• Journal of Conservation Science
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• v.33 no.6
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• pp.417-429
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• 2017

This study aimed at the identification of the black coating materials on the pottery surface and manufacturing technique of black burnished pottery excavated from the Pungnaptoseong, Seoul, which is estimated to be royal fortress of Beakje. According to observation of black coated surface and raw materials, potteries can be divided into two groups. The first group potteries have black inner and black surface with well-selected particles. Second group potteries are black in surface only with unevenly selected particles. Each group seems to represent different manufacturing technique in clay selection, color development timing and method. The black burnished pottery contains high values of CaO, $P_2O_5$, L.O.I. and lower content of $Fe_2O_3$ compared with gray pottery excavated from the same site, which indicates plant ashes were used for coloring the surface of pottery in black. According to the result of SEM-EDS mapping of black burnished pottery, carbon was concentrated on pottery surface, while iron was concentrated on the surface of the gray pottery. Based on XRD analysis, firing temperature of the black burnished potteries were fired low temperature range at 700 to $900^{\circ}C$, and that of the gray potteries ranged from $900^{\circ}C$ to $1000^{\circ}C$.

• Journal of Conservation Science
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• v.29 no.2
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• pp.171-185
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• 2013

The purpose of this study were to interpret making characteristics and clay sources for Proto-Three Kingdoms period potteries which were excavated from Bakjimeure site in Tangjeong, Asan, Korea, on the basis of shape types. The pottery samples of the studied included deep bowl pottery, cylinder shaped pottery, duck shaped pottery and rounded based jar with short neck. And the last jar was dominant among them. This is supported in nearby Yongduri Jinter site, Galmaeri site and Baekseokdong site. They vary in terms of color of clay, absorption ratio and mineral classification. Based on the fact that their absorption ratio range was 4.50 to 25.19% and firing temperature range was 850 to $1,150^{\circ}C$, they were thought to be widely used. The equivalence of cylinder shaped pottery, duck shaped pottery and deep bowl pottery was high in terms of material characteristics and their firing temperature range was 850 to $950^{\circ}C$. However, the deep bowl pottery, compared to other pottery shapes, contained great amount of coarse grained quartz and feldspar, and was different from others in terms of function. For soil sample collected from relative plains (area 3) in the southernmost part of the site, their mineralogical and geochemical characteristics were the most similar to those of the potteries excavated from the Bakjimeure site and even most of the potteries collected from different sites.

• Analytical Science and Technology
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• v.13 no.4
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• pp.403-411
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• 2000

This study described a method of thermoluminescence dating of pottery shards using subtraction method. TL measurement was achieved using two different types of samples prepared by quartz inclusion method and fine-grain technique. Fine grains (size range: $5-10{\mu}m$) were separated by suspending grounded pottery samples into acetone solution and sedimentation quantitatively. In quartz inclusion method quartz grains in the size range of 90 to $125{\mu}m$ diameter were obtained by extracting the quartz crystals embed in the pottery shards and etching them with 1.0 M HF solutions. The archaeological dose of both the quartz and fine grains was determined from the dose calibration curves obtained from sequential irradiation of $^{137}Cs$ gamma and $^{241}Am$ alpha source to the samples and TL measurement of natural samples, in which the alpha dose of 4.60 Gy for the Packjae pottery was obtained using subtraction method. Annual alpha dose rates ($3.05{\pm}0.11$ mGy/yr.) were determined by the analysis of U, Th contents in the pottery shards and evaluation of the values with Bell's equation. Dividing the alpha dose accumulated in the pottery shards by the annual alpha dose rate, we found age of approximately $1508{\pm}80$ years B.P. (AD. ca. 492 yr.) for the Packjae pottery. It matches well with the archeological age estimate (middle of 5th century) within 10 percent uncertainty and thereby conforms the age of the pottery sample.

