• 한국마이크로전자및패키징학회:학술대회논문집
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• 한국마이크로전자및패키징학회 2002년도 춘계 기술심포지움 논문집
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• pp.109-114
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• 2002

The adhesion of electroless plated Ni layer on Al/Si substrates has been investigated. The zincating treatment was conducted with a conventional method and a modified method. In a modified method, ultrasonic agitation was applied during zincating. Adhesion strength was evaluated by a pull-off test. The ultrasonic agitation during zincating increased the nucleation density of Zn particles and refined Zn particle size. the adhesion strength of electroless Ni layer deposited on the modified zincated surface was higher than that on the conventionally zincated surface. the improvement of adhesion was attributed to the fine and dense Zn particles.

• 한국재료학회지
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• 제29권6호
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• pp.378-384
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• 2019

Ice accumulation on Aluminum Conductor Steel Reinforced(ACSR) cable during winter is an important matter in terms of safety, economy, and efficient power supply. In this work, the ice adhesion strengths of ACSR cable oxidized during different periods(7 years oxidized and 15 years oxidized) are evaluated. At first, a plate type dry oxidation standard specimen, whose surface characteristics are similar to those of ACSR cable, is prepared. Dry oxidation standard specimens are heat-treated at $500^{\circ}C$ for 20, 60, and 120 minutes in order to obtain different degrees of oxidation. After the dry oxidation, surface properties are analyzed using contact angle analyzer, atomic force microscopy, spectrophotometer, and gloss meter. The ice adhesion strengths are measured using an ice pull-off tester. Correlations between the surface properties and the ice adhesion strength are obtained through a regression analysis indicating a Boltzmann equation. It is revealed that the ice adhesion strength of 15-year oxidized ACSR cable is approximately 8 times higher than that of ACSR-bare.

• 산업기술연구
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• 제22권A호
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• pp.185-192
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• 2002

The performance of old and the new concrete construction depends upon bond strength between old and the new concrete. Current adhesive and strength measurement method ignores the effect of stress concentration from shape of specimens. Therefore, this research calculates stress concentration coefficient as the ratio of drilling depth to drilling diameter($h_s/D$), the ratio of overlay thickness to drilling diameter($h_0/D$), the ratio of steel disk thickness to drilling diameter(t/D), the ratio of overlay elastic modulus to substrate modulus($E_1/E_0$), the distance from core to corner border(L_$_{corner}$) and the distance between cores(L_$_{coic}$) vary. The finite element method is adapted to analysis The results from 'the F.E.M analysis are as follows. The stress concentration effects can be minimized when the ratio of drilling depth to drilling diameter($h_s/D$) is 0.20~0.25, the elastic modulus ratio($E_1/E_0$) is 06~1.0, and the ratio of steel disk thickness to drilling diameter(t/D) is 3.0. The overlay thickness, the distance from specimens to corner border(L_$_{corner}$), the distance between cores(L_$_{coic}$) almost do not affect to the stress concentration.

• Corrosion Science and Technology
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• 제19권2호
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• pp.51-56
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• 2020

The objective of this study was to improve properties of plasma sprayed HAp layer to titanium substrate by introducing an intermediate layer with two different methods. Before applying Zn doped HAp coating on titanium substrate, an intermediate layer was introduced by titanium plasma spray or titanium anodization. Heat treatments were conducted for some samples after titanium intermediate layer was formed. Zn doped HAp top layer was applied by plasma spraying. Three-point bending test and pull-off adhesion test were performed to determine the adhesion of Zn doped HAp coatings to substrates. Long-term credibility of Zn doped HAp plasma sprayed coatings on titanium was assessed by electrochemical impedance measurements in Hanks' solution. It was found that both titanium plasma sprayed and titanium anodized intermediate layer had excellent credibility. Strong adhesion to the titanium substrate was confirmed after 12 weeks of immersion for coating samples with titanium plasma sprayed intermediate layer. Samples with titanium anodized intermediate layer showed good bending strength. However, they showed relatively poor resistance against pulling off. The thickness of titanium anodized intermediate layer can be controlled much more precisely than that of plasma sprayed one, which is important for practical application.

