• Title/Summary/Keyword: resonance measurements

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Magnetic Field Standards Using Magnetic Resonance

  • Park, Po Gyu;Kim, Wan-Seop;Joo, Sung Jung;Lee, Hyung Kew
    • Journal of the Korean Magnetic Resonance Society
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    • v.21 no.1
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    • pp.7-12
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    • 2017
  • The nuclear magnetic resonance (NMR) and atomic magnetic resonance (AMR) plays a fundamental role in achieving a high accuracy of magnetic field measurements. Magnetic field unit (T) was realized based on the shielded proton gyromagnetic ratio (${\gamma}^{\prime}_P$), helium-4 gyromagnetic ratio (${\gamma}_{4He}$) and related techniques. The magnetic field standard system has been disseminated by the NMR magnetometer and electromagnet, a Helmholtz coil system, and AMR magnetometer in the nonmagnetic laboratory. A magnetic field standard below 1 mT has been developed by using Cs and Cs- $^4He$ AMR with automatic compensation of an external magnetic field noise. The standards serve for the calibration of magnetometers and support the test of sensors and materials in the range from $5{\mu}T$ to 2.0 T with (1 to 50) ${\mu}T/T$ uncertainty (k=2).

$^{11}B$ Nuclear Magnetic Resonance Study of Calcium-hexaborides

  • Mean, B.J.;Lee, K.H.;Kang, K.H.;Lee, Moo-Hee;Lee, J.S.;Cho, B.K.
    • Journal of the Korean Magnetic Resonance Society
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    • v.7 no.2
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    • pp.80-88
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    • 2003
  • We have performed $^{11}$ B nuclear magnetic resonance (NMR) measurements to microscopically investigate an electronic structure of the ferromagnetic state in three different compositions of calcium-hexaboride single crystals. Although the crystal structure of Ca $B_{6}$ is cubic and three NMR lines may be expected for the nuclear spin 3/2 of $_{11}$ B, a larger number of NMR resonance peaks have been observed. The frequency and intensity of those peaks distinctively changes depending on the angle between crystalline axis and magnetic field. Analyzing this behavior, we find that the electric field gradient(EFG) tensor at the boron has its principal axis perpendicular to the six cubic faces with a quadrupole resonance frequency $v_{Q}$ 600 kHz. Even though the magnetization data highlight the ferromagnetic hysteresis, $^{11}$ B NMR linewidth data show no clear microscopic evidence of the ferromagnetic state in three different compositions of Ca $B_{6}$ single crystals.s.

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Velocity measurements in complex flows of non-Newtonian fluids

  • Muller, Susan J.
    • Korea-Australia Rheology Journal
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    • v.14 no.3
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    • pp.93-105
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    • 2002
  • Experimental methods for making quantitative measurements of velocity fields in non-Newtonian fluids are reviewed. Techniques based on light scattering spectroscopy - laser Doppler velocimetry and homodyne light scattering spectroscopy, techniques based on imaging the displacement of markers - including particle image velocimetry and molecular tagging velocimetry, and techniques based on nuclear magnetic resonance imaging are discussed. The special advantages and disadvantages of each method are summarized, and their applications to non-Newtonian flows are briefly reviewed. Example data from each technique are also included.

Measurements of Elastic Moduli of Rock Cores Using Free-Free Resonance Tests (자유단 공진시험을 이용한 암석의 탄성계수 측정)

  • 목영진
    • Proceedings of the Earthquake Engineering Society of Korea Conference
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    • 1998.10a
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    • pp.353-360
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    • 1998
  • Dynamic measurements are used rather sparingly to determine the elastic moduli of rock cores and modulus values are not much utilized in design practice. The reason seems to result from the general perception that values obtained by dynamic measurement are much higher (about 10 times) than those determined statically. This paper presents results from dynamic and static tests on rock cores. The findings are : 1) elastic moduli can be consistently determined by laboratory seismic testing. 2) nonlear deformation characteristic of rock cores was tentatively proposed with variation in elastic modulus with strain.

