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Push-out bond strength and intratubular biomineralization of a hydraulic root-end filling material premixed with dimethyl sulfoxide as a vehicle

  • Ju-Ha Park;Hee-Jin Kim;Kwang-Won Lee;Mi-Kyung Yu;Kyung-San Min
    • Restorative Dentistry and Endodontics
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    • v.48 no.1
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    • pp.8.1-8.8
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    • 2023
  • Objectives: This study was designed to evaluate the parameters of bonding performance to root dentin, including push-out bond strength and dentinal tubular biomineralization, of a hydraulic bioceramic root-end filling material premixed with dimethyl sulfoxide (Endocem MTA Premixed) in comparison to a conventional powder-liquid-type cement (ProRoot MTA). Materials and Methods: The root canal of a single-rooted premolar was filled with either ProRoot MTA or Endocem MTA Premixed (n = 15). A slice of dentin was obtained from each root. Using the sliced specimen, the push-out bond strength was measured, and the failure pattern was observed under a stereomicroscope. The apical segment was divided into halves; the split surface was observed under a scanning electron microscope, and intratubular biomineralization was examined by observing the precipitates formed in the dentinal tubule. Then, the chemical characteristics of the precipitates were evaluated with energy-dispersive X-ray spectroscopic (EDS) analysis. The data were analyzed using the Student's t-test followed by the Mann-Whitney U test (p < 0.05). Results: No significant difference was found between the 2 tested groups in push-out bond strength, and cohesive failure was the predominant failure type. In both groups, flake-shaped precipitates were observed along dentinal tubules. The EDS analysis indicated that the mass percentage of calcium and phosphorus in the precipitate was similar to that found in hydroxyapatite. Conclusions: Regarding bonding to root dentin, Endocem MTA Premixed may have potential for use as an acceptable root-end filling material.

A Study on the Slip Test of Shear Connector in Fire (전단 연결재의 고온 성능 평가에 관한 연구)

  • Han, Sang-Hoon;Park, Won-Sup;Lee, Choul-Ho
    • Proceedings of the Korea Institute of Fire Science and Engineering Conference
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    • 2008.04a
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    • pp.48-51
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    • 2008
  • Shear connector is the element which resist in the horizontal shear force between steel and concrete of composite members and the stud bolt is often used because of its constructional convenience and serviceability. Although the push-out test is the most common method to evaluate shear slip behaviour, it is suitable for only room temperature conditions. In this study, we investigated about shear force, temperature distribution and slip displacement of shear connector in high temperature through the modified push-out test with electronic furnace invented for steel part heating.

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Evaluation of Shear-Induced Phase Transformation of $\beta$-Cristobalite by Fiber Push-Out Technique

  • Sang Jin Lee;Dong Zhu;Jae Suk Sung
    • The Korean Journal of Ceramics
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    • v.3 no.3
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    • pp.208-212
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    • 1997
  • Shear-induced phase transformation behavior of chemically stabilized $\beta$-cristobalite was studied by the fiber push-out technique. To obtain the critical grain size for phase transformation, the hot-pressed polycrystalline $\beta$-cristobalite, which was used as the interphase between fiber and matrix, was annealed at $1300^{\circ}C$ for 10h. Two types of fibers, mullite and sapphire fiber, were used in this study. Debonding between mullite fiber and cristobalite interphase occurred at a critical load of 230 MPa. Static friction and fiber sliding were continuously followed by debonding. Shear-induced transformation induced cracks in the cristobalite interphase at the debonding stage. In the case of the sapphire fiber, the debonding occurred at a lower load of 180 MPa due to the residual stress in the interface caused by the difference in thermal expansion coefficients between the fiber and the cristobalite interphase. The load was insufficient for shear-induced phase transformation.

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Study on push-out test and bond stress-slip relationship of circular concrete filled steel tube

  • Yin, Xiaowei;Lu, Xilin
    • Steel and Composite Structures
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    • v.10 no.4
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    • pp.317-329
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    • 2010
  • According to the results of 9 circular concrete filled steel tube (CFT) push-out tests, a new theoretical model for average bond stress versus free end slip curve is proposed. The relationship between verage bond stress and free end slip is obtained considering some varying influential parameters such as slenderness ratio and diameter-to-thickness ratio. Based on measured steel tube strain and relative slip at different longitudinal positions, the distribution of bond stress and relative slip along the length of steel tube is obtained. An equation for predicting the varying bond-slip relationship along longitudinal length and a position function reflecting the variation are proposed. The presented method can be used in the application of finite element method to analyze the behavior of CFT structures.

