• 제목/요약/키워드: residual phase

검색결과 699건 처리시간 0.026초

The Investigation of Ni Thin Film by Atomic Layer Deposition

  • Do K. W.;Yang C. M.;Kang I. S.;Kim K. M.;Back K. H.;Cho H. I.;Lee H. B.;Kong S. H.;Hahm S. H.;Kwon D. H.;Lee J. H.;Lee J. H.
    • 한국반도체및디스플레이장비학회:학술대회논문집
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    • 한국반도체및디스플레이장비학회 2005년도 추계 학술대회
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    • pp.193-196
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    • 2005
  • Low resistance Ni thin films for using NiSi formation and metallization by atomic layer deposition (ALD) method have been studied. ALD temperature window is formed between $200^{\circ}C\;and\;250^{\circ}C$ with deposition rate of $1.25{\AA}$/cycle. The minimum resistance of deposited Ni films shows $4.333\;{\Omega}/\square$ on the $SiO_2/Si$ substrate by $H_2$ direct purging process. The reason of showing the low resistance is believed to be due to format ion of the $Ni_3C$ phase by residual carbon in Bis-Ni The deposited film exhibits excellent step coverage in the trench having 1(100 nm) : 16 (1.6 um) aspect ratio.

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Distribution of Arsenic Fraction in Soil Around Abandoned Mining Area and Uptake by Rice

  • Kim, Hyuck-Soo;Go, Woo-Ri;Kang, Dae-Won;Yoo, Ji-Hyock;Kim, Kye-Hoon;Kim, Won-Il
    • 한국토양비료학회지
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    • 제48권5호
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    • pp.391-396
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    • 2015
  • Arsenic (As) contamination of agricultural soils resulting from mining activity has caused major concern due to the potential health risk. Therefore the current study was carried out to investigate the relationship between fractionation of As in soil and rice uptake and to provide a basic information for adequate management of As contaminated agricultural soil. Twenty agricultural soils and rice affected by the abandoned mining sites were collected. Soil chemical properties and As concentrations (total and sequential extracted) in soils were determined and As concentrations in polished rice were analyzed. The average concentration of As in non-specifically adsorbed (F1), specifically adsorbed (F2), amorphous hydrous oxides of Fe and Al (F3), crystalline hydrous oxides of Fe and Al (F4) and residual phase (F5) were 0.08, 1.38, 10.34, 3.26 and $10.98mgkg^{-1}$, respectively. Both soil pH and available phosphorus were positively correlated with the concentrations of As in F1 and F2. These results indicate that increasing the soil pH and available phosphorus can significantly increase the easily mobile fractions of As (F1 and F2). The average concentration of As in polished rice was $0.09mgkg^{-1}$. The concentrations of As in F1 and F2 showed a positive correlation with the concentrations of As in polished rice. Therefore soil pH and available phosphorus affect the distribution of As fractionation in soils and thus affect As bioavailability.

정규화된 결합 공간 분할 다중화 기법의 제한된 피드백 환경에서 성능 분석 (Limited Feedback Performance Aanlysis of Regularized Joint Spatial Division and Multiplexing Scheme)

  • 송창익
    • 전기전자학회논문지
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    • 제25권3호
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    • pp.420-424
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    • 2021
  • 5G통신의 핵심 기술인 거대다중안테나 시스템은 송신단에서 많은 양의 채널정보가 필요하기 때문에 제한된 채널 피드백을 사용하는 주파수 분할 이중 시스템에서 구현이 어려운 문제점이 있었다. 이러한 문제점을 해결하기 위해 장시간 변하지 않는 채널 상관도 정보를 이용하여 단말 그룹 간 간섭을 제거함으로써 채널정보 요구량을 비약적으로 감소시키는 Joint Spatial Division and Multiplexing(JSDM)기법이 제안되었고, 최근에는 그룹 간 잔여 간섭을 허용함으로써 성능을 더욱 향상시키는 정규화된 JSDM기법이 제안된 바 있다. 하지만 기존 JSDM관련 연구들은 주로 그룹 간 간섭제거에 초점을 두고 설계되었기 때문에, 그룹내 간섭 제거 단계에서 제한적인 피드백을 가정한 보다 실제적인 환경에서 성능분석이 이루어지지 못하였다. 본 논문에서는 JSDM기법과 정규화된 JSDM기법을 제한된 피드백 환경에서 그룹 수와 그룹 내 사용자 수에 따른 성능을 분석하고 시뮬레이션 결과를 통해 정규화된 JSDM기법이 제한된 피드백 환경에서 기존 JSDM대비 더욱 두드러지는 이득을 보임을 입증한다.

