• Title/Summary/Keyword: sample and holder

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Experimental Verification on Factors Affecting Core Resistivity Measurements (II)-Characteristics of Time Series Data and Determination Method of Resistivity (코어비저항 측정에 미치는 영향요소에 대한 실험적 고찰(Ⅱ) - 시계열자료의 특성과 대표비저항 값의 결정)

  • Kim, Yeong Hwa;Choe, Ye Gwon
    • Journal of the Korean Geophysical Society
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    • v.2 no.4
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    • pp.269-276
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    • 1999
  • As a part of trying to get the resistivity values correctly from laboratory core resistivity measurement, the effect of sample holders in resistivity measurement was analyzed and a better way to determine the representative resistivity value from the time series resistivity data was searched. Modified GS type and modified two-electrode type sample holders were devised and their effects have been compared with those of GS and two-electrode type sample holders. The modified two-electrode type sample holder has benefits both in repetition and simplicity in data acquisition. The analysis of distribution trend of the time series resistivity data obtained with different kind of sample holders and source frequencies shows that the maximum curvature point method gives the best result in determining representative resistivity value.

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THE NONDESTRUCTIVE MEASUREMENT OF THE SOLUBLE SOLID AND ACID CONTENTS OF INTACT PEACH USING VIS/NIR TRANSMITTANCE SPECTRA

  • Hwang, I.G.;Noh, S.H.;Lee, H.Y.;Yang, S.B.
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 2000.11b
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    • pp.210-218
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    • 2000
  • Since the SSC(soluble solid contents) and titratable acidity of fruit are highly concerned to the taste, the need for measuring them by non-destructive technology such as NIR(Visual and Near-infrared) spectroscopy is increasing. Specially, in order to grade the quality of each fruit with a sorter at sorting and packing facilities, technologies for online measurement satisfying the tolerance in terms of accuracy and speed should be developed. Many researches have been done to develop devices to measure the internal qualities of fruit such as SSC, titratable acidity, firmness, etc. with the VIS(Visual)/NIR(Near Infrared) reflectance spectra. The distributions of the SSC, titratable acidity, firmness, etc. are different with respect to the position and depth of fruit, and generally the VIS/NIR light can interact with fruit in a few millimeters of pathlength, and it is very difficult to measure the qualities of inner flesh of fruit. Therefore, to measure the average concentrations of each quality factor such as SSC and titratable acidity with the reflectance-type NIR devices, the spectra of fruit at several positions should be measured. Recently, the interest about the transmittance-type VIS/NIR devices is increasing. NIR light can penetrate through the fruit about 1/10-1/1,000,000 %. Therefore, very intensive light source and very sensitive sensor should be adopted to measure the transmitted light spectra of intact fruit. The ultimate purpose of this study was to develop a device to measure the transmitted light spectra of intact fruit such as apple, pear, peach, etc. With the transmittance-type VIS/NIR device, the feasibility of measurement of the SSC and titratable acidity in intact fruit cultivated in Korea was tested. The results are summarized as follows; A simple measurement device which can measure the transmitted light spectra of intact fruit was constructed with sample holder, two 500W-tungsten halogen lamps, a real-time spectrometer having a very sensitive CCD array sensor and optical fiber probe. With the device, it was possible to measure the transmitted light spectra of intact fruit such as apple, pear and peach. Main factors affecting the intensity of transmitted light spectra were the size of sample, the radiation intensity of light source and the integration time of the detector. Sample holder should be designed so that direct light leakage to the probe could be protected. Preprocessing method to the raw spectrum data significantly influenced the performance of the nondestructive measurement of SSC and titratable acidity of intact fruit. Representative results of PLS models in predicting the SSC of peach were SEP of 0.558 Brix% and R2 of 0.819, and those in predicting titratable acidity were SEP of 0.056% and R2 of 0.655.