Interfacial shear resistance of angle shear connectors welded to concrete filled U-shaped CFS beam

  • Oh, Hyoung Seok;Shin, Hyeongyeop;Ju, Youngkyu;Kang, Thomas H.K.
    • Steel and Composite Structures
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    • v.43 no.3
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    • pp.311-325
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    • 2022
  • For multi-story structural systems, Korean steel industry has fostered development of a steel-concrete composite beam. Configuration of the composite beam is characterized by steel angle shear connectors welded to a U-shaped cold formed-steel beam. Effects of shear connector orientation and spacing were studied to evaluate current application of the angle shear connector design equation in AC495. For the study, interfacial shear resistance behavior was investigated by conducting 24 push-out tests and attuned using unreinforced push-out specimens. Interfacial shear to horizontal slip response was reported along with corresponding failure patterns. Pure shear connector strength was also evaluated by excluding concrete shear contribution, which was estimated in relation to steel beam-slab interface separation or interfacial crack width.

The effect of individualization of fiberglass posts using bulk-fill resin-based composites on cementation: an in vitro study

  • Lins, Rodrigo Barros Esteves;Cordeiro, Jairo Matozinho;Rangel, Carolina Perez;Antunes, Thiago Bessa Marconato;Martins, Luis Roberto Marcondes
    • Restorative Dentistry and Endodontics
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    • v.44 no.4
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    • pp.37.1-37.10
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    • 2019
  • Objectives: This study evaluated the bond strength of various fiberglass post cementation techniques using different resin-based composites. Materials and Methods: The roots from a total of 100 bovine incisors were randomly assigned to 5 treatment groups: G1, post + Scotchbond Multi-Purpose (SBMP) + RelyX ARC luting agent; G2, relined post (Filtek Z250) + SBMP + RelyX ARC; G3, individualized post (Filtek Z250) + SBMP; G4, individualized post (Filtek Bulk-Fill) + SBMP; G5, individualized post (Filtek Bulk-Fill Flow) + SBMP. The samples were subjected to the push-out (n = 10) and pull-out (n = 10) bond strength tests. Data from the push-out bond strength test were analyzed using 2-way analysis of variance (ANOVA) with the Bonferroni post hoc test, and data from the pull-out bond strength test were analyzed using 1-way ANOVA. Results: The data for push-out bond strength presented higher values for G2 and G5, mainly in the cervical and middle thirds, and the data from the apical third showed a lower mean push-out bond strength in all groups. No significant difference was noted for pull-out bond strength among all groups. The most frequent failure modes observed were adhesive failure between dentine and resin and mixed failure. Conclusions: Fiberglass post cementation using restorative and flowable bulk-fill composites with the individualization technique may be a promising alternative to existing methods of post cementation.

An Evaluation on the Shear Strength of New Type Shear Connectors for a Simple Steel-Concrete Composite Deck (초간편 강합성 바닥판 신형식 전단연결재의 전단내력 평가)

  • Yoon, Ki Yong;Kim, Sang Seup;Han, Deuk Cheon
    • Journal of Korean Society of Steel Construction
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    • v.20 no.4
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    • pp.519-528
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    • 2008
  • A simple steel-concrete composite deck is developed for preventing the lateral torsional buckling of girders that are under construction and for reducing the term of works using H-shaped rolled beams as bridge girders. A new type of shear connectors is also developed for the composite behavior between a simple steel-concrete composite deck and the rolled beams by the connecting conditions between the deck and the girders. One is a connector bolt that is lengthened and split or tightened with two nuts and the other is an I-shaped rolled beam welded on a steel plate with a number of holes punched through the web. In this study, to estimate the shear strength of those shear connectors the push-out tests are performed and the test results are compared with that of the previous studies and the codes. The result of the push-out tests of the connector bolts showed that the shear performance is similar to that of the stud connector and revealed that the equation for the shear strength in the Korean Specification of Highway Bridge overestimates the shear capacity of the connector bolt whose diameter is larger than 19mm. From the push-out tests of punched I-shaped rolled beams with varying welding amounts, with the small amount of welding, shear capacity is governed by the shear capacity of welding. On the other hand, shear capacity is governed by the size of the punched I-shaped rolled beams, regardless of the amount of welding.

