• Title/Summary/Keyword: preparation process

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Basic research for development of evaluation criteria for invention education program (발명교육 프로그램 평가준거 개발을 위한 기초 연구)

  • Lim, Byeong-ung;Choi, Wan-Sik
    • 대한공업교육학회지
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    • v.45 no.2
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    • pp.86-107
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    • 2020
  • The purpose of this study is to increase the effectiveness and efficiency of invention education by presenting basic evaluation criteria that can be used when designing and preparing invention education programs in various educational institutions that operate invention education. The results of this study are as follows. First, the stage of the Invention Education Program was named '4P stage' as 4 stages of 'Planning, Preparation, Process, and Product'. Second, the areas of evaluation of the planning stage of the invention education program are 'goal setting, demand analysis' and curriculum design. The preparatory stage evaluation area is 'Developing an Invention Education Program, Securing Human Resources, Securing Physical Resources'. The evaluation area of the course level is 'program operation, program management, learner management'. The evaluation area of the calculation stage is 'education performance, achievement results, and education evaluation'. Invention education program evaluation criteria will play a role to enhance and manage the quality of invention education program. In addition, it is judged that this will be the basic data for developing evaluation criteria for the invention education program through the reconciliation process through reflux and the validation process of related experts at various invention education institutions.

Peculiarities of ReBaCuO superconductor preparation

  • Fan, Zhanguo;Soh, Dea-Wha;Li, Ying-Mei;Park, Jung-Cheol;Korobova, N
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.913-916
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    • 2001
  • From 1994 the cooperation between NEU of China and MJU of South Korea for study of ReBaCuO (Re=Rare earth elements) superconductors has been carried out. The progress has been got in following projects. Critical current density ($J_c$) of YBaCuO superconductor prepared by Melting Textured Growth (MTG) was improved. In the preparation of textured YBaCuO, 20 wt.% of YBaCuO 211 phase was added, which would be climactic for the microcracks in the textured YBaCuO. The effects of the 211 phase and Ag content on the superconductivity were studied and discussed in detail. The improved $J_c$ value was reached to 8$\times$10^4 A/cm^2 (77K,0T). Single phase $YbBa_{2}Cu_{3}O_{x}$ superconductor was sintered by the traditional powder metallurgical method, and its reaction process was studied. In recent years, NdBaCuO superconductor is being performed. The behavior of $Nd_{4}Ba_{2}Cu_{2}O_{10}$(Nd422 phase) and the solid solubility, x in the superconductor $Nd_{1+x}Ba_{2-x}Cu_{3}O_{y}$ by the heat treatment in the low oxygen partial pressure (1%) or Ar at $950{\circ}C$ were investigated. The zone-melting process was used to make oriented NdBaCuO superconductor in order to increase the critical current density.

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Preparation and Adhesion Characteristics of Binary Blended Waterborne Polyurethane (이성분계 혼합 폴리우레탄 수분산체의 제조 및 접착 특성 연구)

  • Kim, Eun Ji;Park, In Kyu;Park, Jae Hyung
    • Journal of Adhesion and Interface
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    • v.19 no.1
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    • pp.5-12
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    • 2018
  • The purpose of this study is to evaluate the adhesive properties of polyurethane mixed aqueous dispersions by omitting the primer, dealing with the preparation of skins for synthetic leather with excellent adhesion by omitting the pre-treatment process. The two-component mixed polyurethane water dispersion was prepared by synthesizing an ester-based polyurethane resin (PU-T) and a carbonate-based polyurethane resin (PU-C) to obtain the final resin. As a result of measuring the peel strength of the adhesive specimens omitting the pre-treatment agent, it was confirmed that the state adhesive strength (ethylene vinyl acetate (middle): $4.2kg_f/cm$ and rubber (outsole): $4.4kg_f/cm$) there was. This makes it possible to omit the pre-treatment process which has been indispensably used in the shoe manufacturing process, thereby reducing the process time and reducing the amount of volatile organic compounds (VOCs) generated in the pre-treatment product, resulting in environmentally advantageous.

