• Title/Summary/Keyword: primary matrix

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TEM Observation of Microstructure in Al-Sc alloys (투과전자현미경에 의한 Al-Sc합금의 미세구조 관찰)

  • 이영호;문정호;이갑호;이명현;서원선
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2003.11a
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    • pp.44-44
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    • 2003
  • Scandium을 소량 첨가한 Al합금은 용체화 처리 후 시효에 의해 강화되며, 합금의 주 강화상은 Ll2 type의 규칙구조를 갖는 A1$_3$Sc상으로 열처리시 아주 미세한 정합의 구형입자로 석출한다. Scandium은 Al합금에서 첨가원소의 at%에 따른 경량화 효과가 Gold 다음으로 크다. 현재까지의 Al-Sc계 합금에 대한 연구는 시효경화에 따른 기계적 특성 변화에 대해서만 이루어져 왔으나 본 연구에서는 투과전자현미경을 이용하여 열처리에 따른 미세조직의 변화, 급냉 상태에서 생성된 A13Sc입자의 형성 및 계면구조, 시효에 따른 석출거동을 규명하였다. 실험에 사용된 alloy는 미국의 Ashurst 사에서 제조된 Al-2wt%Sc모합금과 순도 99.9%의 Al을 혼합하여 Arc melting법으로 제조하였다. Primary A13Sc상은 Ll2 type으로 응고시에 용융상태에서 먼저 핵생성되어 Al의 핵생성 site로 작용한다. 635$^{\circ}C$에서 용체화 처리한 시편에서는 수백 nm 크기를 갖는 $Al_3$Sc상이 계면과 matrix내에 구형으로 존재함을 확인하였다. 수백 nm 크기의 $Al_3$Sc상의 내부에는 역위상 경계(Antiphase boundary)이 존재로 인한 특징적인 contrast가 관찰되었으며, 이 $Al_3$Sc상은 응고시 생성된 작은 $Al_3$Sc상들이 모여져 생성된 것으로 추측된다. 수백 nm 크기 의 $Al_3$Sc사와 Al matrix 사이의 계면에는 격자상수 차이에 의한 많은 edge dislocation들이 관찰된다.

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Precipitation Behaviors of HgTe Nanoinclusions Formed in Thermoelectric PbTe: Initial Induced Lattice Mismatch, Theoretical Calculation and Experimental Verification (PbTe 열전재료에 형성된 HgTe 나노개제물의 석출거동: 초기 격자 불일치의 형성, 이론적 계산 및 실험적 증명)

  • Kim, Kyung-Ho;Kwon, Tae-Hyung;Park, Su-Han;Ahn, Hyung-Keun;Lee, Man-Jong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.24 no.7
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    • pp.599-604
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    • 2011
  • A highly strained nanostructure comprising crystallographically aligned HgTe nanoinclusions and a surrounding PbTe matrix has been synthesized using a precipitation process of supersaturated HgTe-PbTe alloys. From the early precipitation stage, HgTe nanoinclusions take disk shape, which is transformed from initial HgTe nuclei, although there is no lattice constant difference of the two end components at standard state. As a primary reason for the morphological transformation of the initial spherical HgTe nuclei to HgTe nanodisks, the induced lattice mismatch is suggested. On the condition that the HgTe nanodisks maintain perfect coherent nature with PbTe matrix, the stress-free lattice constant of constrained HgTe nanodisks has been calculated based on the defined concept of the strain-induced tetragonality, the linear elasticity and the actual measurement in HRTEM images.

The Effect of Extrusion Temperatures on Microstructures and Mechanical Properties of Ultra-Fine Structured and Extruded Al81Si19 Alloys (초 미세조직 Al81Si19 합금분말 압출재의 미세조직과 기계적 성질에 미치는 압출온도의 영향)

  • 이태행;홍순직
    • Journal of Powder Materials
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    • v.10 no.5
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    • pp.325-332
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    • 2003
  • The effect of extrusion temperature on the microstructure and mechanical properties was studied in gas atomized TEX>$Al_{81}Si_{19}$ alloy powders and their extruded bars using SEM, tensile testing and wear testing. The Si particle size of He-gas atomized powder was about 200-800 nm. Each microstructure of the extruded bars with extrusion temperature (400, 450 and 50$0^{\circ}C$) showed a homogeneous distribution of primary Si and eutectic Si particles embedded in the Al matrix and the particle size varied from 0.1 to 5.5 ${\mu}m$. With increasing extrusion temperature from 40$0^{\circ}C$ to 50$0^{\circ}C$, the ultimate tensile strength (UTS) decreased from 282 to 236 ㎫ at 300 K and the specific wear increased at all sliding speeds due to the coarse microstructure. The fracture behavior of failure in tension testing and wear testing was also studied. The UTS of extrudate at 40$0^{\circ}C$ higher than that of 50$0^{\circ}C$ because more fine Si particles in Al matrix of extrudate at 40$0^{\circ}C$ prevented crack to propagate.