• The Journal of Engineering Geology
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• v.32 no.4
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• pp.685-696
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• 2022

Although the use of pottery-making soils has a long history, its use in the pottery industry requires that physical and geotechnical properties of the materials be established to define the suitability for various purposes. The main purpose of this study is to identify the different types of clays and mineral composition and to perform the geotechnical evaluation of the clays for making pottery products. Soils investigated in this study include raw materials used for making Baekja (white porcelains), Chungja (celadons), Buncheong, Sancheong, and Johyung. Pottery-making soils are manufactured by using different types of soils and sold by individual ceramic clay company. This study includes physical tests of soil and chemical analysis of major elements using XRF and XRD instrumentation. Grain size distributions, mineralogical composition, and a range of plasticities of soils for making different types of potteries are presented. Correlations between specific type of pottery clays and geotechnical and mineralogical characteristics are determined by comparing the test results. Since quantitative research using laboratory tests for pottery-making soils are rarely performed in Korea, further research should be done in the future to improve the Korean pottery industry.

• Journal of environmental and Sanitary engineering
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• v.15 no.1
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• pp.62-68
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• 2000

This study was investigated to the recovery of alumina from the first calcined waste pottery using alkaline sintering. This study was based on calcination result of a commercial ${\alpha}-Al2_O_3$ with NaOH powder. $NaAlO_2$ was formed by calcination of ${\alpha}-Al_2O_3$ with NaOH and conversion of $NaAlO_2$ from ${\alpha}-Al_2O_3$ was 91.4% at calcination condition ; weight ritio of $NaOH/{\alpha}-Al2_O_3$ 1.5, $800^{\circ}C$, and 90min. The first calcined waste porrery from the manufacturing Procedure of H Ltd. was grinded to 170/270mesh by a ball mill and calcined over $500^{\circ}C$ with NaOH powder. The calcined sample was dissolved in $25^{\circ}C$ water and sodiumaluminosilicate solid was formed. After filtration, the contained aluminum was leached out by dissolving sodiumaluminosilicate solid in 1N HCl. We estimated the efficiency of Al extraction from waste pottery by ICP analysis and NaOH was added to the filtrate and then aluminum compound was precipitated with $Al(OH)_3$ and recovered. The investigation was carried out with the variables ; the calcination temperature($500-900^{\circ}C$), the calcination time(30~90min), and the weight ratio of NaOH/waste pottery(0.5~1.5). The treatment efficiency of the waste pottery and the recovery of Al as 97.9%, 91.9% were obtained under the optimum conditions as followed ; the weight ratio of NaOH/waste pottery was 1.5 and the calcination conditions were $900^{\circ}C$ and 60min.

• The Journal of the Korea Contents Association
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• v.7 no.10
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• pp.157-164
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• 2007

Human made a vessel which was made naturally to store something being hunted and picked, which was a great invention.(n modern times, society changed and development of science gave us convenience in making a vessel and various kinds of store instruments which was made of pure natural material), They have built the house which became to be a part of nature, and studied a method of storing food to eat for four seasons, then displayed a storage house and storage containers everywhere of the house. Now Korean has the custody of kimchi in refrigerator at every house. With hot wind of well-being, Korean food is becoming to be globalized, according to this the world shows concern seriously about the pottery This study have three purposes, the first. checking documents about the development history of pottery which is a kind of ceramic, and then the second, through an scientific experiment, with studying characteristic of pottery being built by the wisdom of ancestors, informing the merit of pottery and necessity to the world, and futhermore, the third, working up the development of close environmental vessels putting to use the characteristic of pottery.