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Structural and Morphological Changes of Co Nanoparticles and Au-10at.%Pd Thin Film Studied by in Situ Heating in a Transmission Electron Microscope

  • Ji, Yoon-Beom;Park, Hyun Soon
    • Applied Microscopy
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    • v.47 no.3
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    • pp.208-213
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    • 2017
  • The microstructural changes in Co nanoparticles and an Au-10at.%Pd thin film have been investigated using an in situ heating holder with a micro-electro-mechanical system (MEMS). In Co nanoparticles, two phases (face-centered cubic and hexagonal close-packed crystal structures) were found to coexist at room temperature and microstructures at temperatures, higher than $1,000^{\circ}C$, were observed with a quick response time and significant stability. The actual temperature of each specimen was directly estimated from the changes in the lattice spacing (Bragg-peak separation). For the Au-10at.%Pd thin film, at a set temperature of $680^{\circ}C$, the actual temperature of the sample was estimated to be $1,020^{\circ}C{\pm}123^{\circ}C$. Note that the specimen temperature should be carefully evaluated because of the undesired effects, i.e., the temperature non-uniformity due to the sample design of the MEMS chip, and distortion due to thermal expansion.

An Improved Soil Core Sampler (개량(改良)된 토양(土壤) 코어 시료(試料) 채취기(採取器))

  • Hwang, Jae Hong;Son, Yowhan;Kim, Jong Sung
    • Journal of Korean Society of Forest Science
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    • v.90 no.6
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    • pp.788-791
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    • 2001
  • An improved double-cylinder hammer-driven sampling device was designed to extract undisturbed soil cores. The improvements consist of 1) separation of hammer from the driving head, 2) a split inside cylinder, and 3) a plastic sample holder. Pushing the sampler deep into the soil before hammering would result in less compression of the sample. Core samples should be taken in soils of medium moisture content. The improved soil core sampler provides sufficiently accurate volumetric soil samples with original soil layers and soil cores of 40cm in length and 5cm in diameter.

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Comparison of Analytical Methods for α-Quartz by FTIR and XRD (FTIR과 XRD를 이용한 α-Quartz 분석법 비교)

  • Kim, Boo-Wook;Lee, Jong-Seong;Choi, Byung-Soon
    • Journal of Environmental Health Sciences
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    • v.35 no.2
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    • pp.130-142
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    • 2009
  • This study compared FTIR with XRD method for the analysis of quartz by % recovery, coefficient of variation (CV) and influence of the interference. the results were as the following. 1. In FTIR method, the coefficient of determination ($r^2$) was 0.9998 in a calibration curve of $695\;cm^{-1}$, and the limit of detection was $4.9{\mu}g/sample$. 2. The highest recovery was $799\;cm^{-1}$ (98.2%). 3. The CVpooled of the FTIR method was approximately 10% in three wave numbers. 4. The analysis of qualitative and quantitative for quartz is difficult with mixed cristobalite and iron oxide. 5. In XRD method with rotating sample holder and LynxEye detector, the coefficient of determination was 0.9996 in a calibration curve, and the limit of detection was $5.9{\mu}g/sample$. 6. The recovery and CV pooled were 104.3%, and 11 %, respectively. 7. In muffle furnace ashing, the quartz weight decreased to 34% when the maximum weight of the iron oxide was more than eight times. In conclusion, the accuracy (% recovery) and precision (CV) of FTIR and XRD method for analyzing $\alpha$-quartz were similar. FTIR method was a disadvantage for sample matrix because it indicates possibility of interference. However, XRD method distinguished specific crystalline forms of silica, and the majority of silicate minerals. In addition, XRD method recommend filter dissolution to pretreatment method.

Effect of open Mg sintering ambiance on the in-field critical current density of ex-situ MgB2

  • Sinha, Bhavesh B.;Jang, S.H.;Chung, Kookchae
    • Progress in Superconductivity and Cryogenics
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    • v.14 no.4
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    • pp.12-15
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    • 2012
  • $MgB_2$ superconductor is highly sensitive to the Mg content. Even if the samples are synthesized with the appropriate looking stoichiometric ratio, the heat treatment leads to the loss of Mg either to ambiance or to MgO. To avoid it, either excess Mg is added in the starting powder or sealed ampoule annealing is employed. In this paper the effect of open Mg sintering ambiance on the ex-situ $MgB_2$ was studied to enhance its superconducting properties. The open Mg ambiance was created to avoid any overpressure of Mg by providing a hole in Fe tube used as sample holder. The decrease in resistivity of the synthesized sample was observed through the increased temperature dependence of electron-phonon interactions. A clear enhancement in the superconducting cross-sectional area and hence the in-field critical current density is obtained.