The Geometric Modeling for 3D Information of X-ray Inspection (3차원 정보 제공을 위한 X-선 검색장치의 기하학적 모델링)

  • Lee, Heung-Ho;Lee, Seung-Min
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.62 no.8
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    • pp.1151-1156
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    • 2013
  • In this study, to clearly establish the concept of a geometric modeling I apply for the concept of Pushbroom, limited to two-dimensional radiation Locator to provide a three-dimensional information purposes. Respect to the radiation scanner Pushbroom modeling techniques, geometric modeling method was presented introduced to extract three-dimensional information as long as the rotational component of the Gamma-Ray Linear Pushbroom Stereo System, introduced the two-dimensional and three-dimensional spatial information in the matching relation that can be induced. In addition, the pseudo-inverse matrix by using the conventional least-squares method, GCP(Ground Control Point) to demonstrate compliance by calculating the key parameters. Projection transformation matrix is calculated for obtaining three-dimensional information from two-dimensional information can be used as the primary relationship, and through the application of a radiation image matching technology will make it possible to extract three-dimensional information from two-dimensional X-ray imaging.

The Effect of a Long-Term Cyclic Strain on Human Dermal Fibroblasts Cultured in a Bioreactor on Chitosan-Based Scaffolds for the Development of Tissue Engineered Artificial Dermis

  • Lim, Sae-Hwan;Son, Young-Sook;Kim, Chun-Ho;Shin, Heung-Soo;Kim, Jong-Il
    • Macromolecular Research
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    • v.15 no.4
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    • pp.370-378
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    • 2007
  • Mechanical stimulation is known to activate several cellular signal transduction pathways, leading to the induction of signaling molecules and extracellular matrix (ECM) proteins, thereby modulating cellular activities, such as proliferation and survival. In this study, primary human dermal fibroblasts (HDFs) were seeded onto chitosan-based scaffolds, and then cultured for 3 weeks in a bioreactor under a cyclic strain of 1 Hz frequency. Compared to control samples cultured under static conditions, the application of a cyclic strain stimulated the proliferation of HDFs in I week, and by week 3 the thickness of the cell/scaffold composites increased 1.56 fold. Moreover, immunohistochemical staining of the culture media obtained from the cell/scaffold samples subjected to the cyclic strain, revealed increases in the expression and secretion of ECM proteins, such as fibronectin and collagen. These results suggest that the preconditioning of cell/scaffold composites with a cyclic strain may enhance the proliferation of HDFs, and even facilitate integration of the engineered artificial dermal tissue into the host graft site.

Hybrid Approach of Texture and Connected Component Methods for Text Extraction in Complex Images (복잡한 영상 내의 문자영역 추출을 위한 텍스춰와 연결성분 방법의 결합)

  • 정기철
    • Journal of the Institute of Electronics Engineers of Korea SP
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    • v.41 no.6
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    • pp.175-186
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    • 2004
  • We present a hybrid approach of texture-based method and connected component (CC)-based method for text extraction in complex images. Two primary methods, which are mainly utilized in this area, are sequentially merged for compensating for their weak points. An automatically constructed MLP-based texture classifier can increase recall rates for complex images with small amount of user intervention and without explicit feature extraction. CC-based filtering based on the shape information using NMF enhances the precision rate without affecting overall performance. As a result, a combination of texture and CC-based methods leads to not only robust but also efficient text extraction. We also enhance the processing speed by adopting appropriate region marking methods for each input image category.

The effect of aging on the Microstructure and Hardness of Stellite 12 alloy overlayer by PTA process (PTA법에 의한 스텔라이트 12합금 육성층의 미세조직 및 경도에 미치는 시효처리의 영향)

  • 정병호;김무길;이성열
    • Journal of Advanced Marine Engineering and Technology
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    • v.26 no.1
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    • pp.68-75
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    • 2002
  • Stellite 12 alloy-powders were overlaid on 410 stainless steel valve seat by plasma transferred arc(PTA)process. Variation of microstructure and hardness of overlaid deposit with aging time at $750^{\circ}C$ was investigated. The deposit showed hypoeutectic microstructure, which was consisting of primary cobalt dendrite and networked $M_{7}C_{3}$type eutectic carbides. After aging new M_{23}C_{6}$ carbide was formed by the partial decomposition of $M_7C_3$ type eutectic carbides and finely dispersed $M_{23}C_6$ type carbides were also precipitated in the matrix. Hardness of the deposit was increased with increase of aging time at $750^{\circ}C$ and showed maximum value at 35hours. After showing maximum value, it was fallen down again at 70hours because of overaging. The increase of hardness in aging is ascribed to the formation of new stable $M_{23}C_6$ type carbide by the partial decomposition of $M_7C_3$ type eutectic carbides and also precipitation of finely dispersed $M_{23}C_6$ carbides in matrix.