A STUDY OF WORKING EFFICIENCY AND FILE DEFORMATION OF GT ROTARY FILE IN CURVED CANALS (GT rotary file을 이용한 만곡 근관형성시 작업 효율 및 file 변형 발생에 관한 연구)

  • 신주희;백승호;배광식;임성삼;윤수한;김병현
    • Restorative Dentistry and Endodontics
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    • v.26 no.5
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    • pp.418-435
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    • 2001
  • Root canal preparation process is of utmost importance in successful treatment of root canal. Also, one of the most important purpose of the root canal preparation is to enlarge the root canal three dimensionally without changing the curvature of the root canal However as the curvature of the root canal increases, there are many difficulties involved in formation of optimum root canal. Therefore in order to solve the above mentioned problems, new developments in methods of root canal preparation and equipments for such purposes were made. Recently, vigorous studies about newly introduced engine-driven nickel-ti-tanium rotary file are conducted. As shown in research results to dates, it is well established that the use of nickel-titanium file is better suited for curved root canal than stainless steel file in maintaining the curvature or root canal and reducing the deformation of root canal. However it is also acknowledged that there are a few discrepancies in research results according to protocol, due to failure to remove variables in experiments. In addition, although it is recommended by the manufacturer that the GT rotary file should maintain a low rotational speed of 150~350rpm and 'light pressure' as light as not to break the lead of a pencil, academic studies about the vertical force which is not yet standardized are not sufficiently explored. Therefore, this research devised and utilized a special research equipment to standardize the appropriate range of vertical force for GT rotary file through experiments by breaking of the lead of a pencil as expressed by the manufacturer and to accurately measure factors involved through repeating and recreating the environment of root canal preparation. Forming nine experimental groups by varying the vertical forces (150g. 220g, 300g) and rpm (150rpm, 250rpm, 350rpm), the effects of changing vertical forces and rpm on working efficiency were measured in terms of time expended in root canal preparation by crown-down method using a transparent resin block with 35 degree curvature and GT rotary file (z-test). The following research using this special research equipment that involved nine experimental groups and varying the vertical force for root canal preparation from 300g which is within the normal vertical force range to 700g and 1000g which fall outside the normal rpm range. The results were as follows : 1. Analysis of the experiment results revealed that the time spent in root canal preparation decreased as the vertical forces and rpm increased (p<0.05). Also, the effects of rpm were greater than those of the vertical forces within the normal vertical force range ($\beta$-weight test). 2. Observation of the deformation of GT rotary file revealed that deformation increases in a direct correlation with the vertical force increase and in a reverse correlation with the rpm decrease. In the case of the vertical forces close to the normal range, the probability of GT rotary file deformation were quite different depending on the rpm changes. In the case of greater vertical forces, the occurrences of deformation of the file were more frequent regardless of the rpm changes. 3. Deformation and breakage of file were also commonly observed in the expended time measurement experiments and GT rotary file deformation experiments in which low speed rpm (150rpm) was used and at the curved portion of the resin block.

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Preparation and Characterization of Porous Silicon and Carbon Composite as an Anode Material for Lithium Rechargeable Batteries

  • Park, Junsoo;Lee, Jae-Won
    • Journal of Powder Materials
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    • v.22 no.1
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    • pp.15-20
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    • 2015
  • The composite of porous silicon (Si) and amorphous carbon (C) is prepared by pyrolysis of a nano-porous Si + pitch mixture. The nano-porous Si is prepared by mechanical milling of magnesium powder with silicon monoxide (SiO) followed by removal of MgO with hydrochloric acid (etching process). The Brunauer-Emmett-Teller (BET) surface area of porous Si ($64.52m^2g^{-1}$) is much higher than that before etching Si/MgO ($4.28m^2g^{-1}$) which indicates pores are formed in Si after the etching process. Cycling stability is examined for the nano-porous Si + C composite and the result is compared with the composite of nonporous Si + C. The capacity retention of the former composite is 59.6% after 50 charge/discharge cycles while the latter shows only 28.0%. The pores of Si formed after the etching process is believed to accommodate large volumetric change of Si during charging and discharging process.

