• Title/Summary/Keyword: resin

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Effects of Formaldehyde to Urea Mole Ratio on Thermomechanical Curing of Urea-Formaldehyde Resin Adhesives

  • Park, Byung-Dae;Kim, Jae-Woo
    • Journal of the Korean Wood Science and Technology
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    • v.35 no.5
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    • pp.76-86
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    • 2007
  • This study was conducted to investigate the effects of formaldehyde to urea (F/U) mole ratio on thermomechanical curing of UF resin adhesives with different F/U mole ratios. Thermomechanical curing of these UF resin adhesives was characterized using parameters of dynamic mechanical analysis (DMA) such as the gel temperature, maximum storage modulus, and peak temperatures of storage and loss modulus. As the F/U mole ratio decreased, the gel temperature of UF resin adhesives increased. The maximum storage modulus as an indicator of the rigidity of UF resin adhesives decreased with decreasing F/U mole ratio. The peak temperature of tan $\delta$ increased with decreasing F/U mole ratio, indicating that the vitrification occurred faster for high F/U mole ratio of UF resin adhesives than for the one of lower F/U mole ratio. These results partially explained the reason why UF resin adhesives with lower F/U mole ratio resulted in relatively poor adhesion performance when they were applied.

A study on the Shrinkage Reduction and Strengths of Unsaturated Polyester Mortar (불포화 폴리에스테르 레진 모르타르의 수축저감 및 강도특성에 관한 연구)

  • 최낙운;최길섭;김완기;조영국;소양섭
    • Proceedings of the Korea Concrete Institute Conference
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    • 1999.04a
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    • pp.343-348
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    • 1999
  • The purpose of this study is to evaluated the effects of added expanded polystyrene on the basic properties of UP mortar. Polyester resin mortars are prepared with expanded polystyrene ratio in styrene monomer (EPS/PS), and the ratio of total polystyrene resin to UP resin (PS/UP). And it is tested for viscosity of UP resin added PS resin, slump-flow test, working life, flexural and compressive strengths, and curing shrinkage test. From the test result, Viscosity of resin for polymer mortar increases with increasing PS content. Curing shrinkage of UP mortar is considerably smaller than that of plain UP mortar, nevertheless, reduction in the strengths is not recognized according to adding PS resin. In this study, we can obtain the optimum mix proportions of polymer mortar using PS resin.

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A Study on new Photoinitiator of Visible Light Dental Composite Resin (치과용 가시광선 중합형 복합수지의 새로운 광개시제에 관한 연구)

  • Choi, Yong-Seok;Sun, Gum-Ju
    • Journal of Technologic Dentistry
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    • v.23 no.2
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    • pp.49-59
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    • 2002
  • The photopolymerization efficiency and surface hardness of composite resin containing 1,2-phenylpropanedione (PD) and diacetyl (DA) as photoinitiators were studied by IR and Vickers hardness and the results were compared with that of camphorquinone (CQ). Relative photopolymerization efficiency of the photoinitiators increased in the order of DA < CQ < PD. Vickers hardness of composite resin containing the photoinitiators increased in the order of CQ < PD < DA. Thus, PD is a new visible light photoinitiator for dental composite resin with higher photopolymerization efficiency and surface hardness than that of CQ. Mechanical properties such as Vickers hardness, diametral tensile strength, and flexural strength of the experimental resin composite prepared by addition of the photosensitizer into a resin of bis-GMA improved with increasing the photosensitizer content and irradiation time. The resin composite of bis-GMA containing DA or PD shows better mechanical properties than that of CQ.

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Effect of phenoxy resin content on Properties of Epoxy Bonding Film (Epoxy bonding film의 phenoxy resin 함량에 따른 특성 변화)

  • Kim, Sang-Hyun;Lee, Woo-Sung;Kang, Nam-Kee;Yoo, Myong-Jae
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.228-228
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    • 2008
  • 본 논문에서는 epoxy bonding film의 phenoxy resin의 함량변화에 따른 특성 변화에 대하여 연구하였다. epoxy bonding film은 미세패턴 구현을 위해서 사용되는 기판재료로써 epoxy, hardener, silica, phenoxy resin 등이 첨가되어진다. phenoxy resin 함량을 변화를 주면서 tape casting 방법을 통해서 flim 형성을 한 후, 제작된 film의 phenoxy resin 함량변화에 따른 조도 특성의 연구를 위해서 sweller, desmear 공정을 후 RA(Roughness Average)를 측정하고, SEM으로 표면을 관찰하였다. 또한 제작된 bonding film을 가열 가압 후 구리 도금공정을 거쳐 peel strength를 측정하였다. phenoxy resin 함량이 증가 할수록 RA가 증가되어지는 것이 관찰되어졌고, 또 한 peel strength 증가하였다.

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The Effect of Thermal Decomposition of Epoxy Resin for a Variation of Hardener (에폭시수지의 경화제 변화량에 따르는 열분해 영향)

  • Park, Keun-Ho;Lee, Yong-Sook;Song, Ju-Yeong;Lee, Soo;Kim, Sung-Il
    • Journal of the Korean Applied Science and Technology
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    • v.24 no.4
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    • pp.393-398
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    • 2007
  • We investigated heat stability of epoxy resin products and epoxy resin according to the influence hardener. The heat flow which shows the degree of thermal decomposition of the epoxy resin product and epoxy resin measured by using the differential scanning calorimeter (DSC). As a result, we found that in the case of heat stability for epoxy resin as hardener was added, the ratio of one to one (epoxy resin : hardener) was the most suitable in air condition and nitrogen atmosphere.

