• Title/Summary/Keyword: proficiency test

검색결과 290건 처리시간 0.024초

BTEX 분석용 토양 숙련도 표준시료(PTMs) 개발에 관한 연구 (A Study on the Development of Soil-based PTMs for Analysis of BTEX)

  • 이민효;이군택;이법열;이원석;김금희;홍석영
    • 한국지하수토양환경학회지:지하수토양환경
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    • 제18권5호
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    • pp.15-25
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    • 2013
  • In this study, two kinds of soil-based proficiency testing materials (PTMs), NICE-012L and NICE-012R were prepared and certified for Benzen, Toluene, Etylbenzene and Xylene with evaluation of uncertainties. In order to analyse BTEX (Benzen Toluene Etylbenzene Xylene) for the candidate materials, GC/MS was used after pretreatment according to methods of soil analysis by Ministry of Environment. For the homogeneity test among bottles in terms of candidate materials, ISO 13528 and IUPAC Protocol were used and according to the result, both candidate materials showed sufficient homogeneity. Also, the stability test over the candidate materials was accessed according to the ISO Guide 35 by classifying short-term and long-term stability and the result showed that both candidate materials showed decent stability. The reference values of the two candidate materials depending on BTEX components were derived from the average of the 11 samples that were used for verification of the samples' homogeneity. Uncertainty of measurement was combined by uchar that was caused by a characteristic value, $u_{bb}$ that was caused by between-bottle homogeneity, and $u_{stab}$ that was caused by stability, and then combined uncertainty ($u_{PTM}$) was multiplied to the coverage factor (k) derived from the effective degree of freedom from each factor that leads to expanded uncertainty (U) in about 95% of confidence level. The proficiency testing materials developed through this study were supplied to National Institute of Environmental Research (NIER) and utilized as an external proficiency testing materials for evaluating analysis capacity of soil agencies with specialty in terms of soil analysis approved by Minister of Environment.

경질유 유량표준장치의 신뢰도 검증을 위한 측정정확도 비교 (Intercomparison of Light Oil Flow Standard System for the Reliability of Measurement Accuracy)

  • 임기원
    • 대한기계학회논문집B
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    • 제32권9호
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    • pp.712-719
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    • 2008
  • Light Oil Flow Standard System(LOFSS), as a national oil flow standard system, in Korea Research Institute of Standards and Science(KRISS) was developed for oil flowmeter calibration, and the expanded uncertainty of flow quantity determination was estimated within 0.04 %. In order to improve the reliability of the LOFSS measurement, a proficiency test was carried out in the flow range of 20 and $240\;m^3/h$ (Reynolds number $20,000{\sim}900,000$). A turbine flowmeter was used as a transfer package in round robin test. The water flow standard system of KRISS, the pipe prover of the national calibration and test organization and the master meter calibrator of the turbine flowmeter supplier, which used the different working fluid respectively, were compared with the turbine flowmeter measurement. The maximum difference of measurement was 0.15 % between the LOFSS and the pipe prover. The En numbers of the each system measurement were evaluated at the same Reynolds number. It was found that the En numbers were less than 1 in the comparison, which means the procedures of the uncertainty estimation of the each calibrators were reasonable and reliable.

공학계열 대학생 물리 기초학력평가 문항분석 및 성취수준 설정 사례연구 (A Case Study on Item Analysis and Standard Setting of the Physics Basic Ability Test for Engineering College Students)

  • 이금호;정혜경
    • 공학교육연구
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    • 제26권6호
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    • pp.40-50
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    • 2023
  • This study is to examine the validity of assessing basic-level proficiency in physics among incoming engineering freshmen through item analysis and standard setting. For empirical analysis, we examined the physics subject taken by the freshman class of 2021 at K University, considering its significance for engineering students. In this study, we initially performed item analysis utilizing both classical test theory and item response theory. Subsequently, leveraging the item and test information, we employed a modified Angoff method and the Bookmark method for standard setting. Consequently, the difficulty level initially set during item development was found to be higher than the actual performance level exhibited by the students. This study highlights a discernible disparity between the expected university standard and the real proficiency level of incoming freshmen in terms of basic academic ability in physics. Based on these research findings, a comprehensive discussion on the fundamental academic competence of engineering students was conducted, underscoring the necessity for formulating a tailored learning approach leveraging the outcomes from the basic ability test.

