• Title/Summary/Keyword: scanning electron microscopy (SEM) scale

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Scanning Electron Microscopic Study of Scales Surrounding the Surface of Newborn Hair (신생아 모발 표면을 둘러싸고 있는 비늘에 관한 주사전자현미경적 연구)

  • Jung, Hee Joong;Jin, Hyun Sook;Jang, A Young;Jang, Eun Joo;Chang, Byung Soo;Kim, Kyung Sook
    • Journal of Convergence for Information Technology
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    • v.10 no.5
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    • pp.216-223
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    • 2020
  • We investigated the morphology of the scalp hair shaft from the base to the distal end of the newborn hair and the ratio of the longitudinal axis diameter of the scale exposed to the surface of the hair to the diameter of the hair by scanning electron microscopy(SEM). Neonatal hair was observed to taper from the area adjacent to the scalp toward the end of the hair. In this study, as the thickness of the hair increases, the ratio of the long axis diameter of the exposed scale becomes relatively small, but the long axis diameter of the exposed scale on the surface of the hair is similar in length regardless of the thickness of the hair. In conclusion, it was confirmed that the major axis diameter of the scales exposed to the surface of fine or thick hair does not change significantly.

Innovative Remediation of Arsenic in Groundwater by Nano Scale Zero-Valent Iron

  • Kanel, Sushil-Raj;Kim, Ju-Yong;Park, Heechul
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2003.09a
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    • pp.87-90
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    • 2003
  • This research examines the feasibility of using laboratory-synthesized nano scale zero-valent iron particles to remove arsenic from aqueous phase. Batch experiments were performed to determine arsenic sorption rates as a function of the nano scale zero-valent iron solution concentration. Rapid adsorption of arsenic was achieved with the nano scale zero-valent iron. Typically 1 mg $L^{-1}$ arsenic (III) was adsorbed by 5 g $L^{-1}$ nano scale zero-valent iron below the 0.01 g $L^{-1}$ concentration within 7min. The kinetics of the arsenic sorption followed pseudo-first-order reaction kinetics. Observed reaction rate constants ( $K_{obs}$) varied between 11.4 to 129.0 $h^{-1}$ with respect to different concentrations of nano scale zero-valent iron. A variety of analytical techniques were used to study the reaction products including HGAAS (hydride generator atomic adsorption spectrophotometer), SEM (scanning electron microscopy) and TEM (transmission electron microscopy). Our experimental results suggest novel method for efficient removal of arsenic Iron groundwater.r.

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Effect of Co-solvent Ratios and Solution Concentrations on Morphologies of Electrospun Zein Nanomaterials

  • Rabbani, Mohammad Mahbub;Kim, Young Hun;Yeum, Jeong Hyun
    • Current Research on Agriculture and Life Sciences
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    • v.31 no.1
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    • pp.11-17
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    • 2013
  • To investigate the effects of co-solvents on the morphology of nano-scale zein materials, zein solutions were electrospun with different co-solvent ratios of EtOH/$H_2O$. Different zein solution concentrations were used to study the effects of the zein content on the electrospun materials. The resulting electrospun materials were all characterized using field-emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). The diameters of the electrospun nanoparticles and nanofibers were found to increase when increasing the EtOH ratio at certain zein concentrations. Furthermore, increasing the zein content changed the morphology of the electrospun materials from nanoparticles to nanofibers.

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Preparation of Cellulose Acetate Membrane and Its Evaluation as a Forward Osmosis Membrane (셀룰로오스 아세테이트 분리막 제조 및 정삼투 성능 평가)

  • Ahn, Hyeryun;Kim, Jinhong;Kwon, Young-Nam
    • Membrane Journal
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    • v.24 no.2
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    • pp.136-141
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    • 2014
  • In this study, cellulose acetate (CA) membrane was prepared by phase inversion precipitation and then evaluated the forward osmosis (FO) membrane performance. Differences in water flux and salt rejection between RO and FO with prepared membranes were observed. The different structure membranes were prepared with various solvent which evaluate the influence of membrane structure on permeability. The structure of the prepared membrane was confirmed through scanning electron microscopy (SEM) and the permeability changes were estimated using the bench-scale FO test equipment.

Development of a Blended Corrosion, Scale and Micro-Organism Inhibitor for Open Recirculating Cooling System

  • Choi, Dong-Jin;You, Seung-Jae;Kim, Jung-Gu;Hwang, Woo-Suk
    • Corrosion Science and Technology
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    • v.4 no.3
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    • pp.89-94
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    • 2005
  • This paper presents the results of a study that was undertaken to optimize the ratio of the components of a new multi-component inhibitor blend composed of orthophosphate/ phosphonates/ acrylate copolymer/ isothiazolone. The effects of newly developed inhibitor on carbon steel dissolution in synthetic cooling water were studied through weight loss tests, electrochemical tests, scale tests, and micro-organism tests. The obtained results were compared to blank (uninhibited specimen) and showed that developed inhibitor revealed very good corrosion, scale, and micro-organism inhibition simultaneously. All measurements indicated that the efficiency of the blended mixture exceeded 90 %. The inhibitive effects arose from formation of protective films which might contain calcium phosphate, calcium phosphonate, and iron oxide. The nature of protective films formed on the carbon steel was studied by scanning electron microscopy (SEM) and auger electron spe ctroscopy (AES). Inhibitor used in this study appeared to have better performance for scale inhibition due to their superior crystal modification effect and excellent calcium carbonate scale inhibition properties. The effect of inhibitor on microorganisms was evaluated through minimum inhibitory concentration (MIC) test. All kinds of micro-organisms used in this study were inhibited under 78ppm concentration of inhibitor.

