In this paper, we propose a lane marker detection algorithm robust to environmental variation targeting low cost embedded computing devices. The proposed algorithm consists of two phases: initialization phase which is slow but has relatively higher accuracy; and the tracking phase which is fast and has the reliable performance in a limited condition. The initialization phase detects lane markers using a set of filters utilizing the various features of lane markers. The tracking phase uses Kalman filter to accelerate the lane marker detection processing. In a tracking phase, we measure the reliability of the detection results and switch it to initialization phase if the confidence level becomes below a threshold. By combining the initialization and tracking phases we achieved high accuracy and acceptable computing speed even under a low cost computing resources in which we cannot use the computing intensive algorithm such as deep learning approach. Experimental results show that the detection accuracy is about 95% on average and the processing speed is about 20 frames per second with Raspberry Pi 3 which is low cost device.

Analysis of Domestic Manual Lymph Drainage (MLD)-related Research Trend (국내 림프드레나지(MLD) 연구에 관한 논문 동향 분석)

  • Mun, Ji-Hyun;Kim, Min-Hee
    • Fashion & Textile Research Journal
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    • v.24 no.5
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    • pp.636-646
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    • 2022
  • This study attempted to investigate the research trend of MLD studies which were issued from 2001 to March 2022 by research period/area/method/purpose through the analysis of academic theses and journals and use the results for the growth and of MLD. The study results found the followings: First, in terms of the results by research period, a total of 84 academic papers and journals were published: Phase 1 (15), Phase 2 (47), Phase 3 (22). Second, when analyzed by research area, 'cosmetology' was the highest with 19 papers in terms of the number of studies. In fact, the field of study accounted for the largest portion in all three phases. Third, when analyzed by research method, quantitative research showed the largest percentage in all three phases. Fourth, when analyzed by research purpose, a practical approach was dominant with 81 papers out of the total number of 84 (3 papers in theoretical approach). Concerning a domestic MLD-related research trend, it is an essential step for MLD study establishment and qualitative improvements. Such research analysis of MLD studies is meaningful in that it has not been attempted before. In addition, it is anticipated that the study results would be helpful in searching a direction for the academic growth and development of MLD.

A Study on the Development of a MOOC Design Model

  • LEE, Gayoung;KEUM, Sunyoung;KIM, Myungsun;CHOI, Yoomi;RHA, Ilju
    • Educational Technology International
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    • v.17 no.1
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    • pp.1-37
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    • 2016
  • The purpose of this study was to develop a MOOC design model that would improve the current practice of MOOC development in Korea by specifying easy-to-use course development procedures and guiding strategies. Following Richey and Klein (2007)'s conceptual model development procedure, the first step was to perform critical review of relevant literature and observe typical MOOC development processes. As a result, the initial model was developed. The second step was to conduct the expert review with five educational technology and MOOC researchers to secure the internal validity of the model. Based on the experts' suggestions, the model was revised and once again reviewed by the same experts. This process resulted in the development of the 2nd version of model. The third step was to carry out external validation research in order to test the effectiveness, efficiency, and usability of the model. A basic model may be confirmed or corrected based on examination of its results. Consequently, the model was elaborated as the final model. In the final model, 6 procedural phases and 9 specific steps were included. The six procedural phases are: Analysis (1st Iteration), Design, Development (Course Development), Implementation, Evaluation, and Analysis (2nd Iteration), a slight variation of ADDIE model. The specific steps include: 1) Goal Setting, 2) Environment Analysis, 3) Content Design, 4) Style Design, 5) Course Development, 6) Implementation Plan, 7) Course Implementation, 8) Summative Evaluation, and 9) Need Reflection. The study concluded with suggestions for further research and application of the MOOC design model.

Effect of Calcining Temperature on the Sintering Behaviors and Microwave Dielectric Properties of $Ba(Mg_{1/3}Ta_{2/3})O_3$ Ceramics (하소온도의 변화에 따른 $Ba(Mg_{1/3}Ta_{2/3})O_3$계 세라믹스의 소결 거동과 마이크로파 유전특성)

  • 이정아;김정주;이희영;김태홍;최태구
    • Journal of the Korean Ceramic Society
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    • v.31 no.12
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    • pp.1561-1569
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    • 1994
  • Effect of calcining temperature on the sintering behaviors and microwave dielectric properties of BMT[Ba(Mg1/3Ta2/3)O3] ceramics was studied. The calcining temperatures were varied from 80$0^{\circ}C$ to 130$0^{\circ}C$, respectively. It was found that, as calcining temperature lowered below 125$0^{\circ}C$, second phase such as Ba5Ta4O15 phases started to appear in calcined powder with unreacted powders. After sintering, exaggerately grown Ba5TaO3 phase could be found amang the uniform BMT grains in sintered body. Basis on the infiltration experiment, Ba0.05TaO3 phase should be formed by reaction of BMT grain and BaO-MgO eutectic liquid. But increase of calcining temperature above 125$0^{\circ}C$, there was not any second phase or unreated component in calcined powder and sintered body. As result, low calcining temperature led to precipitation of second phase in specimen and resulted decrease of Q value of BMT ceramics.

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The empirical study on e-learning quality and its relevant constructs (이러닝 품질과 관련 변인에 대한 실증연구)

  • Lee, Misook
    • Journal of Korean Society for Quality Management
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    • v.45 no.4
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    • pp.917-932
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    • 2017
  • Purpose: This study aims to identify the most important quality construct among system quality, information quality, and service quality, which are integrated as the second-order construct; perceived quality, and to investigate the relationship between perceived quality, learner satisfaction, learner enjoyment, switching cost, and learner loyalty. Method: Data were collected from learners who had taken e-learning course, and the analysis was conducted in two phases. The first phase described demographic characteristics using SPSS23.0; the second phase involved the second order CFA of perceived quality and the analysis of measurement model and structural model through AMOS 23.0. Results: (1) The explanatory power of system quality, information quality, and service quality appears to be almost equal; (2) Perceived quality positively influences only both learner satisfaction and switching cost; (3) Only learner satisfaction positively influences learner loyalty and switching cost negatively influences learner loyalty. Conclusion: Learner enjoyment does not play an important role in this study, which could be extrapolated in regard to the characteristics of sample. The respondents are over high school students, who emphasize on the acquisition of knowledge rather than enjoyment. Additionally, the result implies that respondents show low loyalty in the high switching cost.