• Title/Summary/Keyword: refinement-recovery

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Improvement of Mechanical and Corrosion Properties of Mg-Ca-Zn Alloy by Grain Refinement (Grain Refinement를 통한 Mg-Ca-Zn합금의 기계적 특성 및 부식 특성 향상)

  • Kim, Dae-Han;Choi, Jong-Min;Lim, Hyun-Kyu
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.9
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    • pp.418-424
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    • 2017
  • Magnesium has a higher specific strength than other metals and is widely used industry wide due to its excellent vibration absorption ability and electromagnetic wave shielding property.For example, it is used for automobile parts such as car seat frames and cylinder heads, and is widely used in electronic products such as notebook cases and mobile phone cases. In addition, it is in the spotlight as a bone-implant material used to assist in the treatment of damaged bones when the bones are cracked or broken. Currently, Ti alloy, stainless steel and Co-Cr-Mo alloy are used as the implant material, and the Mg alloy remains in research stage. The current problem with bone implant implants is that the patients must undergo reoperation to remove the implants after joint surgery. Magnesium, however, can achieve sufficient strength compared to current materials. In addition, since it is self-decomposed after the recovery, reoperation is not necessary. In this paper, Mg alloys were designed by adding harmless Ca and Zn to the human body. In order to improve the strength and corrosion resistance, the final alloy was designed by adding a small amount of Sr as a grain refiner. The radioactive elements of Sr are harmful to the human body, but other naturally occurring Sr elements are harmless. Microstructure analysis of the alloys was performed by optical microscopy and scanning electron microscopy. The mechanical properties and corrosion characteristics were evaluated by tensile test, potentiodynamic test and immersion test.

Application of Ordinary Kriging Interpolation Method for p-Adaptive Finite Element Analysis of 2-D Cracked Plates (2차원 균열판의 p-적응적 유한요소해석을 위한 정규크리깅 보간법의 적용)

  • Woo, Kwang-Sung;Jo, Jun-Hyung;Park, Mi-Young
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.19 no.4 s.74
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    • pp.429-440
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    • 2006
  • This paper comprises two specific objectives. The first is to examine the applicability of ordinary kriging interpolation(OK) to the p-adaptivity of the finite element method that is based on variogram modeling. The second objective Is to present the adaptive procedure by the hierarchical p-refinement in conjunction with a posteriori error estimator using the modified S.P.R. (superconvergent patch recovery) method. The ordinary kriging method that is one of weighted interpolation techniques is applied to obtain the estimated exact solution from the stress data at the Gauss points. The weight factor is determined by experimental and theoretical variograms for interpolation of stress data apart from the conventional interpolation methods that use an equal weight factor. In the p-refinement, the analytical domain has to be refined automatically to obtain an acceptable level of accuracy by increasing the p-level non-uniformly or selectively. To verify the performance of the modified S.P.R. method, the new error estimator based on limit value has been proposed. The validity of the proposed approach has been tested with the help of some benchmark problems of linear elastic fracture mechanics such as a centrally cracked panel, a single edged crack, and a double edged crack.

Refinement of Low Resolution DEM Using Differential Interferometry

  • Kim Chang-Oh;Lee Dong-Cheon;Kim Jeong-Woo;Kim Sang-Wan;Won Joong-Sun
    • Proceedings of the KSRS Conference
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    • 2004.10a
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    • pp.522-525
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    • 2004
  • Interferometry SAR (InSAR) is a technique to generate topographic map from complex data pairs observed by antennas at different locations. However, to obtain topographic information using InSAR is difficult task because it requires series of complicated process including phase unwrapping and precise recovery of the SAR geometry. Especially, accuracy of the DEM (Digital Elevation Model) produced by repeat pass single SAR pair could be influenced by atmospheric effect. Recently, a new InSAR technique to improve accuracy of DEM has been introduced that utilizes low resolution DEM with a number of SAR image pairs. The coarse DEM plays an important role in reducing phase unwrapping error caused by layover and satellite orbit error. In this study, we implemented DInSAR (Differential InSAR) method which combines low resolution DEMs and ERS tandem pair images. GTOPO30 DEM with 1km resolution, SRTM-3 DEM with 100m resolution, and DEM with 10m resolution derived from 1:25,000 digital vector map were used to investigate feasibility of DInSAR. The accuracy of the DEMs generated both by InSAR and DInSAR was evaluated.

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Adaptive Crack Propagation Analysis with the Element-free Galerkin Method (Element-free Galerkin 방법을 이용한 적응적 균열진전해석)

  • 최창근;이계희;정흥진
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.13 no.4
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    • pp.485-500
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    • 2000
  • In this paper the adaptive crack propagation analysis based on the estimated local and global error in the element-free Galerkin (EFG) method is presented. It is possible to keep consistency and accuracy of analysis in each propagation step by adaptive analysis. The adaptivity analysis in crack propagation is achieved by adding and removing the node along the background integration cell that are refined or recovered as estimated error. These errors are obtained by calculating the difference between the values of the projected stresses and original EFG stresses. To evaluate the performance of proposed adaptive procedure, the convergence behavior is investigated lot several examples. The results of these examples show the efficiency of proposed scheme in crack propagation analysis.