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Comparison between Resonance Frequency and Histomorphometric Measurements of Mandibular Implants in Beagle Dogs (비글견의 하악골에 식립된 임플랜트에 대한 공진주파수와 조직계측분석의 비교 연구)

  • Kim, Woo-Young;Jang, Kyung-Soo;Kim, Chang-Whe;Kim, Yung-Soo
    • Journal of Dental Rehabilitation and Applied Science
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    • v.19 no.4
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    • pp.291-296
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    • 2003
  • The use of resonance frequency analysis (RFA) provides a possibility to clinically measure implant stability and osseointegration. The implant stability quotient (ISQ) value of RFA is well known that influenced by effective abutment length and stiffness of the implant in the surrounding tissues. Among these factors stiffness is not accurately defined histologically yet. And the purpose of this study was to find the histolgical relationship of RFA. 17 implants in 3 beagle dogs were used for this study. Among these implants 10 were survived for 7 months, 4 were survived for 3 months and 3 were immediate status after placement. Resonance frequency analyses were conducted and the dogs were sacrificed. Percentage of the bone to implant contact (BIC) in the interface, percentage of the mineralized bone (bone area) within the threads of the implant, and marginal bone level were measured under light microscopy. The correlation between resonance frequency and histomorphometric measurements were analysed and following results were obtained. 1. There was statistically significant correlation between ISQ value and BIC on healed implants. But ISQ value and BIC of all implants were not significantly correlated. (P<0.01) 2. Significant correlation between ISQ value and bone area was not found in this study. 3. There was statistically significant correlation between ISQ value and marginal bone level on all implants as well as on healed implants. (P<0.01).

Evaluating Paraspinal Back Muscles Using Computed Tomography (CT) and Magnetic Resonance Imaging (MRI): Reliability Analysis and Correlation with Intervertebral Disc Pathology

  • Hwang, Eunjin;Antony, Chermaine Deepa;Choi, Jung-Ah;Kim, Minsu;Khil, Eun Kyoung;Choi, Il
    • Investigative Magnetic Resonance Imaging
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    • v.25 no.2
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    • pp.109-117
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    • 2021
  • Purpose: To investigate the reliability of CT and MRI for quantitative and qualitative analyses of lumbar paraspinal muscle fatty infiltration (PSFI) and correlation of PSFI with intervertebral disc pathology. Materials and Methods: Lumbar spine CT and MRI of 36 subjects were reviewed retrospectively. Two observers independently outlined lumbar paraspinal muscles at each mid-intervertebral disc level. Paraspinal muscles on CT and MRI were graded according to the Goutallier grading system (GGS). The area, mean value, and standard deviation (SD) of the Hounsfield unit (HU) were obtained. Intervertebral discs were assessed on axial image of T2WI at each level. Correlations between qualitative and quantitative data and intervertebral disc pathology, age, and sex were evaluated. Results: Inter- and intra-observer agreements for results of GGS on MRI were substantial (κ = 0.79) and moderate (κ = 0.59), respectively. Inter- and intra-observer agreements for results of GGS on CT were almost perfect (κ = 0.88) and substantial (κ = 0.66), respectively. Quantitative measurements of HU showed almost perfect inter- and intra-observer reliabilities (κ = 0.82 and κ = 0.99, respectively). There were statistically significant correlations between intervertebral disc pathology and PSFI at L1-2, L2-3, and L4-5 levels on MRI and at L1-2 and L3-4 levels on CT. Age showed significant correlation with results of GGS at all levels on CT and MRI. Conclusion: This study showed that GGS results and HU measurements could be useful for evaluating PSFI because they showed correlations with intervertebral disc pathology results at certain levels.

Validation of Magnetic Resonance Velocimetry by Turbulent Pipe Flow (자기공명유속계를 이용한 난류 유동장 가시화)

  • Lee, Jeesoo;Song, Simon;Cho, Jee-Hyun
    • Journal of the Korean Society of Visualization
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    • v.12 no.1
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    • pp.35-42
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    • 2014
  • Magnetic resonance velocimetry (MRV) is a versatile flow visualization technique using magnetic resonance imaging machine developed for the medical purpose. Recently, MRV is often utilized to analyze engineering flows due to its superior features of MRV such as capabilities of measuring flows with complicated, opaque flow geometry unlike optical techniques, 3-dimensional volumetric velocity vectors within a few hours, and etc. The purpose of this study was to validate the MRV data and evaluate the accuracy of the mean velocity profiles that we acquired for a turbulent flow in a circular pipe using a MR machine installed in Korea Basic Science Institute, Ochang, Korea. In addition, we briefly describe a procedure of parameter optimization for the operation of MRV. The results indicate that the MRV measurements provided well resolved mean velocity fields with a quite reasonable accuracy according to the inner and outer layer scaling laws of the turbulent pipe flows.

