• Journal of the Speleological Society of Korea
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• no.78
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• pp.23-27
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• 2007

In this paper, we have investigated the characteristics of the magnetic abrasive using sludge on polishing of internal finishing of seamless stainless steel tube applying magnetic abrasive polishing. Either white alumina grain was used to resin sludge at a low temperature, and the sludge of magnetic abrasive powder was synthesized and crushed into 200 meshes. Surface roughness was measured before and after polishing, and more than 40% of improvement of surface roughness was achieved when grain was used under a specific condition. Even though some degree of surface roughness due to deeper scratches still exist, but the result showed a prospective magnetic abrasive polishing using sludge with white alumina grains.

• Journal of the Korean Ceramic Society
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• v.13 no.1
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• pp.25-29
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• 1976

The properties vary with quality of ferric-oxide that is major material of ferrites. In this point of view, a manufacturing method of pure and homogeneous fine ferric oxide is very important. The characters of this study are as follows: 1) Ferric oxide was made from waste pickling liquor of steel. 2) The crude ferric-oxide that is made by roasting the pickling liquor was dissolved in 20% HCI solution and then produced ferric chloride is purified by ethyl ether extraction. 3) The methanol solution of purified ferric chloride was sprayed into the refractory tube with compressed air and propane gas and then ignited leading to the ferric-oxide powder. 4) The produced oxide powder was introduced to the scrubber type vessel throught cooling system in order to collect the powder. 5) Crystalline phase of the powder was identified by X-ray diffraction and particle size, crystalline shape of the powder were investigated by settling method and electron microscope and the effects of concentration of ferric chloride in methanol on grain size were discussed. Results were obtained as fellows: 1) Total impurity in the ferric oxide produced from waste pickling liquor was 3.7%. 2) The solubilityof crude ferric oxide that was made from waste pickling liquor in HCI solution increased with the HCI concentration and reached to saturation range at 15% HCI concentration. 3) Extraction of FeCl3 increased with HCI concentration which is solvent. 4) Alpha ferric oxide obtained was very fine crystalline particles, the mean crystalline grain increased with the concentration of ferric chloride, and mean grain size distributed from 3.5$\mu$(at 0.5mole/l) to 0.5$\mu$(at 0.05mole/l).

• Progress in Superconductivity
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• v.10 no.2
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• pp.79-86
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• 2009

We successfully fabricated C-doped ex-situ $MgB_2$ wires using two different methods such as mechanical alloying(MA) and combined process(CP) of in-situ and ex-situ. In the MA, the precursor powder was prepared with a mixture of $MgB_2$ and 1 at% C powders by planetary ball milling for 0-100 h. In the CP, on the other hand, C-doped $MgB_2$ powder was prepared with Mg, B, and C powders by in-situ process via compaction, sintering, and crushing. The powders prepared by two methods were loaded into Fe tube and then the assemblages were drawn by a conventional powder-in-tube technique. The MA treatment of C-added $MgB_2$ decreased the particles/grains size and resulted in C-doping into $MgB_2$ after sintering, improving the critical current density($J_c$) in high external magnetic field. For the C-doped $MgB_2$ wire by MA for 25 h, the $J_c$ was $4.1{\times}10^3A/cm^2$ at 5 K and 6.4 T, which was 5.9 times higher than that of pure and untreated $MgB_2$ wire. The CP also provided C-doping into $MgB_2$ and improved the $J_c$ in high magnetic field; the C-doped $MgB_2$ wire fabricated by CP exhibited a $J_c$ being 2.3 times higher than that of the ex-situ wire used commercial $MgB_2$ powder at 5 K and 6.0 T($2.7{\times}10^3A/cm^2\;vs.\;1.2{\times}10^3A/cm^2$).

• Proceedings of the Materials Research Society of Korea Conference
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• 2009.11a
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• pp.27.2-27.2
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• 2009

Grinding characteristics for aluminium and carbon nanotubes (CNTs) powder during traditional and planetary ball milling investigated from the viewpoint of particle behaviour with the aimat developing CNT-dispersed samples ground based on powder metallurgy routes.In this work, a comparison between the pure aluminium and CNT input aluminium grinding was carried out to determine grinding time effect on size reduction.We observed that the use of the curly small-diameter multi-walled carbon nanotubes (MWCNTs) attributed to the beneficial role of the MWCNTs as grinding aids. It is suggested that careful choices of the sizes of CNTs and Al powders would allow fine-grinding of composite particles with uniformly distributed CNT reinforcements thereby ensuring improved properties of the final composites produced by low-temperature compacting.

