• Title/Summary/Keyword: reactive extraction

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Inhibition of Reactive Oxygen Species (ROS) and Nitric Oxide (NO) by Gelidium elegans Using Alternative Drying and Extraction Conditions in 3T3-L1 and RAW 264.7 Cells

  • Jeon, Hui-Jeon;Choi, Hyeon-Son;Lee, OK-Hwan;Jeon, You-Jin;Lee, Boo-Yong
    • Preventive Nutrition and Food Science
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    • v.17 no.2
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    • pp.122-128
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    • 2012
  • Gelidium (G.) elegans is a red alga inhabiting intertidal areas of North East Asia. We examined anti-oxidative and anti-inflammatory effects of G. elegans, depending on drying and extraction conditions, by determining reactive oxygen species (ROS) and nitric oxide (NO) in 3T3-L1 and RAW 264.7 cells. Extraction yields of samples using hot air drying (HD) and far-infrared ray drying (FID) were significantly higher than those using natural air drying (ND). The 70% ethanol extracts showed the highest total phenol and flavonoid contents compared to other extracts (0, 30, and 50% ethanol) under tested drying conditions. The scavenging activity on 2,2-diphenyl- 1-picrylhydrazyl (DPPH) and nitrite correlated with total phenol or flavonoid content in the extracts. The greatest DPPH scavenging effect was observed in 70% ethanol extract from FID and HD conditions. The production of ROS and NO in 3T3-L1 and macrophage cells greatly decreased with the 70% ethanol extraction derived from FID. This study suggests that 70% ethanol extraction of G. elegans dried by FID is the most optimal condition to obtain efficiently antioxidant compounds of G. elegans.

Extraction of Acetic Acid by Aliphatic Amino Extractants (지방족 아민 추출제에 의한 초산의 추출)

  • Lee, Han-Seob
    • Applied Chemistry for Engineering
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    • v.5 no.1
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    • pp.121-126
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    • 1994
  • To elucidate the effect on the reactive extraction of acetic acid, various carriers and modifiers were investigated. Carriers used were secondary and tertiary amines and solvation extractant. Diluent was n-butylacetate. Modifiers were 4-nonylphenol, TBP(Tti-n-butyl phospate) and isodecanol. Besides the effect of temperature and pH in aqueous phase were studied. The mixture of 50% tri-n-octyl/n-decylamine tertiary amine, gave higher degree of extraction and selectivity than other extractants in the extraction of acetic acid. It was found that 4-nonylphenol as modifier fairly good. The degree of extraction was higher with decreasing the pH in aquous phase and the temperature of extraction system.

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Electrokinetic Extraction of Pollutants from the Vicinity of Unregulated Landfill Site (동전기적 추출에 의한 비위생매립지 주변 오염지반의 정화)

  • Lee, MyungHo;Chung, Ha-Ik
    • Journal of the Korean Geosynthetics Society
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    • v.5 no.2
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    • pp.17-22
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    • 2006
  • This paper presents preliminary field investigations on the electrokinetic (EK) remediation coupled with permeable reactive barrier (PRB) system. unregulated and old-fashioned landfills are one of the primary contributors to various contaminated soil problems. In-situ EK remediation technology has been successfully applied to the environs of unregulated landfill site, located in Kyeong-Ki province, Korea. Atomizing slag was adopted as a PRB reactive material for the remediation of groundwater contaminated with inorganic and/or organic substances. From the preliminary investigations, the coupled technology of EK with PRB system would be effecitve to remeidate contaminated grounds without the extraction of pollutants from subsurface due to the reactions between the reactive materials and contaminants.

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Separation Characteristics of Lactic Acid by Using Mixed Tertiary Amine Extractants (혼합아민 추출제를 이용한 젖산의 분리특성)

  • Hong, Yeon-Gi;Hong, Won-Hui;Hong, Tae-Hui
    • KSBB Journal
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    • v.14 no.5
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    • pp.566-571
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    • 1999
  • Lactic acid is of interested as the raw material of biodegradable polymer. In this study lactic acid was separated by reactive extraction with mixed tertiary amine extractant dissolved in 1-octanol/n-heptane. Mixed tertiary amine extractant was composed of tripropylamine(TPA) and trioctylamine(TOA). The concentration range of lactic acid is ca. 5wt% which is the concentration of lactic acid obtained from fermentation.Maximum distribution coeficient was obtained at 8:2 weight ratio of TPA/TOA and their extraction efficiencies were above 90%.

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Separation of Cr(VI) from Heavy Metal Salts Mixed Solution by using Hollow Fiber Module (실관막모듈에 의한 중금속염 혼합용액으로부터 Cr(VI) 분리)

  • 최대웅
    • Journal of Environmental Health Sciences
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    • v.27 no.3
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    • pp.107-112
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    • 2001
  • This work reports the application of a hollow fiber module(HFM) for Cr(VI) extraction from heavy metal salts mixed solution by using microporous hydrophobic hollow fiber module. In HFM configuration, the organic extraction used for the extraction of Cr(VI) was di-(2-ethyl hexyl) phosphoric acid(D2EHPA) diluted with n-heptane. The study of HFM includes the influence of hydrodynamic and chemical condition, i.e., the flow rate of feed solution, the time of reactive extraction, the concentration of feed solution, and the pH of aqueous phase solutions. Several experiments with synthetic solution of different mixed components system of Cr(VI) solutions established optimum condition to achieve a clean separation of Cr(VI). It was possible to separate Cr(VI) in the presence of metal salts mixed solution, such as Zn(II), Ni(II), Cu(II), and Cd(II) using the HFM technique.

