• 펄프종이기술
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• 제42권5호
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• pp.67-73
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• 2010

Paper packaging materials are essential in protection and transportation of commercial or industrial products. Raw materials for packaging paper production are mainly obtained from various grades of waste paper. For this reason, the recycled fibers from waste paper would probably have possibility of containing heavy metals. This study was focused on the development of optimum pre-treatment method for the quantitative analysis of mercury. The optimum pre-treatment for open digestion system were obtained at the treatment conditions of acid combination with $HNO_3/HCl/H_2O_2$ or $HNO_3/H_2SO_4$ at $80^{\circ}C$. The optimum pre-treatment conditions in closed digestion system were determinated by the acid combination with $HNO_3/HCl/H_2O_2/HF$ in microwave at 320 W for 20 min. The recovery rate in open digestion system was 85~94% and in closed digestion system was indicated as about 100%. Therefore, the closed system is superior than the open system in pre-treatment method for the quantitative analysis of mercury, and the detected mercury contents in the sample of KOCC, AOCC and kraft sack paper were measured below 1 ppm.

• Korean Chemical Engineering Research
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• 제52권4호
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• pp.413-424
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• 2014

에너지원으로 바이오가스에 대한 잠재적 가능성이 인식되면서 최근에 바이오가스의 생산기술을 제고하고 에너지 효율을 개선하기 위한 기술개발이 지속적으로 진행되고 있다. 본 논문의 목적은 혐기성 소화 과정에서 바이오가스 생산을 증가시키기 위한 효과적이고 효율적인 슬러지 전처리 방법에 대하여 분석하였다. 이를 위해 본 논문에서는 각각의 전처리 방법의 장점과 단점을 분석하여 바이오가스 생산에 미치는 영향요인을 비교 분석하였다.

• Journal of Radiation Protection and Research
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• 제40권2호
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• pp.101-109
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• 2015

대기 중에 존재하는 우라늄 동위원소 분석을 위해서 일반적으로 알파분광분석법(alpha spectrometry)이 사용되고 있으며, 정확한 분석을 위해서는 정밀한 방사화학 전처리가 요구된다. 보편적인 방사화학 전처리 방법으로는 회화법(ashing method) 및 알칼리 용융법(alkali fusion method)가 있다. 그러나 회화법의 경우 전처리 시간이 길어 빠른 분석이 어렵다는 단점이 있으며, 이와 달리 알칼리 용융법은 단시간 내에 전처리가 가능하다는 장점은 있으나 보편적으로 전처리 장비의 무게가 무겁고 분석 소요 비용 역시 상당히 높다는 단점이 있다. 이러한 단점들은 신속한 분석 결과가 요구되는 방사능 사고 분석 또는 IAEA 안전조치 물자재고 검사(Physical Inventory Verification, PIV) 수행시, 효율성을 저하시키는 원인이 된다. 이에 본 연구에서는 간편하면서도 주어진 짧은 시간 내에 공기 중 우라늄 동위원소 분석을 완료하는 것을 목적으로, 초음파 세척법(ultrasonic cleaning method)을 이용한 새로운 방사화학 전처리 방법을 개발하였다. 또한 초음파 세척법의 효율성 분석을 위해 전처리 소요시간, 편의성, 소요비용, 우라늄 동위원소 회수율의 측면에서 기존의 방법들과 비교 분석하였다. 동일 조건의 공기 포집시료에 대해 비교실험을 수행한 결과, 본 연구에서 개발한 초음파 세척법을 활용한 공정은 상대적으로 전처리 시간도 짧고, 이동이 간편하며, 저가이며, 단순함에도 불구하고 기존 방식과 비교하여 유사한 회수율을 보였다.