Effect of quaternary ammonium compounds on microbial contamination levels in dental clinics (치과 진료실의 미생물 오염도에 대한 4차 암모늄 화합물의 효과)

  • Baik, Sae Yun;Park, YounJung;Choi, Seung Ho;Kim, Hee Jae;Kim, Seong Taek
    • Journal of Dental Rehabilitation and Applied Science
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    • v.36 no.1
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    • pp.55-60
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    • 2020
  • The aim of this study was to investigate the change of microbial contamination levels in the different areas and at the different time points after application of a quaternary ammonium compound (QAC) that has mechanical antimicrobial effect. The microbial contamination levels were measured in three different areas; unit chair handle, spit sink area and hand piece holder at different time points using adenosine triphosphate (ATP) monitoring system and ATP surface test kit. Hand piece holder showed the highest level of microbial contamination. In most of the clinics, QAC significantly reduced the levels of microbial contamination, and maintained antimicrobial activity for 4 to 6 months. QAC may be used effectively in dental clinics due to the duration of antimicrobial effect and the minimal exposure of chemicals and further studies are needed with large sample size.

Suspended Particulate Concentration at the Drilling Site of Underground Coal Mines in Taebaek Area (태백지역 석탄광업 굴진부서의 부유분진 농도)

  • 윤영노;김영식;이영신
    • Journal of Environmental Health Sciences
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    • v.17 no.1
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    • pp.32-38
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    • 1991
  • Airborne suspended particulate concentration in drilling sites of underground coal mines in Taebaek area was evaluated. And respirable coal dust exposure level was evaluated. Airborne suspended particulate mass include total suspended particle(TSP) and thoracic particle(TPM). TSP (by open-face filter holder) and TPM(by elutriator) concentration were determined by low volume air samplers. Personal air samplers were attached to the coal workers including drillers, coal cutters, and their assistants. Normality and log-normality of TSP, TPM, and respirable dust(RPM) concentration were tested by Kolmogorov-Smirnov one-sample test. Differences of means of TSP, TPM, and RPM concentration were tested by paired t-test. Relation between TSP, TPM, and RPM with pairs were tested by regression test and Pearson's correlation.

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Complex Permittivity Extraction of Blood Glucose at Microwave Frequency

  • Jeong, You-Chul;Lee, Hee-seok;Kim, Joung-ho
    • Journal of electromagnetic engineering and science
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    • v.1 no.2
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    • pp.139-145
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    • 2001
  • In this paper, a coaxial sample holder is proposed with its de-embedding and parameter extraction procedure. The S-parameters were measured up to 1 GHz using network analyzer, HP8753D, and N-type connector together with the de-embedding of N-type connector. The proposed de-embedding procedure is performed to extract electrical parameters of blood glucose, which gives the permittivity of blood glucose. We also analyzed the error of extracted parameters, which are caused by instrument error and geometrical error. Using these error analyses, we reduced the error factors of extracted parameters. We extracted electrical parameters of glucose samples through these all extraction procedure and confirmed the possibility of glucose diagnosis system based on microwave system.

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16 Channel Strain Gauge Measuring Ubiquitous System Development (유비쿼터스 지향의 16채널 스트레인 게이지 계측 시스템 개발)

  • Jang, Soon-Suk;Kim, Kyung-Suk;Won, Yong-Ill;Kim, Dae-Gon
    • Journal of Institute of Control, Robotics and Systems
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    • v.12 no.9
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    • pp.912-917
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    • 2006
  • A strain gauge weight measuring instrumentation system was designed with RF sensor network facilities. In the sensor module system data conversion and a series of signal processing were totally equipped. 16 strain gauges are incoming sensors and each output of the strain gauge was amplified and filtered for proper analog signal processing. Several measuring instrumentation OP amps and general purposed OP amps were used. 12 bits A/D converters converted analog signals to digital bits and a PIC microprocessor controlled the 16 channels of strain gauges. RF RS232 modules were used for wireless communication between the PIC microprocessor and an Ethernet host far a remote sensor monitoring system development.