The K-band push-push type miniaturized haripin resonator oscillator (소형 Haripin 공진기를 이용한 K 대역 Push-Push형 발진기)

  • 주한기
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.22 no.5
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    • pp.967-973
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    • 1997
  • In this paper, the designed and fabrication of a K-band push-push oscillator using miniaturized hairpin resonator have been presented. One experimenal oscillator has been designed and fabricated for K-band point-to-point operation. the miniaturized harpin resonator has been analyzed theoretically and simulated by MPIE(Mixed Potential Integral Equation) method. With this results, the analysis of hairpin resonator which coupled microstrip line has been carried out with transmission-mode using this results. an optimized output matching network for the suppression of the fundamental and the 3rd order harmonic was acquired by using a nonlinear analysis method. The fabricated oscillator shows the output power of -2.28dBm, the fundamental frequency suppression of -19dBc, the 3rd order harmonic suppressionof -24dBc and 0.33 percent effiiency at 22.8GHz. The experimental outputs are in good agreement with the theoretical and simulated results.

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LDO Regulator with Improved Fast Response Characteristics and Push-Pull Detection Structure (Push-Pull Detection 구조 및 빠른 응답 특성을 갖는 LDO 레귤레이터)

  • Lee, Joo-Young
    • Journal of IKEEE
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    • v.25 no.1
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    • pp.201-205
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    • 2021
  • In this paper present Low Drop-Out (LDO) regulator that improved load transient characteristics due to the push-pull detection structure. The response characteristic of the voltage delta value is improved due to the proposed push-pull sensing circuit structure between the input terminal of the LDO regulator pass transistor and the output terminal of the internal error amplifier. Voltage value has improved load transient characteristics than conventional LDO regulator. Compared to the conventional LDO regulator, it has an improved response speed of approximately 244 ns at rising time and approximately 90 ns at falling time. The proposed circuit was simulated by the samsung 0.13um process using Cadence's Specter and Virtuoso simulator.

Effect of Blood Contamination on the Push-Out Bond Strength and Surface Morphology of Tricalcium Silicate Materials (혈액오염이 Tricalcium Silicate 재료의 압출강도와 표면형태에 미치는 영향)

  • Park, Misun;Kim, Jaehwan;Choi, Namki;Kim, Seonmi
    • Journal of the korean academy of Pediatric Dentistry
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    • v.43 no.1
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    • pp.36-43
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    • 2016
  • The aim of this study was to evaluate the effect of blood contamination on the push-out bond strength and surface morphology of tricalcium silicate materials; Biodentine$^{(R)}$, Theracal$^{(R)}$ and mineral trioxide aggregate. The standardized lumens of root slices prepared from extracted single-root human teeth were filled with Biodentine$^{(R)}$, Theracal$^{(R)}$ and mineral trioxide aggregate by manufacturer's instruction. The specimens were randomly divided into 2 groups (n = 20) for each material and then incubated for 4 days at $37^{\circ}C$; control group (phosphate buffered saline solution) and experimental group (fetal bovine serum). The push-out bond strengths were then measured by a universal testing machine and the surface morphology of each experimental group was analyzed by scanning electron microscope. Biodentine$^{(R)}$ and Theracal$^{(R)}$ showed higher push-out bond strength compared with mineral trioxide aggregate after exposure to fetal bovine serum. A substantial change in the surface morphology of each material was observed after exposure to fetal bovine serum. In conclusion, the push-out bond strengths of Biodentine$^{(R)}$ and Theracal$^{(R)}$ were higher than mineral trioxide aggregate when exposed to blood contamination. Therefore, it is supposed that the use of Biodentine$^{(R)}$ and Theracal$^{(R)}$ is appropriate in the presence of blood.