Triple isotope-[13C, 15N, 2H] labeling and NMR measurements of the inactive, reduced monomer form of Escherichia coli Hsp33

  • Lee, Yoo-Sup;Ko, Hyun-Suk;Ryu, Kyoung-Seok;Jeon, Young-Ho;Won, Hyung-Sik
    • Journal of the Korean Magnetic Resonance Society
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    • v.14 no.2
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    • pp.117-126
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    • 2010
  • Hsp33 is a molecular chaperone achieving a holdase activity upon response to a dual stress by heat and oxidation. Despite several crystal structures available, the activation process is not clearly understood, because the structure inactive Hsp33 as its reduced, zinc-bound, monomeric form has not been solved yet. Thus, we initiated structural investigation of the reduced Hsp33 monomer by NMR. In this study, to overcome the high molecular weight (33 kDa), the protein was triply isotope-[$^{13}C$, $^{15}N$, $^2H$]-labeled and its inactive, monomeric state was ensured. 2D-[$^1H$, $^{15}N$]-TROSY and a series of triple resonance spectra could be successfully obtained on a high-field (900 MHz) NMR machine with a cryoprobe. However, under all of the different conditions tested, the number of resonances observed was significantly less than that expected from the amino acid sequence. Thus, a possible contribution of dynamic conformational exchange leading to a line broadening is suggested that might be important for activation process of Hsp33.

[ $^{11}B$ ] Nuclear Magnetic Resonance Study of Spin Structures in Terbium Tetraboride

  • Mean, B.J.;Kang, K.H.;Kim, J.H.;Hyun, I.N.;Lee, Moo-Hee;Cho, B.K.
    • Journal of the Korean Magnetic Resonance Society
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    • v.10 no.2
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    • pp.197-202
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    • 2006
  • [ $^{11}B$ ] nuclear magnetic resonance (NMR) measurements were performed on the single crystals of $TbB_4$ to investigate local electronic structure and 4f spin dynamics. $^{11}B$ NMR spectrum, Knight shift, spin-lattice and spin-spin relaxation rates were measured down to 4K at 8T. $^{11}B$ NMR shift and linewidth are huge and strongly temperature dependent due to the 4f moments. In addition, both are proportional to magnetic susceptibility, indicating that the hyperfine field at the boron site originates from the 4f spins of Tb. Below $T_N$, the single broad resonance peak of $^{11}B$ NMR splits into several peaks reflecting the local magnetic fields due to antiferromagnetic spin arrangements. The longitudinal and the transverse relaxation rates, $1/T_1\;and\;1/T_2$, independent of temperature above $T_N$, decreases tremendously confirming huge suppression of spin fluctuation below $T_N$.

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Estimation of Sensitivity Enhancements of Material-Dependent Localized Surface Plasmon Resonance Sensor Using Nanowire Patterns (금속물질에 따른 나노구조를 이용한 국소 표면 플라즈몬 공명 센서 특성 분석)

  • Ahn, Heesang;Ahn, Dong-Gyu;Song, Yung Min;Kim, Kyujung
    • Journal of the Korean Society for Precision Engineering
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    • v.33 no.5
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    • pp.363-369
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    • 2016
  • We explored localized plasmonic field enhancements using nanowire patterns to improve the sensitivity of a surface plasmon resonance (SPR) sensor. Two different materials, gold and silver, were considered for sample materials. Gold and silver nanowire patterns were fabricated by electron beam lithography for experimental measurements. The wavelength SPR sensor was also designed for these experiments. The material-dependent field enhancements on nanowire patterns were first calculated based on Maxwell's equations. Resonance wavelength shifts were indicated as changes in the refractive index from 1.33 to 1.36. The SPR sensor with silver nanowire patterns showed a much larger resonance wavelength shift than the sensor with gold nanowire patterns, in good agreement with simulation results. These results suggest that silver nanowire patterns are more efficient than gold nanowire patterns, and could be used for sensitivity enhancements in situations where biocompatibility is not a consideration.