• 제목/요약/키워드: rapid sintering

검색결과 214건 처리시간 0.025초

펄스전류활성 소결 공정을 이용한 Ni 함량변화에 따른 WC 소재의 특성평가 (Characteristic Evaluation of WC Hard Materials According to Ni Content Variation by a Pulsed Current Activated Sintering Process)

  • 박현국
    • 한국재료학회지
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    • 제30권12호
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    • pp.672-677
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    • 2020
  • Expensive PCBN or ceramic cutting tools are used for the processing of difficult-to-cut materials such as Ti and Ni alloy materials. These tools have a problem of breaking easily due to their high hardness but low fracture toughness. To solve this problem, cutting tools that form various coating layers are used in low-cost WC-Co hard material tools, and researches on various tool materials are being conducted. In this study, WC-5, 10, and 15 wt%Ni hard materials for difficult-to-cut cutting materials are densified using horizontal ball milled WC-Ni powders and pulsed current activated sintering method (PCAS method). Each PCASed WC-Ni hard materials are almost completely dense, with a relative density of up to 99.7 ~ 99.9 %, after the simultaneous application of pressure of 60 MPa and electric current for 2 min; process involves almost no change in the grain size. The average grain sizes of WC and Ni for WC-5, 10, and 15 wt%Ni hard materials are about 1.09 ~ 1.29 and 0.31 ~ 0.51 µm, respectively. Vickers hardness and fracture toughness of WC-5, 10, and 15 wt%Ni hard materials are about 1,923 ~ 1,788 kg/mm2 and 13.2 ~ 14.3 MPa.m1/2, respectively. Microstructure and phase analyses of PCASed WC-Ni hard materials are performed.

방전플라즈마 소결 공정을 이용한 WC-6wt.%Co 소결체 제조 및 기계적 특성 평가 (Fabrication and Mechanical Properties of ultra fine WC-6wt.%Co by Spark Plasma Sintering Process)

  • 박현국;이승민;윤희준;방기상;오익현
    • 대한금속재료학회지
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    • 제49권1호
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    • pp.40-45
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    • 2011
  • Using the spark plasma sintering process (SPS process), the WC-6wt.%Co hard materials were densified using an ultra fine WC-Co powder. The WC-Co was almost completely dense with a relative density of up to 100% after the simultaneous application of a pressure of 60 MPa and the DC pulse current for 3 min without any significant change in the grain size. The average grain size of WC that was produced through this experiment was about $0.2{\sim}0.8{\mu}m$. The hardness and fracture toughness were about $1816kg/mm^2$ and $15.1MPa{\cdot}m^{1/2}$, respectively, for 60 MPa at $1200^{\circ}C$.

쾌속조형 기술과 진공성형법을 이용한 시작차량용 대형 중공 부품의 제작에 관한 연구 (A Study on the Manufacturing of Large Size Hollow Shape Parts for Prototype-Car using Rapid Prototyping Technology and Vacuum Molding)

  • 박경수;양화준;최경현;이석희
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2000년도 추계학술대회 논문집
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    • pp.362-365
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    • 2000
  • Rapid Prototyping(RP) techniques have revolutionized traditional manufacturing methods. These techniques allow the user to fabricate a part directly from a conceptual model before investing in production tooling and help develop new models with significant short time. This paper suggests to new process to manufacture large size hollow shape parts for prototype-car using Rapid Prototyping technology and Vacuum Molding with the reduction of delivery time. In addition, This paper introduces the dividing and combining method to make large size RP master model in spite of the limit of the build chamber dimensions of commercialized RP system and post-processing method to achieve sufficient surface quality.

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RP 공정의 정밀도 비교 평가 (Comparison of Accuracy of RP Processes)

  • 변홍석;신행재;이관행
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2000년도 추계학술대회 논문집
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    • pp.330-333
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    • 2000
  • Dimensional accuracy and surface quality are very important in rapid prototyping especially when the models are used for the production of tools. This paper presents the development of benchmarking part to investigate dimensional accuracy and surface finish. A new test part is designed to perform benchmarking of major rapid prototyping processes such as selective laser sintering, laminated object manufacturing, stereolithography apparatus, and fused deposition modeling. The test part design includes basic manufacturing features such as holes, walls, squares, cylinder and etc. In addition, the small features are included in order to evaluate the fine details that can be manufactured by a specific RP process. The CMM program that automatically measures different features in the test part is also developed. The evaluation of accuracy as well as surface roughness are discussed for major rapid prototyping processes.