Analyses of Fouling Mechanism using Visualization Techniques in a Lab-scale Plate-Type Heat Exchanging System (실험실용 판형 열교환 시스템에서 가시화를 이용한 파울링 기구 해석)

  • 성순경;서상호;노형운
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.16 no.4
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    • pp.349-354
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    • 2004
  • Scale is formed when hard water is heated or cooled in heat transfer equipments such as heat exchangers, condensers, evaporators, cooling towers, boilers, and pipe walls. When the scale deposits in a heat exchanger surface, it is conventionally called fouling. The objective of the present study is to analyze the process of the fouling formation in a heat exchanger according to different types of water using visualization techniques. In order to experimentally investigate the formation of the fouling, this study built a lab-scaled heat exchanging system. Using the visualization techniques of Scanning Electron Microscopy (SEM) and X-Ray diffraction method, the three dimensional configurations of the fouling formation could be successfully obtained. Based on the experimental results, it was found that the configurations of the fouling formation were different when using tap water compared to river water.

Flexural behavior of carbon nanotube-modified epoxy/basalt composites

  • Kim, Man-Tae;Rhee, Kyong-Yop
    • Carbon letters
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    • v.12 no.3
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    • pp.177-179
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    • 2011
  • The use of carbon nanotubes (CNTs) as a reinforcing material in a polymer matrix has increased in various industries. In this study, the flexural behavior of CNT-modified epoxy/basalt (CNT/epoxy/basalt) composites is investigated. The effects of CNT modification with silane on the flexural properties of CNT/epoxy/basalt composites were also examined. Flexural tests were performed using epoxy/basalt, oxidized CNT/epoxy/basalt, and silanized CNT/epoxy/basalt multi-scale composites. After the flexural tests, the fracture surfaces of the specimens were examined via scanning electron microscopy (SEM) to investigate the fracture mechanisms of the CNT/epoxy/basalt multi-scale composites with respect to the CNT modification process. The flexural properties of the epoxy/basalt composites were improved by the addition of CNTs. The flexural modulus and strength of the silane-treated CNT/epoxy/basalt multi-scale composites increased by approximately 54% and 34%, respectively, compared to those of epoxy/basalt composites. A SEM examination of the fracture surfaces revealed that the improvement in the flexural properties of the silane-treated CNT/epoxy/basalt multi-scale composites could be attributed to the improved dispersion of the CNTs in the epoxy.

Application of Scanning Electron Microscopy (SEM) for Biotically Induced Microstructure Observation in Sedimentary Sample of Natural Condition (주사전자현미경 분석을 활용한 자연환경 퇴적시료의 생물기원구조 관찰)

  • Park, Hanbeom;Kim, Jinwook
    • Korean Journal of Mineralogy and Petrology
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    • v.33 no.3
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    • pp.165-173
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    • 2020
  • The activity of living microorganism directly or indirectly affects to the biomineralization in sediments and rocks that display the unique biotic structure. Minerals in the biotic structures showed unique properties and bypass the thermodynamic and kinetic barriers. Therefore, investigations on the biotically induced microstructure is essential to identify the new mineral formation mechanism by analyzing crystal structures and morphology at a nano-scale. The significant implication as well as advantages of using scanning electron microscopy to characterize the biotic structures were discussed in this paper for the examples of hydrothermal vent area microbial mat and deep-sea ferromanganese crust sample.

Fabrication and Thermal Oxidation of ZnO Nanofibers Prepared via Electrospinning Technique

  • Baek, Jeong-Ha;Park, Ju-Yun;Kang, Ji-Soo;Kim, Don;Koh, Sung-Wi;Kang, Yong-Cheol
    • Bulletin of the Korean Chemical Society
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    • v.33 no.8
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    • pp.2694-2698
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    • 2012
  • Materials on the scale of nanoscale have widely been used as research topics because of their interesting characteristics and aspects they bring into the field. Out of the many metal oxides, zinc oxide (ZnO) was chosen to be fabricated as nanofibers using the electrospinning method for potential uses of solar cells and sensors. After ZnO nanofibers were obtained, calcination temperature effects on the ZnO nanofibers were studied and reported here. The results of scanning electron microscopy (SEM) revealed that the aggregation of the ZnO nanofibers progressed by calcination. X-ray diffraction (XRD) study showed the hcp ZnO structure was enhanced by calcination at 873 and 1173 K. Transmission electron microscopy (TEM) confirmed the crystallinity of the calcined ZnO nanofibers. X-ray photoelectron spectroscopy (XPS) verified the thermal oxidation of Zn species by calcination in the nanofibers. These techniques have helped us deduce the facts that the diameter of ZnO increases as the calcination temperature was raised; the process of calcination affects the crystallinity of ZnO nanofibers, and the thermal oxidation of Zn species was observed as the calcination temperature was raised.

Surface Measurement of Microstructures Using Optical Pick-up Based Scanner (광픽업 스캔 장치를 이용한 미소 구조물의 표면 측정)

  • Kim, Jae-Hyun;Park, Jung-Yul;Lee, Seung-Yop
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.34 no.1
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    • pp.73-76
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    • 2010
  • The issue of inspection and characterization of microstructures has emerged as a major consideration in design, fabrication, and detection of MEMS devices. However, the conventional measurement techniques, including scanning electron microscopy (SEM) imaging, atomic force microscopy (AFM) scanning, and mechanical surface profiler, require often destructive process or may be difficult to measure with a wafer scale. In this paper, we characterize the surface profiles of microstructures using an optical scanner based on a DVD pick-up module. Scanning images of the microstructures are successfully generated using the intensity of reflected light from different depths of the surface profiles, based on the focus error signal (FES) from photodiodes. It is shown that the proposed optical scanner can be used as an alternative measurement system with high performance and low cost, compared to conventional measurement techniques.