• Korean Chemical Engineering Research
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• v.61 no.1
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• pp.39-44
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• 2023

In this study, the particle size of Si polycrystals was controlled through wet-sedimentation method, and changes in the capacity and cyclic characteristics of the Si anode material according to the particle size were observed. After wet-sedimentation of Si particles pulverized by a vibration mill, the non-uniform particle distribution of Si was uniformly controlled. The d₅₀ of a sample in which Si was sedimented for 24 hours decreased to 0.50 ㎛. As a result of the electrochemical characteristic analysis, the Rct value representing the resistance in the electrode was significantly reduced due to the decrease in particle size. The unclassified Si sample exhibited a discharge capacity of 2,869 mAh/g in the first cycle, and decreased to 85.7 mAh/g after 100 cycles. The sample in which Si was classified for 24 hours showed a capacity of 3,394 mAh/g initially, and maintained a capacity of 1,726 mAh/g after 100 cycles. As the size of the Si particles decreased, the discharge capacity increased and the cycle life was also increased.

• International Journal of Reliability and Applications
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• v.12 no.1
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• pp.61-77
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• 2011

One of the most important problems in the estimation of the parameter of the failure model, is the cost of experimental sampling units, which can be reduced by using any prior information available about ${\theta}$, and devising a two-stage pooling shrunken estimation procedure. We have proposed an estimator of the reliability function (R(t)) of the exponential model using two-stage time censored data when a prior value about the unknown parameter (${\theta}$) is available from the past. To compare the performance of the proposed estimator with the classical estimator, computer intensive calculations for bias, mean squared error, relative efficiency, expected sample size and percentage of the overall sample size saved expressions, were done for varying the constants involved in the proposed estimator (${\tilde{R}}$(t)).

• Textile Coloration and Finishing
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• v.11 no.6
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• pp.1-6
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• 1999

The porosities of PET fibers were investigated using a nitrogen porosimeter according to oxygen plasma treatment and dyeing with a disperse dye, and they were discussed in terms of the change of internal micro-structure of the PET fiber. The total pore volume, surface area and average pore size of the plasma treated PET fibers increased expectably compared with the untreated sample. The PET fibers treated with oxygen plasma and then dyed with a disperse dye were increased significantly in the surface area and the total pore volume comparing with those of plasma treated only, but decreased in the average pore size. The increase of the surface area, after dyeing, of the plasma treated PET fibers was due to addition of the surface area of the dye itself to that of the PET fiber. The increase of the total pore volume of the plasma treated PET fibers by dyeing, which is the opposite result to the general idea that the pore volume of fibers would be reduced by occupation of dye molecules in the pores, could be explained by the free-volume model. This is that the amorphous region in the fiber expanded by occupation of dye molecules, and the marginal space surrounding dyes was generated as many smaller pores, and the decrease of the average pore size of the dyed sample also could be explained The decrease of the average pore size was caused by the splitting of a larger pore into smaller pores.

• Advanced Composite Materials
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• v.16 no.3
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• pp.245-258
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• 2007

The single-modal Weibull model has been assessed on Tyranno ZMI Si-Zr-C-O fiber if a set of shape and scale parameters accurately reproduced the effect of the size of the diameter on strength. The tensile data of a single fiber have been divided into two expedient groups as 'small diameter' group and 'large diameter' group in deriving the parameters, which should be consistent if the Weibull model accurately reproduced the size effect. However, the derived Weibull parameters were inconsistent between the two groups. Thereby the authors have concluded that the parameters of the single-modal Weibull model are dependent on the fiber diameter, so that the model is inadequate to reproduce the strength size effect. On the other hand, Weibull parameters were found consistent between the two groups by excluding the data of 'large mirror zone' sample, which was defined as the sample around 10% mirror zone area of the fracture surface. What is more, the exclusion reduced the strength variance more drastically in the 'large diameter' group than in the 'small diameter' group, even though the 'large mirror zone' samples were found identical in the percentage between the two groups. The authors therefore conclude that diameter limitation to the 'small diameter' group level can lead to drastically less distributed strength values than the estimated strength through the Weibull scaling on the present Tyranno ZMI Si-Zr-C-O fiber.