• Corrosion Science and Technology
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• 제20권1호
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• pp.26-36
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• 2021

Pipes operating in the seawater environment faces cavitation degradation and corrosion of the metallic component, as well as a negative synergistic effect. Cavitation degradation shows the mechanism by which materials deteriorate by causing rapid change of pressure or high-frequency vibration in the solution, and introducing the formation and explosion of bubbles. In order to rate the cavitation resistance of materials, constant conditions have been used. However, while a dynamic cavitation condition can be generated in a real system, there has been little reported on the effect of ultrasonic amplitude on the cavitation resistance and mechanism of composites. In this work, 3 kinds of epoxy coatings were used, and the cavitation resistance of the epoxy coatings was evaluated in 3.5% NaCl at 15 ℃ using an indirect ultrasonic cavitation method. Eleven kinds of mechanical properties were obtained, namely compressive strength, flexural strength and modulus, tensile strength and elongation, Shore D hardness, water absorptivity, impact test, wear test for coating only and pull-off strength for epoxy coating/carbon steel or epoxy coating/rubber/carbon steel. The cavitation erosion mechanism of epoxy coatings was discussed on the basis of the mechanical properties and the effect of ultrasonic amplitude on the degradation of coatings.

• 한국구조물진단유지관리공학회 논문집
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• 제18권5호
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• pp.41-50
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• 2014

본 연구에서는 섬유종류에 따른 인발특성과 섬유보강 콘크리트의 휨특성에 대하여 평가하기 위하여, 섬유의 재질 및 형상 다른 후크형 강섬유, 비정질 강섬유 및 폴리아미드 섬유에 대하여 인발시험과 섬유보강 콘크리트 시험체를 제작하여 휨특성을 평가하였다. 그 결과, 후크형 강섬유의 경우 최대인발하중에서 섬유가 매트릭스로부터 인발되었지만, 비정질 강섬유는 섬유와 매트릭스의 부착강도가 섬유자체의 인장강도보다 높아 섬유가 매트릭스로부터 인발되지 않고 파괴되는 현상을 나타내었다, 한편, 폴리아미드 섬유는 연신율에 의해 최대인발 하중까지 변위가 크게 발생하였으며, 최대하중이후에 섬유가 끊어지는 파괴특성을 나타내었다. 섬유보강 콘크리트의 휨특성에 있어서 비정질 강섬유는 매트릭스와의 부착강도가 높고, 섬유의 혼입개체수가 많아 콘크리트의 최대휨강도는 높았지만, 균열발생 이후 섬유가 매트릭스로부터 인발되지 않고 섬유가 파괴되는 것에 의해 응력의 저하가 급격하게 발생하지만, 후크형 강섬유보강 콘크리트는 균열발생 이후 섬유가 인발되면서 응력의 저하가 완만하게 발생하였다. 폴리아미드 섬유보강 콘크리트는 균열발생이후 섬유의 연신률에 의해 응력이 급격하게 저하하는 구간이 발생하였으며, 섬유와 매트릭스의 부착에 의해 재상승하였다가 섬유가 끊어지면서 파괴되었다. 섬유와 매트릭스의 인발특성은 섬유보강 콘크리트의 휨강도 및 변형 능력에 큰 영향을 미치는 것으로 판단된다.