Microstructure of Tool Steel Castings for Cold-Work Die Inserts (냉간금형 인서트(insert)용 주강의 미세조직)

  • Kang, Jun-Yun;Park, Jun-Young;Kim, Hoyoung;Kim, Byunghwan
    • Journal of the Korean Society for Heat Treatment
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    • v.30 no.5
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    • pp.197-206
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    • 2017
  • The microstructure of a high-carbon and high-chromium cast steel (HK700) for cold-work die inserts was analyzed by advanced scanning electron microscopy. A continuous network of primary $M_7C_3$ carbide was developed among austenitic matrix after casting. A small amount of $M_2C$ was added to the carbide network owing to the enrichment of Mo and W during the solidification. After quenching in which the austenitization was performed at $1030^{\circ}C$ and double tempering at $520^{\circ}C$, the network structure of $M_7C_3$ was preserved while most of the matrix was transformed to martensite because of additional carbide precipitation. The $M_2C$ in the as-cast microstructure was also transformed to $M_6C$ due to its instability. The continuous network of coarse carbides owing to the absence of hot-working had little influence on the hardness after quenching and tempering, whereas it resulted in severe brittleness upon flexural loading.

A Study on the Generative Diagram in Guarino Guarini's Religious Buildings (구아리노 구아리니의 종교 건축에서 나타나는 생성 다이어그램에 관한 연구)

  • Kim, Hong-Su;Jung, In-Ha
    • Journal of architectural history
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    • v.14 no.4 s.44
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    • pp.157-175
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    • 2005
  • Guarino Guarini(1624-1683) is one of great Baroque architects who developed new spatial concept in architecture. He refused to static space typically appeared in Renaissance architecture. Instead, to make it possible to generate complicate form and moving space, he made use of generative diagram. It provide him with an abstract machine to generate automatically architectural inferiority. His generative diagram consists of three types: single circle diagram, matrix diagram and longitudinal diagram. The first diagram uses single circle as primary generator and develop this by means of overlap and equiangular division. La Cappella della Santissima Sindone, Sanctuary of Chiesa di Oropa, Chiesa dei Padri Somaschi, San Gaetano are designed according to this diagram. The generator of the second diagram is nine circles in $3{\times}3$ matrix, which provide the base for the interpenetration of space in Guarini's architecture. He inspired this diagram from Kepler's $\ulcorner$Harmonices mundi$\lrcorner$. The Churches of San Lorenzo, Ste-Anne-la-Royale, San Filippo Neri, San Gaetano are generated by this diagram. The third diagram has several circles in Lantin-cross plan. Guarini adopted this diagram because he had chances to design several churches in Northern Europe. The churches of Santa Maria di Ettinga, Immacolata Concezione, San Maria della Divina Providenza, Church without Name, San Filippo Neri are representative examples for this diagram.

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Minimum Row Weight and Polar Spectrum Based Puncture Polar Codes Construction Algorithm

  • Liu Daofu;Guo Rui
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • v.17 no.8
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    • pp.2157-2169
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    • 2023
  • In order to handle the problem that puncture patterns will change the position distribution of original information bits and frozen bits in polar codes, which affects performance of puncture polar codes further, a minimum row weight and polar spectrum based puncture polar codes construction algorithm (called PA-MRWP) is proposed in this paper. The algorithm calculates row weight of generator matrix and sorts the row weight in ascending order first. Next, the positions with the minimum row weight are selected as initial puncture positions. If the rows with the same row weight cannot all be punctured, polar spectrum based auxiliary puncture scheme is used. In sub-channels with the same row weight, rows corresponding to the polarized sub-channels with higher reliability are selected as puncture positions to construct puncture vector, and the reliability is calculated based on polar spectrum. It is actually a two-step selection strategy, the proposed minimum row weight puncture (MRWP) algorithm is used for primary selection and polar spectrum based auxiliary puncture is used for adjustment. Simulation results show that, compared with worst quality puncture (WQP) algorithm, the proposed PA-MRWP algorithm and Gaussian approximation-aided minimum row weight puncture (GA-MRWP) algorithm provide gains of about 0.46 dB and 0.29 dB at bit error rate (BER) of 10-4, respectively when code length N=400, code rate R=1/2. In addition, the proposed puncture algorithms improve the BER performance significantly with respect to quasi-uniform puncture (QUP) algorithm.