• 제목/요약/키워드: rare-earth

검색결과 988건 처리시간 0.029초

稀土類中 토리움의 分離定量 에 관하여 (第一報) 過酸化水素法에 對한 檢討 (Th-determination in Rare Earth(1) studies on the Hydrogen Peroxide Method of Th-determination)

  • 최한석;박순자
    • 대한화학회지
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    • 제4권1호
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    • pp.10-12
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    • 1957
  • On the performance of the hydrogen peroxide method for Th-determination we encountered some difficulties, namely the formation of the insoluble matter occured in the nearly neutral solution after evaporation. We carried out the Th-determination in the mixture of the Th and some kind of the rare earth, and found that the insoluble matter was not formed in case of the mixture of Th and some kind of rare earth, but formed in case of Monazite. The formation of the insoluble matter in the case of Monazite sand, however, could be avoid by using the beaker instead of the evaporating dish and by adding the water repeatedly before it was completely evaporated to dryness.

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A Magnetic Hysteresis Curve Tracer for Rare Earth

  • Rhee, J.R.
    • Journal of Magnetics
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    • 제1권2호
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    • pp.94-100
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    • 1996
  • A hysteresis loop tracer using a pulsed high magnetic field of 113.4 kOe, which is suitable for rare earth based permanent magnets, is constructed. The high pulsed magnetic field is generated by discharging a large capacitance charge (5 mF) with a voltage of 600 V into an air solenoid with the inner diameter of 14 mm, outer diameter of 36 mm and the lingth of 34 mm. A computer simulation method is used for the construction of an electromagnet to optimize the many parameters such as the discharge current, generated pulsed magnetic field intensity, thermal dissipation, capacitance, charged voltage, period of damping oscillation and solenoid geometry. By using the hysteresis loop tracer constructed in this work, we are able to measure hystersis loops of several rare earth based permanent magnets with large values of the remanent magnetization, coercvity and energy product.

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Spinel Ferrite에 관한 연구 (I) Mn-Zn계 Ferrite의 자기특성에 대한 희토류산화물의 첨가효과 (Studies on Spinel Ferrites (I) Effects of Addition of Rare-Earth Oxides on the Magnetic Properties of Mn-Zn Ferrites)

  • 김태옥
    • 한국세라믹학회지
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    • 제14권2호
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    • pp.78-81
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    • 1977
  • The effects of variation in composition and the addition of small amount of the rare-earth oxides La2O3, CeO2 and Sm2O3 on the magnetic properties of Mn-Zn system ferrites, 0.5MnO.0.5ZnO.(1+0.1X) Fe2O3(X=-1, 0, 1, 2), were investigated in the range of frequencies of 0.1~100 kHz. It was shown that the magnetic permeability of the specimens with the composition Mn 0.5 Zn 0.5 Fe2O4 was maximum in the Mn-Zn system ferrites, and that the addition of a small amount of the rare-earth oxides to the composition 0.5 MnO.0.5ZnO.0.9 Fe2O3 caused the sharp increase of magnetic permeability and the decrease of the loss factors.

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전동식 조향장치용 스위치드 릴럭턴스 모터 드라이브 개발 (Development of Switched Reluctance Motor Drive for Electric Power Steering System)

  • 정민창;주민기;김재혁
    • 전기학회논문지
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    • 제63권11호
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    • pp.1511-1518
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    • 2014
  • Demand for high fuel efficiency and smart features of the vehicles, research has been intensified. Hence, research and development on electric power steering (EPS) system to replace the existing hydraulic steering system has been actively conducted. Permanent magnet motors are widely used in automotive applications due to their high power density and high efficiency. However, increasing price and limited production of rare-earth permanent magnets has recently prompted the auto parts makers to substitute permanent magnet motors by non- or less rare earth magnet motors. Switched reluctance motors SRMs), known as typical non-rare earth motors have simple structure, low manufacturing cost, and high reliability. This paper discusses design, modeling, simulation, and experimental verification of a prototype SRM drive for electric power steering system.

실험계수법을 이용한 희토류산화물의 X-선 형광분광분석 (The Determination of Rare Earth Oxides by X-Ray Fluorescence Spectrometry Using Empirical Coefficient Method)

  • 김영만;최범석;김선태;이종욱
    • 대한화학회지
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    • 제31권1호
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    • pp.64-70
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    • 1987
  • 모자나이트광에서 희토류원소(Y 및 Th포함)를 분리하여 X-선 형광분광법으로 정량하였다. 희토류원소간의 상호간섭이 있으므로 이를 메트릭스 계수를 이용한 실험계수법으로 보정하였다. 이 방법에서 표준시료의 수는 메트릭스 계수에는 큰 영향을 미치지만 분석결과는 큰 차이가 없었으며 유도결합플라스마 분광법에 의한 분석결과와 비교적 잘 일치하였다.