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Development of Reuse Process Through Recovery and Refinement of Precursor for LED (LED용 precursor 재이용을 위한 회수 및 정제 공정 개발)

  • Yang, Jae Yeol;O, Byung Sung;Yoon, Jae Sik
    • Resources Recycling
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    • v.23 no.1
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    • pp.25-32
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    • 2014
  • The purpose of this research is to develop a process and a system to collect, purify and reuse the residual quantity of trimethylgallium, used as a raw material, upon GaN epitaxial growth for LED from a metal organic chemical vapor deposition(MOCVD) equipment. This research reviews whether TMGa collected from the process can be used through a chemical and structural characteristics evaluation. As a result of analyzing the purity using ICP-MS and ICP-AES, 7N high purity (99.99999%) of TMGa was obtained. According to checking the structural change of TMGa through NMR analysis, TMGa having pure $(CH_3)_3Ga$ structure was obtained without structural change. For reliability review of the collected TMGa, u-GaN was deposited using the MOCVD process and an structural, optical and electrical characteristics evaluation was conducted. As a result, it was found out that the reuse was possible.

Refinement of GRACE Gravity Model Including Earth's Mean Mass Variations (지구 평균 질량 변화를 포함한 GRACE 중력 모델 보정)

  • Seo, Ki-Weon;Eom, Jooyoung;Kwon, Byung-Doo
    • Journal of the Korean earth science society
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    • v.35 no.7
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    • pp.537-542
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    • 2014
  • The Gravity Recovery and Climate Experiment (GRACE) has observed the Earth's mass redistribution mainly caused by the variations of groundwater, ice sheet, and sea level since its launch in April 2002. The global gravity model estimated by the GRACE observation is corrected by barometric pressure, and thus represents the change of Earth mass on the Earth's surface and below Earth's surface excluding air mass. However, the total air mass varies due to the water exchange between the Earth's surface and the atmosphere. As a result, the nominal GRACE gravity model should include the Earth's gravity spectrum associated with the total air mass variations, degree 0 and order 0 coefficients of spherical harmonics ($C_{00}$). Because the water vapor content varies mainly on a seasonal time scale, a change of $C_{00}$ (${\delta}C_{00}$) is particularly important to seasonal variations of sea level, and mass balance between northern and southern hemisphere. This result implies that ${\delta}C_{00}$ coefficients should be accounted for the examination of continental scale mass change possibly associated with the climate variations.

A study on the relationship between women's health status and the experience of Sanhujori, the Korean traditional non-professional postpartal care. (여성의 건강상태와 산후조리 경험과의 관계 연구)

  • Yu, Eun-Gwang
    • The Korean Nurse
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    • v.36 no.5
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    • pp.74-90
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    • 1998
  • This descriptive study sought to define the relationship between women's health status and the experience of Sanhujori, Korean traditional non-professional postpartal care after delivery and abortion. A convenience sample of 308 women in 7 provinces in Korea including Seoul were studied from December, 1994 to December, 1996 for two years. Mean age of respondents was 50.5 years and mean number of children was 3. The rate of abortion was 91.5% and mean frequency was 2.2 times per woman. 82% of respondents did not have Sanhujori after abortion. The period and subjective evaluation of experience of Sanhujori after delivery were decreased according to the increment of the number of childbirth. The health status implies both subjective health status women perceived and physical symptom distress women are experiencing presently, The respondents expressed the physical symptom distress as painful one. 56.7% of respondents perceived unhealthy, such as sick and 99.6% complained more than one symptom. The factors related to health status were the first and third experience of Sanhujori after delivery, such as the period and subjective evaluation whether she did Sanhujori well or not; whether or not of Sanhujori after abortion and menopause: the number of child: and age. at the level of 1% or 5% of significance statistically. The factors related to the rate of physical sumptom distress were only two: the first experience of Sanhujori after delivery, especially the subjective evaluation and whether women did Sanhujori after abortion or not. at the level of 1% or 5% of significance statistically. In conclusion. this finding reconfirmed the possible relationship between women's health status and the experience of Sanhujori after delivery & abortion. It provides a challenge to the professional care givers .to research further on the effects of Sanhujori on the health status. health recovery after abortion or delivery from the various aspects through the cross-sectional and longitudinal research for the refinement of the reality of Sanhujori not only as cultural phenomenon but as conceptual model for the appropriateness of intervention and qualty of care for desirable health outcomes. Besides, it is indispensable to refine and reestablish postpartal caring system by finding universal law through international & cross-cultural research on postpartal traditional care for women's life long health toward the 21C