Effects of Surface Machining by a Lathe on Microstructure of Near Surface Layer and Corrosion Behavior of SA182 Grade 304 Stainless Steel in Simulated Primary Water

  • Zhang, Zhiming;Wang, Jianqiu;Han, En-hou;Ke, Wei
    • Corrosion Science and Technology
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    • 제18권1호
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    • pp.1-7
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    • 2019
  • To find proper lathe machining parameters for SA182 Grade 304 stainless steel (SS), six kinds of samples with different machining surface states were prepared using a lathe. Surface morphologies and microstructures of near surface deformed layers on different samples were analysed. Surface morphologies and chemical composition of oxide films formed on different samples in simulated primary water with $100{\mu}g/L\;O_2$ at $310^{\circ}C$ were characterized. Results showed that surface roughness was mainly affected by lathe feed. Surface machining caused grain refinement at the top layer. A severely deformed layer with different thicknesses formed on all samples. In addition to high defect density caused by surface deformation, phase transformation, residual stress, and strain also affected the oxidation behaviour of SA182 Grade 304 SS in the test solution. Machining parameters used for # 4 (feed, 0.15 mm/r; back engagement, 2 mm; cutting speed, 114.86 m/min) and # 6 (feed,0.20 mm/r; back engagement, 1 mm; cutting speed, 73.01 m/min) samples were found to be proper for lathe machining of SA182 Grade 304 SS.

웹 로그 데이터에 대한 개인정보 위협분석 및 보안 가이드 (The Threat Analysis and Security Guide for Private Information in Web Log)

  • 여성구;심미나;이상진
    • 정보보호학회논문지
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    • 제19권6호
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    • pp.135-144
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    • 2009
  • 본 논문은 오늘날 정보사회의 핵심 정보 자원인 개인정보가 웹 로그를 통해 누출될 수 있는 보안 위협의 심각성을 재인식시키고, 이를 근원적으로 예방하기 위한 대응방안을 제시한다. 최근 개인정보는 정보사회의 발전과 함께 범위 및 종류가 확대되고 그 중요성이 매우 커지게 되었다. 웹 로그는 법 제도적으로 규정된 개인정보가 저장되는 개인정보 파일임에도 불구하고, 웹 서비스의 부산물 정도로만 인식되어 충분한 보호조치가 이루어지지 못하고 있다. 웹 로그를 통해 노출될 수 있는 개인정보를 개발 단계에서 통제하여 웹 로그에 개인정보가 저장되는 것을 최소화하고, 운영 단계에서 적용되어야 하는 기술적 대안을 제시한다. 근본적 보호체계를 통해 법 제도적 규제를 준수하고 개인정보를 효과적으로 보호할 수 있다.

선택적 레이저 조형된 AlSi10Mg합금의 후열처리에 따른 Si-rich상 형상변화가 기계적 특성에 미치는 영향 (Influence of Si-rich Phase Morphologies on Mechanical Properties of AlSi10Mg Alloys processed by Selective Laser Melting and Post-Heat Treatment)

  • 남정우;엄영성;김경태;손인준
    • 한국분말재료학회지
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    • 제28권2호
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    • pp.134-142
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    • 2021
  • In this study, AlSi10Mg powders with average diameters of 44 ㎛ are additively manufactured into bulk samples using a selective laser melting (SLM) process. Post-heat treatment to reduce residual stress in the as-synthesized sample is performed at different temperatures. From the results of a tensile test, as the heat-treatment temperature increases from 270 to 320℃, strength decreases while elongation significantly increases up to 13% at 320℃. The microstructures and tensile properties of the two heat-treated samples at 290 and 320℃, respectively, are characterized and compared to those of the as-synthesized samples. Interestingly, the Si-rich phases that network in the as-synthesized state are discontinuously separated, and the size of the particle-shaped Si phases becomes large and spherical as the heat-treatment temperature increases. Due to these morphological changes of Si-rich phases, the reduction in tensile strengths and increase in elongations, respectively, can be obtained by the post-heat treatment process. These results provide fundamental information for the practical applications of AlSi10Mg parts fabricated by SLM.

중저준위 방폐물 처분 사일로 구조물의 구조거동 수치해석 연구 (Numerical Study of Structural Behavior of Underground Silo Structures for Low-and-Intermediate-level Radioactive Waste Disposal Facility)

  • 김선훈;김광진
    • 한국전산구조공학회논문집
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    • 제35권3호
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    • pp.183-190
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    • 2022
  • 경주 방폐물 처분시설의 1단계 시설로 건설된 지하 사일로 구조는 2014년에 10만 드럼 규모로 완공되어 현재 운영중에 있다. 지하 사일로 구조는 지름 25m, 높이 50m로써 방폐물을 저장하는 실린더부분과 돔 부분으로 구성되어 있으며, 돔부분은 운영터널과 연결되는 하부 돔 부분과 상부 돔 부분으로 구분할 수 있다. 지하 사일로 구조의 벽체는 철근콘크리트 라이너이고, 두께는 약 1m이다. 본 논문에서는 지하 사일로 구조의 건설과정 및 운영과정의 단계별 유한요소해석을 수행하였다. SMAP-3D 프로그램을 사용하여 2차원 축대칭 유한요소해석을 수행하였다. 2차원 축대칭 유한요소모델의 신뢰성을 검토하고자 3차원 유한요소해석도 수행하였다. 본 논문에서는 지하 사일로 구조의 구조거동을 분석하고 구조적 안전성을 검토결과를 제시하였다.