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희토류가 첨가된 Mn-Zn ferrite의 복소투자율 분석 (An analysis of complex permeability of Mn-Zn ferrite doped with rare earth oxide)

  • 김성수;최우성
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 추계학술대회 논문집
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    • pp.93-96
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    • 2000
  • In this study, we investigated the electromagnetic properties of Mn-Zn ferrite doped with rare earth oxide (Dy$_2$O$_3$, Er$_2$O$_3$). The main composition is 52mo1% ${\alpha}$-Fe$_2$O$_3$, 25mol% Mn$_3$O$_4$ 23mo1% ZnO and doped with them(0.05wt% ∼ 0.25wt%, step:0.05wt%). An experimental process has advanced by conventional ferrimagnetism manufacturing that was prepared by standard ceramic techniques. The XRD pattern of all doped sample were observed spinel and secondary phase. The density of sample were measured nearly constant value. As increased the additive, resistivity, initial permeability and real component of the series complex permeability increased with setting limits each other. In case of Mn-Zn ferrite excess doped with them, resistivity, initial permeability and real component of the series complex permeability decreased and magnetic loss increased in proportion to increasing the additive.

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권선계자형 동기전동기의 d축 쇄교자속에 의한 계자전류리플 보상 기법 개발 (Development of Field Current ripple Compensating Method by d-axis Flux-linkage in WRSM)

  • 황대연;구본관
    • 전기학회논문지
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    • 제67권9호
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    • pp.1165-1173
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    • 2018
  • Recently, owing to environmental problems and instability of rare earth resources market, non-rare earth electric motors are attracting attention. As a non-rare earth motor type, a wound rotor synchronous motor(WRSM) has high power density and wide driving range further it can reduce loss by field current control during field weakening control at high speed. However, since the d-axis flux of the WRSM is coupled with the rotor circuit, the fluctuation in the d-axis flux linkage affects the rotor circuit, which causes ripple of the field current and torque. In this paper, we propose the field current ripple compensation method by injecting the feedforward voltage. the proposed compensating method was demonstrated by simulation and experiments.

Separation of Light Rare-Earth Elements Using Gas-Pressurized Extraction Chromatography

  • Kim, Namuk;Park, Jai Il;Um, Wooyong;Kim, Jihye
    • Mass Spectrometry Letters
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    • 제12권4호
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    • pp.186-191
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    • 2021
  • A new method for chemical separation of light rare-earth elements (LREEs) using gas-pressurized extraction chromatography (GPEC) is described. GPEC is a microscale column chromatography system that features a constant flow of solvents, which is created by pressurized nitrogen gas. The separation column with a Teflon tubing was packed with LN resin. The proposed GPEC method facilitates production of lesser chemical wastes and faster separation owing to the use of low solvent volume compared to traditional column chromatography. We evaluated the separation of Ba, La, Ce, and Nd using various elution solvents. The column reproducibility of the proposed GPEC system ranged from 2.4% to 4.9% with RSDs of recoveries, and the column-to-column reproducibility ranged from 3.1% to 6.3% with RSDs of recoveries. The proposed technique is robust, and it can be useful for the fast separation of LREEs.

Recent developments of manganese-aluminium as rare-earth-free magnets

  • Sirisathitkul, Chitnarong
    • Advances in materials Research
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    • 제9권4호
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    • pp.323-335
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    • 2020
  • This article reviews findings and progresses in the past decade on manganese-aluminium (MnAl) based magnets as the interest has been revived to fulfill their potential as commercial magnets. The challenges in developments of these rare-earth-free magnets are to acquire a high remanence and coercivity from the ferromagnetic τ-phase in MnAl alloys. To this end, the phase transformation to this τ-MnAl with L10 body centered tetragonal structure has been promoted by a variety of methods and a few percents of carbon (C) is often added to prevent the phase decomposition. Magnetization and coercivity are not only influenced by the phase composition but also the microstructure. The fabrication processes and factors affecting the phase and microstructure are therefore covered. Finally, the productions of bulk MnAl magnets are addressed.

A review of chromatographic analysis for rare-earth elements with focus on Ln resin

  • Jihye Kim;Kihwan Choi
    • 분석과학
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    • 제36권6호
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    • pp.259-266
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    • 2023
  • The demand for rare-earth elements (REEs) is increasing owing to their significance as prominent materials in electronics, high-tech industries, geological research, nuclear forensics, and environmental monitoring. In general, the utilization of REEs in various applications requires the use of chromatographic techniques to separate individual elements. However, REEs have similar physicochemical properties, which makes them difficult to separate. Recently, several studies have examined the separation of REEs using LN resin as the stationary phase and aqueous nitric acid and hydrochloric acid solutions as eluents. Using this method, light REEs have been separated using dilute acid solutions as the eluent, whereas heavy REEs are separated using solutions with high acid concentrations. To increase the separation resolution between different REEs, either the column length or resin size is changed. In addition, the suggested methods are implemented to decrease the analysis time. This review presents technical information on the chromatographic separation of REEs using the LN resin and discusses the optimal experimental conditions.