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Dental Co-Cr alloys fabricated by selective laser melting: A review article (선택적 레이저 용융 방법으로 제작한 치과용 코발트 크롬 합금에 대한 문헌고찰)

  • Kang, Hyeon-Goo
    • The Journal of Korean Academy of Prosthodontics
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    • v.59 no.2
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    • pp.248-260
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    • 2021
  • Cobalt-chromium alloys are used to fabricate various dental prostheses, and have advantages of low cost and excellent mechanical properties compared to other alloys. Recently, selective laser melting, which is an additive manufacturing method, has been used to overcome the disadvantages of the conventional fabrication method. A local rapid heating and cooling process of selective laser melting induces fine microstructures, grain refinement, and reduction of porosities of the alloys. Therefore, it can improve mechanical properties compared to the alloys fabricated by the conventional method. On the other hand, layering process and rapid heating and cooling cause accumulation of a large amount of residual stresses that can adversely affect the mechanical properties. A heat treatment for removing residual stresses through recovery and recrystallization process caused complicated changes in mechanical properties induced by phase transformation, precipitate and homogenization of the microstructures. The purpose of this review was to compare the manufacturing methods of Co-Cr alloys and to investigate the characteristics of Co-Cr alloys fabricated by selective laser melting.

Microstructural Changes of OFC according to the Processing Number of Multi-Axial Diagonal Forging (MADF) (다축대각단조(MADF) 가공횟수에 따른 OFC의 미세조직 변화)

  • Kim, S.T.;Kwon, S.C.;Kim, D.V.;Lee, S.;Choi, S.H.;Jeong, H.T.
    • Transactions of Materials Processing
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    • v.27 no.6
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    • pp.347-355
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    • 2018
  • This study investigated the effects of the processing number of multi-axial diagonal forging (MADF) on the microstructural changes of OFC fabricated by MADF processes. The as-extruded OFC was cut to $25mm^3$ cube for the MADF processes. The MADF process consists of plane forging with a thickness reduction of 30% and diagonal forging with a diagonal forging angle of $135^{\circ}$. In order to analyze the microstructural evolutions according to the number of repetitions, 1, 2, 3 and 4 cycles of the MADF process were performed. OFC specimens were successfully deformed without surface cracking for up to 4 cycles of MADF. The grain size, average misorientation and average grain orientation spread (GOS) of MADF processed materials were analyzed using EBSD technique and their Vicker's hardness were also measured. The results showed that MADF process effectively refined the microstructure of OFC with initial average grain size of $84.2{\mu}m$. The average grain sizes of specimens MADF processed for 1, 2, 3, 4 cycles were refined to be $8.5{\mu}m$, $2.2{\mu}m$, $1.5{\mu}m$, $1.1{\mu}m$, respectively. The grain refinement seemed to be saturated when OFC was MADF processed over 2 cycles. In the case of specimens subjected to two or more cycles of MADF, the degree of decrease in average grain size was drastically reduced as the number of cycles increased due to softening phenomena such as dynamic recovery or dynamic recrystallization during processing. The degree of increase in average Vicker's hardness was also dramatically reduced as the number of cycles increased due to the same reason.

Microstructural Changes of AA1100 According to the Processing Number of Multi-Axial Diagonal Forging (MADF) (다축대각단조(MADF) 가공횟수에 따른 AA1100의 미세조직 변화)

  • Kwon, S.C.;Kim, S.T.;Kim, D.V.;Kim, M.S.;Lee, S.;Choi, S.H.;Jeong, H.T.
    • Transactions of Materials Processing
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    • v.28 no.2
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    • pp.63-70
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    • 2019
  • This study investigates the effects of multi-axial diagonal forging (MADF) processing number on the microstructures of AA1100 fabricated using MADF processes. The cast AA1100 was annealed at $400^{\circ}C$ for 3hrs in $N_2$ atmosphere and cut into $25mm^3$ cubes for the MADF processes. The MADF process consist of plane forging with a thickness reduction of 30% and a diagonal forging with a diagonal forging angle of 135 degrees. In order to analyze the microstructural variations based on the number of repetitions, 1, 2, 3 and 4 cycles of the MADF process were performed. AA1100 specimens were successfully deformed without cracking of the surface for up to 4 cycles of MADF. The grain size, average misorientation and average grain orientation spread (GOS) of MADF processed materials were analyzed using EBSD technique. The results showed that MADF process effectively refined the microstructure of AA1100 with an initial average grain size of $337.4{\mu}m$. The average grain sizes of specimens which were MADF processed for 2, 3, 4 cycles were refined to be $1.9{\mu}m$, $1.6{\mu}m$, $1.4{\mu}m$, respectively. The grain refinement appeared saturated when AA1100 got MADF processed over 2 cycles. When the specimen was subjected to two or more cycles of MADF, the degree of decrease in the average grain size drastically decreased with an increase in the number of cycle due to the softening phenomena such as dynamic recovery or dynamic recrystallization during processing.