한국인 학습자 영어 모음 발화의 음성학적 차이와 발음 이해도, 말하기 점수와의 관계 (The relation between phonetic differences of Korean learners' production of English vowels, pronunciation intelligibility and speaking proficiency test scores)

  • 김지은
    • 말소리와 음성과학
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    • 제9권2호
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    • pp.1-7
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    • 2017
  • The purpose of this study is to investigate the relations between phonetic differences among Korean learners' production of English front vowels, pronunciation intelligibility and speaking proficiency test score. To do so, thirty Korean university students were asked (1) to read English text book paragraphs and (2) describe a picture. Two English native raters and one Korean rater evaluated Korean subjects' English pronunciation intelligibility and speaking. In addition, subjects' English vowel productions were acoustically analyzed(F0, F1, F2, vowel duration, intensity). The results of the study show that the vowel quality and pitch of the unstressed vowels and lax vowel are related to the pronunciation intelligibility. In addition, the scores of pronunciation intelligibility and speaking are highly related.

A Study on the Development and Operation of Integrated Assessment System for National Competency Standard Professional Basic

  • Chang, Young-Hyun
    • International journal of advanced smart convergence
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    • 제7권4호
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    • pp.121-127
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    • 2018
  • This paper develops and builds an Integrated Assessment System for National Competency Standard Professional Basic. The integrated evaluation system for basic job competency in the National Competency Standards is developed to conduct examination by means of computers, smartphones and tablet PCs. The system can be used for the basic job competency test, examination for online cyber universities, job competency examination for enterprises, and the listening, reading, and speaking test in the foreign language proficiency examination and is even better in terms of facility investment and saved operating costs as well as efficient use of spaces in comparison with conventional evaluation schemes. Even greater synergy effects can be achieved by providing support for the integrated evaluation system for basic job competency in connection with the NCS qualification system. The evaluation system has been tested and practiced at a specialized high school and can be applied to the NCS education evaluation of the college and four-year college and to the selection examination of new employees of the company.

국내 공기 중 섬유상 분진 숙련도 시험용 표준시료 제조 및 평가 (Preparation and assessment of airborne fibrous reference sample for a proficiency test)

  • 임호주;유재혁;최성호;최아름;정현성;류정민;김현욱;장성기
    • 분석과학
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    • 제22권5호
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    • pp.369-375
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    • 2009
  • 저농도 섬유상 분진 표준시료를 제조하여 균질도와 정확성을 조사하고, 모의 숙련도 시험을 통해 최적의 숙련도 시험 방안을 평가하였다. 분석 결과 표준시료 농도와 석면밀도의 상관성이 0.9863~0.9968으로 매우 높게 나타났고, 표준시료를 이용한 모의 숙련도 시험을 통해서, 국내에서의 숙련도 시험 결과 평가 기준은 표준시료 분석결과의 Z값이 ${\mid}Z{\mid}{\leq}2$를 만족하는 것이 타당한 것으로 나타났다.

토마토 농약다성분분석 정도관리용 분석표준물질 개발 (Development of Analytical Reference Material for Proficiency Test of Pesticide Multi-residue Analysis in Tomato)