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Investigation of Spark Plasma Sintering Temperature on Microstructure and Thermoelectric Properties of p-type Bi-Sb-Te alloys

  • Han, Jin-Koo;Shin, Dong-won;Madavali, Babu;Hong, Soon-Jik
    • 한국분말재료학회지
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    • 제24권2호
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    • pp.115-121
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    • 2017
  • In this work, p-type Bi-Sb-Te alloys powders are prepared using gas atomization, a mass production powder preparation method involving rapid solidification. To study the effect of the sintering temperature on the microstructure and thermoelectric properties, gas-atomized powders are consolidated at different temperatures (623, 703, and 743 K) using spark plasma sintering. The crystal structures of the gas-atomized powders and sintered bulks are identified using an X-ray diffraction technique. Texture analysis by electron backscatter diffraction reveals that the grains are randomly oriented in the entire matrix, and no preferred orientation in any unique direction is observed. The hardness values decrease with increasing sintering temperature owing to a decrease in grain size. The conductivity increases gradually with increasing sintering temperature, whereas the Seebeck coefficient decreases owing to increases in the carrier mobility with grain size. The lowest thermal conductivity is obtained for the bulk sintered at a low temperature (603 K), mainly because of its fine-grained microstructure. A peak ZT of 1.06 is achieved for the sample sintered at 703 K owing to its moderate electrical conductivity and sustainable thermal conductivity.

방전플라즈마 소결 공정을 이용한 스퍼터링 타겟용 타이타늄 소결체 제조 및 특성 평가 (Fabrication and Evaluation Properties of Titanium Sintered-body for a Sputtering Target by Spark Plasma Sintering Process)

  • 이승민;박현국;윤희준;양준모;우기도;오익현
    • 대한금속재료학회지
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    • 제49권11호
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    • pp.845-852
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    • 2011
  • The Spark Plasma Sintering(SPS) method offers a means of fabricating a sintered-body having high density without grain growth through short sintering time and a one-step process. A titanium compact having high density and purity was fabricated by the SPS process. It can be used to fabricate a Ti sputtering target with controlled parameters such as sintering temperature, heating rate, and pressure to establish the optimized processing conditions. The compact/target(?) has a diameter of ${\Phi}150{\times}6.35mm$. The density, purity, phase transformation, and microstructure of the Ti compact were analyzed by Archimedes, ICP, XRD and FE-SEM. A Ti thin-film fabricated on a $Si/SiO_2$ substrate by a sputtering device (SRN-100) was analyzed by XRD, TEM, and SIMS. Density and grain size were up to 99% and below $40{\mu}m$, respectively. The specific resistivity of the optimized Ti target was $8.63{\times}10^{-6}{\Omega}{\cdot}cm$.

급속승온공정을 이용한 사출성헝된 Fe 소결체의 미세조직 및 소결거동 (Microstructure and Sintering Behavior of Injection Molded Fe Sintered Body Using Rapid Thermal Heating Process)

  • 김기현;한재길;유지훈;최철진;이병택
    • 한국분말재료학회지
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    • 제11권6호
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    • pp.528-534
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    • 2004
  • Using the nano Fe powders having 50 nm in diameter, Fe compact bodies were fabricated by injec-tion molding process. The relationship between microstructure and material properties depending on the volume ratio of powder/binder and sintering temperature were characterized by SEM, TEM techniques. In the compact body with the volume percentage ratio of 45(Fe powder) : 55(binder), which was sintered at $700^{\circ}C,$ the relative density was about $97{\%},$ and the values of volume shrinkage and hardness were about $66.3{\%}$ and 242.0 Hv, respec-tively. Using the composition of 50(Fe powder) : 50(binder) and sintered at $700^{\circ}C,$ the values of relative density, volume shrinkage and hardness of Fe sintered bodies were $73.3{\%},\;47.6{\%}$ and 152.8 Hv, respectively. They showed brittle fracture mode due to the porous and fine microstructure.

직접식 조형법의 금속 분말 적층부 소결에 관한 연구 (Numerical Analysis for Sintering of Metal Powder Layers of the Direct Metal Prototyping)

  • 손현기;양동열
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 1997년도 춘계학술대회 논문집
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    • pp.552-556
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    • 1997
  • The Direct Metal Prototyping(DMP), one of the rapid prototyping technologies, allows the manufacturing of three-dimensional metallic parts using metal powders directly from the CAD data. Laser power and scanning speed are the most important variables of the process. The objective of this study is to obtain the design data for laser power and scanning speed to bond metal powders effectively using the finite element method. To obtain the design values, a numerical analysis considering two-dimensional heat transfer during the sintering of metal powder layers of the process was performed. The laser beam has been modeled to have directionality in its heat flux distribution, i. e., in the scanning direction a Gaussian beam mode distribution has been assumed and in the thickness direction a square beam mode distribution. The three-dimensional irregular distribution of metal powders of the powder layer is idealized as two-dimensional distribution in which metal powders are located regularly and periodically on the plate. In this study the design values of laser power vs scanning speed have been obtained. Temperature distribution and temperature variation of the powder layers with respect to time have been predicted. The commputed dsign data will be useful in determining the initial conditions of the process.

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