Transparent Conducting Film for Flat Panel Display using CNT by Electrospinning

  • Moon, Jin-San;Park, Jae-Hong;Han, Jae-Hee;Berdinsky, Alexander S.;Nam, Jae-Do;Lee, Dae-Hoi;Yoo, Ji-Beom
    • 한국정보디스플레이학회:학술대회논문집
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    • 2004.08a
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    • pp.978-980
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    • 2004
  • We report the preparation and properties of polymer paste solutions with CNTs using conventional paste forming process. Electrospinning has been used for the fabrication of nano-fiber composite. In this process, dispersion of CNTs is very important matter. So, we emphasize the necessity of dispersion of CNTs in the solution and investigate effects of process parameters of electrospinning. The advantage of simple electrospinning process will be discussed..

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Novel route of enhancing the metal loading in highly active Pt/C electro-catalyst by polyol process (Polyol process를 통한 고비율 백금 담지 촉매 합성)

  • Oh, Hyung-Suk;Kim, Han-Sung
    • 한국신재생에너지학회:학술대회논문집
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    • 2008.05a
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    • pp.560-563
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    • 2008
  • A modified polyol process is developed to enhance Pt loading during the preparation of Pt/C catalysts. With the help of the zeta potential, the effect of pH on the electrostatic forces between the support and the Pt colloid is investigated. It is shown experimentally that the surface charge on the carbon support becomes more electropositive when the solution pH is changed from alkaline to acidic. However, this change does not affect the electronegative surface charge of Pt colloids already attained and stabilized by glycolate anions. This new behavior caused by the change in the solution pH accounts for the enhanced yield of the process and does not affect the Pt particle size. All our experimental results reveal that this simple modification is a cost effective method for the synthesis of highly Pt loaded Pt/C catalysts for fuel cells.

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Synthesis of Cu/Al2O3 Nanostructured Composite Powders for Electrode Application by Thermochemical Process (열화학적 방법에 의한 전극용 나노 Cu/Al2O3 복합분말 합성)

  • 이동원;배정현;김병기
    • Journal of Powder Materials
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    • v.10 no.5
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    • pp.337-343
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    • 2003
  • Nanostructured Cu-$Al_2O_3$ composite powders were synthesized by thermochemical process. The synthesis procedures are 1) preparation of precursor powder by spray drying of solution made from water-soluble copper and aluminum nitrates, 2) air heat treatments to evaporate volatile components in the precursor powder and synthesis of nano-structured CuO + $Al_2O_3$, and 3) CuO reduction by hydrogen into pure Cu. The suggested procedures stimulated the formation of the gamma-$Al_2O_3$, and different alumina formation behaviors appeared with various heat treating temperatures. The mean particle size of the final Cu/$Al_2O_3$ composite powders produced was 20 nm, and the electrical conductivity and hardness in the hot-extruded bulk were competitive with Cu/$Al_2O_3$ composite by the conventional internal oxidation process.

A Study on the Preparation of the Fly ash Adhesion-Activated Carbon and on the Removal of Heavy Metals (석탄회부착활성탄의 제조 및 중금속 제거에 관한 연구)

  • 문옥란;신대윤;고춘남
    • Journal of environmental and Sanitary engineering
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    • v.14 no.4
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    • pp.1-8
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    • 1999
  • This study was aimed ultimately to develop an adsorption process treating heavy metal wastewater by utilizing activated carbon using flyash. The affecting factors in adsorption process on heavy metal by flyash adhesion-activated carbon are s follows. Factors such as pH, and quality of activated carbon, and reaction time made batch adsorption isotherm described adsorption capacity was made use of the investigation to evaluate adsorptive possibility of heavy metal.As the results of this study, H ion has influence on adsorption of heavy metal if pH is low. As reaction time is transformed, factors such as optimum reaction time is taken into consideration an adsorptive process of heavy metal because an adsorption and a reduction process occur. Adsorption isotherm of adhesion-activated carbon was generally obeyed to Freundlich formular than Langmuir formular and Freundlich constant, l/n were obtained in the range of 0.1~0.5.

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