  • 김종환;오영곤;최성길;홍수명;김선배;우인덕;김준영;서종수
    • 한국환경농학회지
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    • 제35권3호
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    • pp.223-233
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    • 2016
  • BACKGROUND: This study was to develop a analytical reference material including twenty pesticides in tomato. To use it for proficiency test, the suitability of homogeneity, storage stability, assigned values and uncertainty for analytical reference material were important.METHODS AND RESULTS: In order to develop a analytical reference material of tomato for multi-residue analysis of pesticides, twenty-pesticides were treated in tomato and the samples were frozen and homogenized. The homogeneity, stability, assigned value and uncertainty were calculated according to the requirements of the KS A ISO Guide 35, KS Q ISO 13528 and EURL-PT protocol. The values of the within-bottle standard variation(swb) and the between-bottle standard variation(sbb) were 0.9~6.5% of assigned value and the uncertainty(u*bb) due to inhomogeneity was also calculated as 0.6~1.9% for all pesticides. This indicated that it was satisfactory to be used as a analytical reference material. The storage stabilities of twenty-pesticides at room temperature and freezing conditions were assessed according to the requirement of the KS Q ISO Guide 35. All pesticides were stable at room temperature (20~30℃) for 8 days and freezing (-20℃) for 23 days.CONCLUSION: The feasibility of analytical reference material for pesticide multi-residue analysis in a tomato matrix was investigated. Homogeneity of within/between-bottle, uncertainty and stabilities at room temperature and freezing condition were satisfactory for a use of proficiency test and quality control. From these results, a analytical reference material would be applicable to monitor the proficiency test of pesticide analysis organizations to improve the reliability and consistency.

정적 및 동적시험법과 실험자에 따른 점토의 액·소성한계 (Liquid and Plastic Limits of Cohesive Soil by Static and Dynamic Test Methods and Testers)

  • 김찬기;여진수;문영석;박형렬;김태형
    • 한국지반공학회논문집
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    • 제33권3호
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    • pp.5-15
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    • 2017
  • 본 연구는 파주점토에 대해 Casagrande법(동적)과 원추관입시험법(정적)으로 액성한계와 소성한계시험을 실시하여 실험방법과 실험자에 따른 액 소성한계 결정에 미치는 영향을 검토하였다. 총 6명의 실험경험을 가진 학생이 참여하였다. 액성한계시험결과, 원추관입시험법으로 구한 액성한계는 Casagrande법으로 구한 액성한계보다 약 4% 정도 작게 나타났다. 원추관입시험법에서 실험횟수의 증가함에 따라 비례적으로 실험자별 실험값의 차이가 작아지고, 숙련도의 변화 폭도 양호해지는 경향을 보였다. 1점법에서 원추콘관입시험법에 의해 결정된 액성한계 값의 변화는 작고 Casagrande법보다 좀 더 양호한 값을 얻을 수 있었다. 소성한계시험결과, 액성한계와는 다르게 두 시험법의 결과 차이는 없는 것으로 나타났다. 즉, 두 시험방법 모두 실험자별 소성한계는 실험횟수가 증가함에 따라 평균 소성한계 값에 근접해 가는 경향을 보이고 있으며 숙련도의 변화도 실험횟수가 증가 할수록 좋아 지는 경향을 보였다.

교사-학생간의 홈페이지를 활용한 자기주도적 학습의 효과 (The effects of self-directed learning through homepage for English reading class)

  • 방영주
    • 영어어문교육
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    • 제12권3호
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    • pp.187-210
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    • 2006
  • This study aims to investigate the effects of the implementation of self-directed learning through the homepage between the teacher and the students for English reading classes. The study focuses on the questions of whether the self-directed learning through the homepage, compared to the teacher-centered learning, would enable a significantly positive change in the students' achievements and of what their responses to this new learning method are. 72 students were grouped into an experimental and a control group, and then each group was subdivided into three levels (high, medium, low) of proficiency. Findings demonstrate that the experimental group showed statistically more significant increases in their scores of reading proficiency test than the control group. For the question of students' responses to the learning experience, the three groups within the experimental group responded to a questionnaire survey with regard to the positive attitude of learning, the effectiveness of self-directed learning and its learning materials, and usability of the homepage. In general, the experimental group considered the experience satisfactory, although the degree of positive responses varied according to the proficiency level of the group. This suggests the importance and effectiveness of self-directed learning using the computer and internet as a supplementary learning tool.

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