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Three-phase Four-wire Series Active Power Filter Control Strategy for The Compensation of Harmonics and Reactive Power Based-on Direct Compensating Voltage Extraction Method (직접 보상전압 추출기법을 이용하여 고조파전류와 무효전력을 보상하는 3상 4선식 직렬 형 능동전력필터의 제어법)

  • 김진선;김영석
    • The Transactions of the Korean Institute of Power Electronics
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    • v.9 no.3
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    • pp.213-221
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    • 2004
  • In recent years, since more and more diode rectifiers with smoothing dc capacitor are used in electronic equipments, household appliances and ac drives, harmonics generated by these loads have become a major issue. In addition, 3-phase 4-wire system is widely employed in distributing electric energy to several office building and manufacturing plants. This systems show excessive currents in the neutral. These neutral currents are fundamentally third harmonic, and their presence is tied to wiring failure, elevating of neutral potentials, transformer overheating, etc. In response to the concerns, this paper proposes a series active power filter scheme based on direct compensating voltage extraction method and the advantage of this control algorithm is direct extraction of compensation voltage reference without multiplying gain. Therefore, the calculation of the compensation voltage reference will becom much simpler than other control algorithm. To verify the effectiveness of the proposed algorithm, a prototype active power filter is built and some experiments are carried out.

A study on Reactor Parameter of Atmosphere Plasma Power Supply

  • Lee, Woo-Cheol
    • Proceedings of the KIPE Conference
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    • 2011.11a
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    • pp.291-292
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    • 2011
  • This paper proposes an extraction method for reactor parameters in atmosphere plasma power supplies. This method is performed by detecting phase difference between inverter voltage and current, and extracting the reactance through reactive power. The validity of the proposed scheme is investigated through simulation results and experimental results.

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Reactive Power Control of Single-Phase Reactive Power Compensator for Distribution Line (배전선로용 단상 무효전력 보상기의 무효전력제어)

  • Sim, Woosik;Jo, Jongmin;Kim, Youngroc;Cha, Hanju
    • The Transactions of the Korean Institute of Power Electronics
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    • v.25 no.2
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    • pp.73-78
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    • 2020
  • In this study, a novel reactive power control scheme is proposed to supply stable reactive power to the distribution line by compensating a ripple voltage of DC link. In a single-phase system, a magnitude of second harmonic is inevitably generated in the DC link voltage, and this phenomenon is further increased when the capacity of DC link capacitor decreases. Reactive power control was performed by controlling the d-axis current in the virtual synchronous reference frame, and the voltage control for maintaining the DC link voltage was implemented through the q-axis current control. The proposed method for compensating the ripple voltage was classified into three parts, which consist of the extraction unit of DC link voltage, high pass filter (HPF), and time delay unit. HPF removes an offset component of DC link voltage extracted from integral, and a time delay unit compensates the phase leading effect due to the HPF. The compensated DC voltage is used as feedback component of voltage control loop to supply stable reactive power. The performance of the proposed algorithm was verified through simulation and experiments. At DC link capacitance of 375 uF, the magnitude of ripple voltage decreased to 8 Vpp from 74 Vpp in the voltage control loop, and the total harmonic distortion of the current was improved.

Antioxidant capacity of silkworm pupa according to extraction condition, variety, pupation time, and sex

  • Lee, Ji Hae;Jo, You-Young;Kim, Seong-Wan;Kweon, HaeYong
    • International Journal of Industrial Entomology and Biomaterials
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    • v.43 no.2
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    • pp.59-66
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    • 2021
  • Silkworm pupa has been used as an edible insect with the high quality of protein and unsaturated fatty acids. In this study, antioxidant activities of pupa according to variety, pupation day, sex, and extraction solvent were analyzed. The 30% ethanol extract showed highest radical scavenging activity compared with the DW, hexane, and 70-100% ethanol extracts. In the DPPH and ABTS radical scavenging assay according to the type of pupa, the antioxidant effect was increased in female with the early stage of pupation day. In cell-based assay, reactive oxygen species (ROS) level was decreased in pupa groups by -30 to -50% followed by tert-butyl hydroperoxide (t-BHP) treatment. The ROS levels were significantly reduced in 7th day in each variety. In conclusion, the free radical and ROS scavenging effects were increased in female pupa with the early pupation day. The result could be used for development of bioactive materials using silkworm pupa.

Mass Transfer of Citric and Acetic Acid by Reactive Extractant in Batch Extractor (회분식 추출기에서 반응추출제에 의한 구연산과 초산의 물질이동)

  • Lee, Han-Seob
    • Applied Chemistry for Engineering
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    • v.5 no.2
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    • pp.223-229
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    • 1994
  • The effect of agitation speed on mass transfer coefficient in the extraction of citric acid from mixed aqueous solutions of citric and acetic acid with n-butylacetate solutions of di-isotridecylamine(DITDA) and 50% mixture of tri-n-octyl and try-n-hexyl phosphine oxide(MOHPO), were studied in batch extractor. Experimental results showed that the degree of extraction was higher with increasing agitation speed, and was best at 200rpm and 30 minutes in batch extractor. The higher degree of extraction was obtained in mixed solution of citric-acetic acid by using DITDA than MOHPO as an carrier. Mass transfer coefficient was proportional to the degree of extraction, and $K_r=1.254{\times}10^{-3}Re^{0.536}$ was found for she extraction of citric acid by DITDA.

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