• Proceedings of the Korean Vacuum Society Conference
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• 2010.02a
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• pp.390-390
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• 2010

Superconducting proximity effects of Nb/Si(111) were investigated with scanning tunneling microscopy(STM) and scanning tunneling spectroscopy(STS). A highly-doped($0.002\;{\omega}{\diamondsuit}cm$) Si wafer pieces were used as substrate and Nb source was thermally evaporated onto the atomically clean silicon substrate. The temperature of the silicon sample was held at $600^{\circ}C$ during the niobium deposition. And the sample was annealed at $600^{\circ}C$ for 30 minutes additionally. Volmer-Weber growth mode is preferred in Nb/Si(111) at the sample temperature of $600^{\circ}C$. With proper temperature and annealing time, we can obtain Nb islands of lateral size larger than Nb coherence length(~38nm). And outside of the islands, bare Si($7{\times}7$) reconstructed surface is exposed due to the Volmer-Weber Growth mode. STS measurement at 5.6K showed that Nb island have BCS-like superconducting gap of about 2mV around the Fermi level and the critical temperature is calculated to be as low as 6.1K, which is lower than that of bulk niobium, 9.5K. This reduced value of superconducting energy gap indicates suppression of superconductivity in nanostructures. Moreover, the superconducting state is extended out of the Nb island, over to bare Si surface, due to the superconducting proximity effect. Spatially-resolved scanning tunneling spectroscopy(SR-STS) data taken over the inside and outside of the niobium island shows gradually reduced superconducting gap.

• Journal of the Korean Institute of Telematics and Electronics A
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• v.32A no.3
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• pp.471-481
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• 1995

Measurement factors for the dielectric properties of low dielectric loss materials (tan${\dalta}{\le}10^{-4}$) were investigated using the dielectric rod resonator method. It was shown that the relative conductivity (${\sigma}_{r}$) should be controlled within a 5% to obtain the standard deviations of less than 0.07 for permittivity .epsilon.r and 0.06${\times}10^{-4}$ for tan.delta.respectively. Surface resistivity (R$_s$) could be reduced when the surface roughness of parallelled conducting plate was less than 0.07 .mu.m. Measurement error for the permittivity was $\pm$0.02% independent of probe loop size, whereas the error in Q value was reduced with the decrease in probe loop size and also with the increase in the absolute values of Q. Reliable Q values were determined with the probe loop size of less than 4mm. The accurate for the distance between the measuring probe loop and the sample could be obtained when the insertion loss of resonant frequency ranged -15dB - -30dB.

• Proceedings of the IEEK Conference
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• 2006.06a
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• pp.263-264
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• 2006

In this paper, an efficient and fast algorithm to reduce calculation amount of FIR(Finite Impulse Responses) filtering is proposed. Proposed algorithm enables arbitrary size of parallel processing, and their structures are also easily derived. Furthermore, it is shown that the number of multiplication/sample is reduced, and number of instructions using MAC(Multiplication and Accumulation) processor are also reduced. For theoretical improvement, numbers of sub filters are compared with those of conventional algorithm. In addition to the theoretical improvement, it is shown that number of element for hardwired implementation are reduced comparison to those of the conventional algorithm.

• Journal of Applied Reliability
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• v.5 no.1
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• pp.167-180
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• 2005

Design of a degradation test without replacement is considered based on tightened critical value to reduce the evaluation testing time. The sample size, number of inspections, and the critical values are determined to assure the same probability of acceptance when the testing time is reduced to some degree. Photo-diode balance of an optical pickup is analyzed as a case study.

• Journal of Korea Society of Industrial Information Systems
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• v.23 no.2
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• pp.19-28
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• 2018

In this paper, we studied on the sampling of ocean meteorological data to analyze signature of naval ships. The newest ocean meteorological data, that was quality controled by the Korea Meteorological Administration(KMA), was collected. Outliers were removed from the data by setting the usable range of data. After that, the data size was reduced through the random sampling method, taking geopolitical significance and effective area of buoy, for probabilistic analysis. Moreover, the sample sizes were set at 100, 200, and 400 by considering the population size and a 95% confidence level. The final sample was obtained using the two-dimensional stratified sampling method based on highly correlated water temperature and air temperature. The sum of the squared errors and the confidence interval was calculated to compare the result of sampling. As a result, this study proposed reasonable sample size for infra­red signature analysis of naval ships.

• Journal of Internet Computing and Services
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• v.17 no.1
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• pp.1-6
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• 2016

The biased zero-error probability and its related algorithms require heavy computational burden related with some summation operations at each iteration time. In this paper, a recursive approach to the biased zero-error probability and related algorithms are proposed, and compared in the simulation environment of shallow water communication channels with ambient noise of biased Gaussian and impulsive noise. The proposed recursive method has significantly reduced computational burden regardless of sample size, contrast to the original MBZEP algorithm with computational complexity proportional to sample size. With this computational efficiency the proposed algorithm, compared with the block-processing method, shows the equivalent robustness to multipath fading, biased Gaussian and impulsive noise.