• 상하수도학회지
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• 제10권2호
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• pp.104-116
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• 1996

Anaerobic digestion is generally used for the treatment of volatile organic solids such as manure and sludge from waste water treatment plants. However, the reaction rate of anaerobic process is slow, and thus it requires a large reactor volume. To minimize such a disadvantage, physical and chemical pre-treatment is generally considered. Another method to reduce the reactor size is to adopt different reactor system other than CSTR. In this paper, the effects of heat pre-treatment and reactor configurations on the anaerobic treatability of volatile solids was studied. Carrot, kale, primary sludge, and waste activated sludge was chosen as the test materials, and the BMP method was used to evaluate the maximum methane production and first order rate constants from each sample. After the heat treatment at $130^{\circ}C$ for 30min., the measured increase in SCOD per gram VS was up to 394 mg/L for the waste activated sludge. However, the methane production potential per gram VS was increased for only primary and waste activated sludge by 17-23%, remaining the same for carrot and kale. The overall methane production process for the tested solids can be described by first order reactions. The increased in reaction constant after heat pre-treatment was also more significant for the primary and waste activated sludge than that for carrot and kale. therefore, the heat pre-treatment appeared to be effective for the solids with high protein contents rather than for the solids with high carbohydrate contents. Among the four reactor systems studied, CSTR, PFR, CSTR followed by PFR, and PFR with recycle, CSTR followed by PFR appeared to be the best choice considering methane conversion rate and the operational stability.

• The Journal of Korean Physical Therapy
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• 제11권1호
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• pp.71-77
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• 1999

The purpose of this study was to investigate the changes of muscle power by transcutaneous electrical nerve stimulation(TBNS), low frequency-low intensity(20pps, invisible muscle contraction intensity), low frequency-high intensity(20pps, visible muscle contraction), high frequency-low intensity(100pps, invisible muscle contraction intensity) and high frequency-high intensity(100pps, visible muscle contraction). The results were as follows. 1. Increased muscle power after 30 minutes of treatment by low frequency-low intensity TENS, and post-treatment 30 minutes muscle power were increased more than pre-treatment power(p<0.05). 2. Decreased muscle power after a 30 minute treatment by low frequency-high intensity TENS, and after the 30 minute treatment was terminated muscle power didn't recover to pre-treatment levels. 3. Decreased muscle power after 30 minute treatment by high frequency-low intensity TENS, but post-treatment 30 minute, muscle power didn't recover to pre-treatment levels. 4. The muscle power was remarkably decreased by high frequency-high intensity TENS after 30 minute treatment, in addition treatment terminated after 30minutes didn,t recover to pre-treatment power(p<0.05). 5. Lower frequency-low intensity TENS are good methods for preventing muscle fatigue, buty high intensity (TENS) are increased muscle fatigue. 6. Traditional TENS by high frequency-low intensity is a good method for preventing muscle fatigue.

• 유기물자원화
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• 제21권3호
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• pp.43-52
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• 2013

본 연구에서는 유입 슬러지에 다양한 전처리 방법을 적용하여 전처리 방법이 중온혐기-고온호기 복합 슬러지 처리 공정의 슬러지 소화효율과 메탄가스 생성량에 미치는 영향을 비교 검증하였다. 실험실 규모의 슬러지 소화장치를 제작하여 서로 다른 유입 슬러지 전처리방법을 적용하여 4단계로 실험을 진행하였다. 1단계에서는 전처리를 하지 않은 슬러지를 공급하였고, 2, 3, 4단계에서는 각각 열처리, 열-알칼리처리, 장기 알칼리 처리(7일)를 거친 유입 슬러지를 공급하였다. 실험 결과, 1단계에서 4단계까지 진행되는 동안 총COD 제거율은 44%에서 76%까지 증가하였으며, 메탄 생성량 또한 101mL/L/day에서 165, 256mL/L/day까지 크게 증가하였다. 한편, 4단계에서는 7일간의 장기 알칼리 처리를 하였음에도 불구하고 3단계에 비해 총COD 제거율과 메탄 생성량이 증가하지 않았다. 결론적으로, 유입 슬러지의 전처리를 통해 복합 슬러지 처리 공정의 슬러지 제거 효율과 메탄생성량을 크게 증가시킬 수 있었으며, 여러 가지 전처리 방법 중 열-알칼리 처리법이 가장 효율적임을 실험결과를 통해 알 수 있었다.