• Composites Research
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• 제33권3호
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• pp.115-124
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• 2020

적층복합재료, 특히 탄소섬유 복합재료는 금속에 비해 가벼우며 상대적으로 비강도 및 비강성이 뛰어나기 때문에 항공 우주 산업 및 자동차 산업 등과같이 광범위한 분야에서 사용되고 있다. 그러나, 적층 복합재료는 섬유의 배열이 모두 면내방향으로 배열되어있기 때문에 박리가 발생한다는 큰 단점이 있으며, 이는 적층복합재료의 응용분야를 제한한다. 본 연구에서는 먼저 π-빔과 평판이 결합된 형태의 적층복합재료 T-빔을 개발하고, 구조해석 및 기계적 물성평가를 통하여 설계변수를 최적화하였다. 이후 적층복합재료 T-빔의 설계변수를 3D 직조 프리폼에 동일하게 적용하여 T-빔을 개발하였으며, 적층구조에 비하여 향상된 기계적 강도를 달성할 수 있었다. 이러한 연구결과는 강도향상을 필요로 하는 기존의 적층복합재료 구조물에 적용 가능할 것으로 기대된다.

• 한국분말재료학회지
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• 제27권4호
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• pp.333-338
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• 2020

In this study, we fabricate a thin- and dense-BCuP-5 coating layer, one of the switching device multilayers, through a plasma spray process. In addition, the microstructure and macroscopic properties of the coating layer, such as hardness and bond strength, are investigated. Both the initial powder feedstock and plasma-sprayed BCuP-5 coating layer show the main Cu phase, Cu-Ag-Cu₃P ternary phases, and Ag phase. This means that microstructural degradation does not occur during plasma spraying. The Vickers hardness of the coating layer was measured as 117.0 HV, indicating that the fine distribution of the three phases enables the excellent mechanical properties of the plasma-sprayed BCuP-5 coating layer. The pull-off strength of the plasma-sprayed BCuP-5 coating layer is measured as 16.5 kg/㎠. Based on the above findings, the applicability of plasma spray for the fabrication process of low-cost multi-layered electronic contact materials is discussed and suggested.

• Advances in Computational Design
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• 제2권2호
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• pp.147-168
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• 2017

Over the past couple decades, externally bonded fiber reinforced polymer (FRP) composites have emerged as a repair and strengthening material for many concrete infrastructure applications. This paper presents an analytical investigation of the use of carbon FRP (CFRP) for a specific problem that occurs in concrete bridge girders wherein the girder ends are damaged by excessive exposure to deicing salts and numerous freezing/thawing cycles. A 3D finite element (FE) model of a full scale prestressed concrete (PC) I-girder is used to investigate the effect of damage to the cover concrete and stirrups in the end region of the girder. Parametric studies are performed using externally bonded CFRP shear laminates to determine the most effective repair schemes for the damaged end region under a short shear span-to-depth ratio. Experimental results on shear pull off tests of CFRP laminates that have undergone accelerated aging are used to calibrate a bond stress-slip model for the interface between the FRP and concrete substrate and approximate the reduced bond stress-slip properties associated with exposure to the environment that causes this type of end region damage. The results of these analyses indicate that this particular application of this material can be effective in recovering the original strength of PC bridge girders with damaged end regions, even after environmental aging.

• Corrosion Science and Technology
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• 제13권5호
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• pp.163-169
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• 2014

The corrosion resistance of epoxy-coated carbon steel was evaluated. The carbon steel surface was subjected to different treatment methods such as steel grit blasting and power tool treatment as well as contamination of water soluble salt. To study the effect of the surface treatments and contamination, the topology of the treated surface was observed by confocal microscopy and a pull-off adhesion test was conducted. The corrosion resistance of the epoxy-coated carbon steel was further examined by electrochemical impedance spectroscopy (EIS) combined with immersion test of 3.5 wt% of NaCl solution. Consequently, the surface contamination by sodium chloride with $16mg/m^2$, $48mg/m^2$ and $96mg/m^2$ didn't affect the adhesion strength for current epoxy coated carbon steel and blister and rust were not observed on the surface of epoxy coating contaminated by various concentration of sodium chloride after 20 weeks of immersion in 3.5 wt% NaCl aqueous solutions. In addition, the results of EIS test showed that the epoxy-coated carbon steel treated with steel grit blasting and power tool showed similar corrosion protection performance and surface cleanness such as Sa 3 and Sa 2.5 didn't affect the corrosion protectiveness of epoxy coated carbon steel.