• Journal of Conservation Science
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• v.26 no.4
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• pp.459-465
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• 2010

The 5th century kiln that produced pottery coffins was found for the first time in Korea, located in the Oryang-dong remains in the city of Naju. This kiln, located in the central area of the Yeongsan River, provides important data for research on mortuary practices in prehistoric society, including the structure of production and patterns of distribution and consumption. For this study, the remains of five ancient tombs and pottery coffins excavated from the 4th century Mandong archaeological site were chosen to determine the area of consumption of pottery coffins produced at the Oryang-dong kiln. The samples from each area of remains were analyzed for minor elements using neutron activation analysis method, and from these results, the identities of the corresponding production areas were investigated using the multi-variant statistical analysis of discriminant analysis. The evidence strongly suggests that pottery coffins produced at the Oryang-dong kiln in Naju were used in ancient tombs of the Bannam mound in Naju, the Okyari mound in Yeongam, and the Banam mound in Hampyeong, reaching those sites through trade and distribution. The findings also suggest that pottery coffins from the Mandong archeological site in Gochang and the Inpyeong mound in Muan were not produced at the Oryang-dong kiln in Naju, but rather were brought from pottery kilns in different production areas, through trade and distribution.

• Conservation Science in Museum
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• v.13
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• pp.1-11
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• 2012

While the project for registering the unregistered relics that had been stored in the relic storage warehouse was in progress, restoration operations were started for the large size pottery pieces that had been excavated from the Geumgangsa Temple Site and it is attempted to explain the pottery pieces and to introduce the process of the overall conservation treatment. About 600 pieces of large size pottery had been separately stored in more than 40 relic boxes in their original damaged condition without making it possible to figure out their shape, size, usage and quantity at all. Due to the enormous number and weight of the pottery pieces, they were, first of all, pre-classified largely into 6 groups of pottery pieces in consideration of the visible features such as pottery thickness, color sense and glaze brilliance, etc. for each kind of pottery raw material. However, as a result of making them adhere together on a temporary basis, they turned out to be only one piece of pottery in reality. In this restoring process, in order to see if the generally used cyanoacrylate adhesive was in fact safe when a very large, heavy and deformed pottery piece was to be put together, its safeness was checked by examining the adhesion velocity, adhesion strength and dissolution velocity for both from low to high viscosities through preliminary experiments. In order to restore the lost parts after putting the existing pieces together, diversified epoxy resins were used to fit their shapes. Considering that the bottom of the restored relic was shaped to be not flat but round without allowing it to stand alone, an exhibition mount was manufactured so that the relic could be stored stably and used readily for exhibition.

• Journal of the Mineralogical Society of Korea
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• v.6 no.1
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• pp.27-37
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• 1993

The clay minerals such as sericite, pyrophyllite, chlorite and smectite abundantly occur in the Bobae pottery stone mine in Pusan. In this study, the processes which are responsible for the formation of these minerals were studied by examing their occurrence and mineralogical properties. The so-called pottery stone of this mine is characterized by the predominance of sericite and quartz. The sericite of the pottery stone is mostly $2M-{1}$ type. And many of quartz particles are smaller than a few micron in diameter. The pottery stone also contained a small amount of pyrophyllite and muscovite. The pottery stone deposit occurs within the Cretaceous rhyodacite and is particularly well developed near the contact with the quartz porphyry which intrudes the rhyodacite. The fact implies that the pottery stone is the product of hydrothermal alteration of the rhyodacite by the intrusion of quartz porphyry. The pottery stone was formed by the alteration that accompanies the dissociation of feldspar and chlorite in parent rocks and subsequent formation of sericte and quartz. Smectite, laumontite and kaolinite occur locally within the altered rocks. These minerals were formed after formation of pottery stone. It is noteworthy that beidellite occurs as a pink-colored clay from the altered rocks in the mine.

• Analytical Science and Technology
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• v.12 no.6
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• pp.558-564
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• 1999

A method for measuring archaeological dose of Packjae pottery shards using thermoluminescence dosimetry(TLD) has been studied. TL measurement has been achieved using quartz crystals in the size range of 90 to $125{\mu}m$ diameter extracted from the pottery shards. The stable temperature region of the TL glow curve which is devoid of anomalous fading components was identified by the plateau test and found to exist from 265 to $300^{\circ}C$. The archaeological dose of the pottery shards was estimated to be 7.43 Gy using the dose calibration curves obtained from sequential irradiation of $^{137}Cs$ gamma source to the samples and TL measurement of natural samples.