• 분석과학
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• 제35권3호
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• pp.129-135
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• 2022

본 연구는 alumina, leucine, alumina와 leucine을 9:1로 혼합한 분말(이하 Al-Leu (9:1)), alumina와 leucine을 5:1로 혼합한 분말(이하 Al-Leu (5:1)), alumina와 sodium lactate를 5:1로 혼합한 분말(이하 Al-Lac (5:1))을 자연상태 시료지문을 남긴 후 1, 7, 14, 30일로 노화시킨 잠재지문에 전처리한 후 cyanoacrylate fuming(이하 CA 훈증법)으로 현출 증강을 시도하였다. 전체적으로 미처리한 후 CA 훈증한 잠재지문보다 alumina, leucine, Al-Leu (9:1), Al-Leu (5:1), Al-Lac (5:1) 분말로 전처리한 잠재지문의 면적값과 특징점 개수가 향상되었다. 따라서 5종류의 개시제가 CA 훈증 시 현출 증강을 향상시키는 것을 확인하였다.

• 한국식품저장유통학회지
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• 제6권1호
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• pp.1-6
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• 1999

Fresh gingers, harvested in Seosan, Choongcheongnam-do, were pre-treated by a washing-pasteurizing-drying process, a curing process, and non-treated, respectively. Then they were stored in a lab-scale storage room(12$^{\circ}C$, >92%RH) to investigate the effect of pre-treatment methods on the quality changes during long-term storage. Weight loss of ginger during storage showed ranges in 0.7∼4.3%, and the weight of gingers pre-treated by washing-drying process showed a tendency to change less than those treated by curing. After storage of 130 days, spoilage rates were about 20% in non-treated, 11% in curing treated, and 12% in washing-drying treated ginger,, showing the effect of pre-treatment. The final rate of sprouting was 13∼15% regardless of treatment methods. The firmness of gingers showed a tendency to decrease in stored ginger for the longer period; however, the values were ranged from 1,200 to 1,400 g/$\textrm{cm}^2$, that is hard enough to show a marketable quality. The contents of reducing sugar showed a tendency to increase with the lapse of storage time.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1999년도 하계학술대회 논문집 G
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• pp.3313-3315
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• 1999

Si direct bonding(SDB) technology is very attractive for both Si-on-insulator(SOI) electric devices and MEMS applications because of its stress free structure and stability. This paper presents on pre-bonding according to HF pre-treatment conditions in Si wafer direct bonding. The characteristics of bonded sample were measured under different bonding conditions of HF concentration, and applied pressure. The bonding strength was evaluated by tensile strength method. The bonded interface and the void were analyzed by using SEM and IR camera respectively. A bond characteristic on the interface was analyzed by using IT- IR. Si-F bonds on Si surface after HF pre-treatment are replaced by Si-OH during a DI water rinse. Consequently, hydrophobic wafer was bonded by hydrogen bonding of Si $OH{\cdots}(HOH{\cdots}HOH{\cdots}HOH){\cdots}OH-Si$. The bond strength depends on the HF pre-treatment condition before pre- bonding (Min:$2.4kgf/crn^2{\sim}Max:14.9kgf/crn^2$)

• Journal of Applied Biological Chemistry
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• 제56권3호
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• pp.171-177
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• 2013

Efficient extraction of total proteins from soil microorganisms is tedious because of small quantity. In this regard, an improved method for extraction of whole cell proteins is developed from soil microorganisms, Saccharomyces cerevisiae and Pichia pastoris. of which the cell wall are very strong. Pretreatment with NH4OH prior to the final extraction using NaOH/SDS was tried under the basis that ammonium ion was possible to enhance the permeability and/or to weaken the yeast cell walls. The pre-treatment of yeast cells with NH4OH drastically enhanced the protein extraction when it was compared with control (without NH4OH pre-treatment). At the pre-treatment of 0.04 N NH4OH at pH 9.0, about 3 fold of proteins was obtained from p. pastoris. Ammonium hydroxide appears to penetrate into the yeast cell walls more readily at basic pH. The effect of NH4OH pretreatment was pH dependent. The methods developed in this experiment might be applicable for an effective extraction of yeast proteins for the purpose of biochemical studies, especially proteomic analysis.