A STUDY ON THE CYTOTOXICITY OF THE INCUBATED RESIN SOLUTION (레진 배양액의 세포독성에 관한 연구)

  • Im, Mi-Kyung;Kim, Eun-Chul;Yoo, Soo-Kyung;Kim, Kang-Ju
    • Restorative Dentistry and Endodontics
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    • v.18 no.2
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    • pp.369-376
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    • 1993
  • To know the in vitro and the in vivo cytotoicity of resin solution, resin solution was applied to cultured fibroblast and was injected into the mouse. The cytotoxic effect of resin solution was measured by MIT assay and in vivo cytotoxicity was examined after Hematoxylin and Eosin staining. The cell activity of resin solution in the concentration of 50% was significantly decreased compared to control group and 5 % group. In histopathologic study of resin solution, there were severe inflammatory cell infiltration, mild interstitial edema, trace hemorrhage, and moderate or severe muscle destruction in resin injected group. These results suggested that there might be some differences between the cell viability of fibroblast and in vivo cell cytotoxicity. Further study is needed to clarify the cytotoxicity by direct implanting of resin mass.

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Study on the Thermal Degradation Properties of Epoxy Resin for the Cast Resin Transformer (몰드변압기용 에폭시 수지의 열 열화 특성에 관한 연구)

  • Nam, K.D.;Jung, J.I.;Huh, C.S.
    • Proceedings of the KIEE Conference
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    • 2000.07c
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    • pp.1572-1574
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    • 2000
  • In this paper, study on the properties of the thermal degradated epoxy resin which is used in cast resin transformer is performed to investigate the problems of the decreasing insulation characteristics and crack in the cast resin transformer. In the test, contact angle, weight loss, surface resistivity and relative dielectric constant are measured. As the results of the above measurements, the epoxy resin has increased to 150$^{\circ}C$ in the contact angle and surface resistivity but at the above 150$^{\circ}C$ the values have decreased. The relative dielectric constants have increased in the thermal treated samples with the degradation temperature. Consequently, the insulation properties of the epoxy resin which is used in cast resin transformer have increased by the 150$^{\circ}C$ but decreased in the above 150$^{\circ}C$.

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A Study on the Mechanical Properties of Fabrics Treated with Water Soluble Resin (수용성 수지처리 직물의 물성변화)

  • Kwon, Yoon-Jung;Lee, Mun-Soo
    • Fashion & Textile Research Journal
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    • v.3 no.4
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    • pp.357-361
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    • 2001
  • This paper is concern with the effect of various conditions on mechanical properties of textile fabrics by water soluble resin treatment. Resin treatment of cotton, acetate, viscose rayon, polyester, nylon and acryl fabrics were made by aqueous resin treatment to improve the mechanical properties. The mechanical properties of fabrics, the breaking strength and strain were measured and surface reflectance was measured by color eye. The breaking strength and surface reflectance of fabrics by water soluble resin treatment showed difference by the different treatment concentration. The surface reflectance was increased by water soluble resin treatment. The breaking strength was lower in fabrics with resin treatment than fabrics with none treatment.

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Algorithm for Segmenting Resin Bleed and Melting on the Surface of QFN Packages (QFN 패키지의 Resin Bleed와 Melting 검출 알고리즘)

  • Wang, Ming-Jie;Park, Duck-Chun;Joo, Hyo-Nam;Kim, Joon-Seek
    • Journal of Institute of Control, Robotics and Systems
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    • v.15 no.9
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    • pp.899-905
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    • 2009
  • There are many different types of surface defects on semiconductor Integrated Chips (IC's) caused by various factors during manufacturing process, such as Scratch, Flash, Resin bleed, and Melting. These defects must be detected and classified by an inspection system for productivity improvement and effective process control. Among defects, in particular, Resin bleed and Melting are the most difficult ones to classify accurately. The brightness value and the shape of Resin bleed and Melting defects are so similar that normally it is difficult to classify the Resin bleed and Melting. In this paper, we propose a segmenting method and a set of features for detecting and classifying the Resin bleed and Melting defects.

Development of hybrid resin to reduce silica in borated water

  • Ramzan Akhtar ;Shahid Latif ;Syed Aizaz Ali Shah ;Shaukat Saeed ;Abdul Aziz
    • Nuclear Engineering and Technology
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    • v.55 no.7
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    • pp.2547-2555
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    • 2023
  • Amberlite IRN-78 resin was incorporated with iron to make a hybrid resin for the removal of silica from the borated water of nuclear power plants. The hybrid resin contained 0.84 wt % iron compounds upon pyrolysis. In batch experiments carried out at room temperature, 1 g of the hybrid resin removed ~60 ㎍ silica from 1 ppm borated water in ~120 min. The efficiency of the hybrid material increased with the resin quantity, decreased with silica concentration, and remained unchanged at different pH values. Freundlich and Temkin isothermal adsorption dominated the silica removal process and followed the pseudo-first-order and intra-particle diffusion mechanism simultaneously. The concentration of the leached iron remained appreciably under the safe limits of 200 ㎍/l during the experiments. This detailed study suggests the use of hybrid resin for the removal of silica from borated water streams and other similar systems.