Improvement and validation of aerosol models for natural deposition mechanism in reactor containment

  • Jishen Li ;Bin Zhang ;Pengcheng Gao ;Fan Miao ;Jianqiang Shan
    • Nuclear Engineering and Technology
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    • 제55권7호
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    • pp.2628-2641
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    • 2023
  • Nuclear safety is the lifeline for the development and application of nuclear energy. In severe accidents of pressurized water reactor (PWR), aerosols, as the main carrier of fission products, are suspended in the containment vessel, posing a potential threat of radioactive contamination caused by leakage into the environment. The gas-phase aerosols suspended in the containment will settle onto the wall or sump water through the natural deposition mechanism, thereby reducing atmospheric radioactivity. Aiming at the low accuracy of the aerosol model in the ISAA code, this paper improves the natural deposition model of aerosol in the containment. The aerosol dynamic shape factor was introduced to correct the natural deposition rate of non-spherical aerosols. Moreover, the gravity, Brownian diffusion, thermophoresis and diffusiophoresis deposition models were improved. In addition, ABCOVE, AHMED and LACE experiments were selected to validate and evaluate the improved ISAA code. According to the calculation results, the improved model can more accurately simulate the peak aerosol mass and respond to the influence of the containment pressure and temperature on the natural deposition rate of aerosols. At the same time, it can significantly improve the calculation accuracy of the residual mass of aerosols in the containment. The performance of improved ISAA can meet the requirements for analyzing the natural deposition behavior of aerosol in containment of advanced PWRs in severe accident. In the future, further optimization will be made to address the problems found in the current aerosol model.

염화물 환경에서 스테인리스강 용접부의 공식저항성 향상을 위한 마찰교반공정 적용효과에 관한 연구 (A study on the Application Effect of Friction Stir Processing for Enhanced Pitting Corrosion Resistance of Stainless Steel Welds in Chloride Environment)

  • 하종문;심덕남;김승현
    • 한국압력기기공학회 논문집
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    • 제19권2호
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    • pp.84-92
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    • 2023
  • As temporary storage facilities for spent nuclear fuels in domestic nuclear power plants are expected to be saturated, external intermediate storage facilities would be required in the future. Spent nuclear fuels are stored in metal canisters and then placed in a dry environment within concrete or metal casing for operation. In the United States, the dry storage method for spent nuclear fuels has been operated for an extended period. Based on the corrosion experiences of dry storage canisters in chloride environments, numerous studies have been conducted to reduce corrosion in welds. With the construction of intermediate storage facilities in Korea for spent nuclear fuels expected near coastal areas adjacent to nuclear power plants, there is a need for research on the corrosion occurrence of welds and mitigation methods for canisters in chloride environments. In this paper, we measured and compared the residual stresses in the Heat-Affected Zones (HAZ) after electron beam welding (EBW) and gas tungsten arc welding (GTAW) processes for candidate materials such as 304L, 316L, and duplex stainless steel(DSS). We investigated the possibility of microstructure control through the application of surface modification processes using friction stir processing (FSP). Corrosion tests on each welded specimen revealed a higher corrosion rate in EBW welds compared to GTAW. Furthermore, it was confirmed that corrosion resistance improved due to phase refinement and redistribution of precipitates when FSP was applied.

Experimental and numerical investigation on the seismic behavior of the sector lead rubber damper

  • Xin Xu;Yun Zhou;Zhang Yan Chen;Song Wang;Ke Jiang
    • Earthquakes and Structures
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    • 제26권3호
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    • pp.203-218
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    • 2024
  • Beam-column joints in the frame structure are at high risk of brittle shear failure which would lead to significant residual deformation and even the collapse of the structure during an earthquake. In order to improve the damage issue and enhance the recoverability of the beam-column joints, a sector lead rubber damper (SLRD) has been developed. The SLRD can increase the bearing capacity and energy dissipation capacity, and also demonstrating recoverability of seismic performance following cyclic loading. In this paper, the hysteretic behavior of SLRD was experimentally investigated in terms of the regular hysteretic behavior, large deformation behavior and fatigue behavior. Furthermore, a parametric analysis was performed to study the influence of the primary design parameters on the hysteretic behavior of SLRD. The results show that SLRD resist the exerted loading through the shear capacity of both rubber parts coupled with the lead cores in the pre-yielding stage of lead cores. In the post-yielding phase, it is only the rubber parts of the SLRD that provide the shear capacity while the lead cores primarily dissipate the energy through shear deformation. The SLRD possesses a robust capacity for large deformation and can sustain hysteretic behavior when subjected to a loading rotation angle of 1/7 (equivalent to 200% shear strain of the rubber component). Furthermore, it demonstrates excellent fatigue resistance, with a degradation of critical behavior indices by no more than 15% in comparison to initial values even after 30 cycles. As for the designing practice of SLRD, it is recommended to adopt the double lead core scheme, along with a rubber material having the lowest possible shear modulus while meeting the desired bearing capacity and a thickness ratio of 0.4 to 0.5 for the thin steel plate.