• Superconductivity and Cryogenics
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• v.6 no.2
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• pp.42-46
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• 2004

금속 테이프 위에 초전도층을 박막형태로 증착시켜서 제조되는 고온초전도 선재인 coated conductor (CC)는 powder-in-tube 공정으로 제조되는 1세대 고온초전도 선재에 비해 액체 질소 온도에서 높은 임계 전류 밀도와 우수한 자장 특성을 가지면서 더 경제적으로 제조 가능하기 때문에 액체질소온도에서 작동 가능한 초전도전력기기 개발에 반드시 필요한 부분으로 인식되고 있다. 최근 국내외적으로 다양한 증착 방법을 사용하여 전력기기 응용이 가능한 장선의 CC 제조공정을 개발하려는 연구가 활발히 진행되고 있다. 특히 외국의 경우 이미 CC 선재의 상업화를 위해 기업체가 중심이 되어 집중적인 연구 개발이 이루어지고 있다.(중략)

• Journal of the Speleological Society of Korea
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• no.82
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• pp.8-12
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• 2007

In this paper, we have investigated the characteristics of the magnetic abrasive using sludge on polishing of internal finishing of seamless stainless steel tube applying magnetic abrasive polishing. Either green carborundum(GC) grain was used to resin sludge at a low temperature, and the sludge of magnetic abrasive powder was synthesized and crushed into 200 meshes. Surface roughness was measured before and after polishing, and more than 38% of improvement of surface roughness was achieved when grain was used under a specific condition. Even though some degree of surface roughness due to deeper scratches still exist, but the result showed a prospective magnetic abrasive polishing using sludge with green carborundum grains.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1993.11a
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• pp.43-46
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• 1993

Superconducting cable (Ic: 60 A at 77K. 10 filaments) with Bi high-Tc superconducting system was developed by powder - in - tube method. Pressing and sintering process of the cables were repeated for growth of 2223 high-Tc superconducting phase. The cable can be fabricate by twist method that is nessary for high current density and cooled circulative system. This cab1e system can be used for commercial.

• 전기의세계
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• v.53 no.8
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• pp.39-42
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• 2004

초전도 재료는 선재의 형태로 가공하면 송전선이나, 변압기, 발전기 및 전력 저장장치와 같이 전력 응용의 효율을 극대화시킬 수 있는 재료로서 널리 활용되고 있다. 1987년 개발된 고온 산화물 초전도체는 액체질소 의 비등점인 77K 이상에서 초전도 현상을 나타내어 초전도 현상의 응용에 대한 기대를 고조시켜 이에 대한 연구 개발을 더욱 향상시키고 있다. 초전도 선재에 관한 연구는 주로 PIT( Powder in Tube )공정을 이용한 Ag/Bi 2223 선재가 우수한 전기적 특성과 가공의 우수성으로 인하여 개발되어 왔다. 그러나 Ag/Bi 2223 선재는 강한 자기장 하에서 통전 특성이 현저하게 저하되는 결점이 있다. (중략)

• Progress in Superconductivity
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• v.7 no.1
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• pp.97-101
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• 2005

Bi-22l2 tubes for fault current limiter (FCL) were fabricated by centrifugal melting process. $SrSO_4$ ($10\;wt.\;\%$) was added to Bi-2212 powder to lower the melting point of Bi-22l2 and to improve the mechanical properties. The BSCCO powder was completely melted at $1300\;^{\circ}C$ using the RF furnace and then poured into rotating steel mold. The steel mold, preheated at $450\;{\circ}C{\sim}550^{\circ}C$ for 2 hour was rotated at $1020{\sim}2520\;RPM$. The solidified BSCCO tube was cooled down to room temperature in the furnace for 48 hours and separated from the mold between Bi-2212 and the mold. $ZrO_2$ solution was used to separate it easily from the mold and Ag tape was attached in the mold inner wall of the mold to analysis electrical property. Bi-22l2 tube was often cracked when the cooling rate was high. BSCCO tubes with $70{\Phi}{\times}100\;mm,\;50{\Phi}{\times}100\;mm$ and $30{\Phi}{\times}150\;mm$ size were fabricated by centrifugal melting process. The $J_{c}s$ of tubes with $50{\Phi}{\times}100\;mm{\times}4.0\;t$ and $50{\Phi}{\times}100\;mm{\times}4.l\;t$ were 178 and $74.2\;A/cm^2$ at 77K, respectively. The processing condition for Bi-2212 tube fabrication was investigated using XRD and SEM analyses.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.21 no.9
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• pp.795-800
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• 2008

A sublimation method using the SiC seed crystal and SiC powder as the source material is commonly adopted to grow SiC bulk single crystal. However, it has proved to be difficult to achieve the high quality crystal and the process reliability because SiC single crystal should be grown at very high temperature in closed system. The present research was focused to improve SiC crystal quality grown by PVT method through using the new inner guide tube. The new inner guide tube was designed to prevent the enlargement of polycrystalline region into single crystalline region and to enlarge the diameter of SiC single crystal. The 6H-SiC crystals were grown by conventional PVT process. The seed adhered on seed holder and the high purity SiC source materials are placed on opposite side in sealed graphite crucible surrounded by graphite insulation. The SiC bulk growth was conducted around 2300 $^{\circ}C$ of growth temperature and 50 mbar in an argon atmosphere of growth pressure. The axial thermal gradient across the SiC crystal during the growth was estimated in the range of 15${\sim}$20 $^{\circ}C$/cm.