• Title/Summary/Keyword: polyethylene powder

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The Study on Storage Stability according to Packaging Material of Traditional Sesame Dasik (깨다식의 포장재에 따른 저장성 조사)

  • 김진숙;한영실
    • The Korean Journal of Community Living Science
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    • v.15 no.2
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    • pp.179-187
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    • 2004
  • The purpose of this study is to investigate the preservation of traditional sesame dasik when stored in different packaging material by comparing its physical and sensorial characteristics. The quality and sensory characteristics of sesame dasik that were evaluated were moisture content, water activity, number of microflora, texture profile, Hunter color different value, and sensory properties (color, chewiness, overall acceptability, etc) during the storage at 35\pm1^\circ{C}$ temperature and $73\pm{2%}$ relative humidity. And the packaging materials were paper boxes (coated 0.02mm thickness polyethylene film), plastic boxes, and oriented polypropylene laminated film. Traditional sesame dasik is made from sesame powder 100g, honey 25g, rice syrup 25g, and table salt 0.5g. During the storage period, the changes in water content and water activity of sesame dasik with different packaging material showed a slight decline. On the other hand, it increased in hardness, and "a" and "b" value of Hunter color difference during the storage. Texture profile analysis data change in hardness was the greatest after the third day in a paper box, and it was affected by the moisture content of dasik and the temperature and relative humidity of the air. Therefore plastic boxes or oriented polypropylene laminated film was found to be better suited than paper boxes for storing sesame dasik.

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Preparation of ZnO2 Nanoparticles Using Organometallic Zinc(II) Isobutylcarbamate in Organic Solvent

  • Kim, Kyung-A;Cha, Jae-Ryung;Gong, Myoung-Seon;Kim, Jong-Gyu
    • Bulletin of the Korean Chemical Society
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    • v.35 no.2
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    • pp.431-435
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    • 2014
  • Zinc peroxide nanoparticles ($ZnO_2$ NPs) were prepared by reacting zinc(II) isobutylcarbamate, as an organometallic precursor, with hydrogen peroxide ($H_2O_2$) at $60^{\circ}C$. Polyethylene glycol and polyvinylpyrrolidone were used as stabilizers, which suppressed aggregation of the $ZnO_2$ NPs. Conditions such as concentrations of $H_2O_2$ and the stabilizer were systemically controlled to determine their effect on the formation of nano-sized $ZnO_2$ NPs. The formation of stable $ZnO_2$ NPs was confirmed by UV-vis, Raman spectroscopy, X-ray photoelectron spectroscopy, transmission electron microscopy (TEM), scanning electron microscopy (SEM), and X-ray diffraction. The TEM images revealed that polyvinylpyrrolidone-stabilized $ZnO_2$ NPs (diameter, 10-30 nm) were well dispersed in the organic solvent. Quite pure ZnO NPs were obtained from the peroxide powder by simple heat treatment of $ZnO_2$. The transition temperature of $170^{\circ}C$ was determined by differential scanning calorimetry.

Evaluation of Piezoelectric Properties in Pb(Zr,Ti)$O_3$-PVDF 0-3Type Composites for Thick Film Speaker Application (후막스피커 응용을 위한 Pb(Zr,Ti)$O_3$-PVDF 0-3형 복합체의 압전 특성 평가)

  • Son, Yong-Ho;Kim, Sung-Jin;Jeong, Joon-Seok;Ryu, Sung-Lim;Kweon, Soon-Yong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.40-41
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    • 2006
  • In this work, we developed the 0-3 type piezoelectric composite to incorporate the advantages of both ceramic and polymer. The PVDF-PZT composites were fabricated with various mixing ratio by 3-roll mi11 mixer. The composite solutions were coated on ITO bottom-electrode deposited on PET (polyethylene terephthalate) polymer film by the conventional screen-printing method. After depositing the top-electrode of silver-paste, 4kV/mm of DC field was applied at $120^{\circ}C$ for 30min to poling the 0-3 composite film. The value of $d_{33}$ was increased as the PZT weight percent was increases. But the $g_{33}$ value showed the maximum at 65 wt% of PZT powder.

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Electrical properties of conducting polymer PTCR containing carbon powders (탄소분말을 함유한 도전성 고분자 PTCR의 전기적 특성)

  • Kim, Kyung-Jong;Lee, Jae-Won;Kim, Young-Hyeok;Kim, Sung-Hoon;Choi, Mun-Seok;Lee, Jae-Shin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.220-221
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    • 2006
  • We investigated the electrical properties of polymer-carbon composite materials for temperature sensitive resistor applications. Cu/polymer/Cu sheets were fabricated by laminating low density polyethylene(LDPE) containing carbon powders. Weight ratio of carbon powder to LDPE was varied in a range of 0.9~2. With increasing the carbon concentration, the electrical resistance of the composite material was decreased from 0.75 to $0.08\;{\Omega}cm$. The composite layer showed a abrupt increase in the electrical resistance at $115^{\circ}C$ because of the softening of the polymer.

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Mechanical Properties and Thermal Stability of Waste PVC/HDPE Blend Prepared by Twin-screw Extruder

  • Lee, Rami;Park, Se-Ho;Baek, Jong-sung;Kye, Hyoungsan;Jhee, Kwang-Hwan;Bang, Daesuk
    • Elastomers and Composites
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    • v.54 no.1
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    • pp.7-13
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    • 2019
  • Recycling of waste polyvinyl chloride plastics has attracted much attention due to environmental problems, but the poor mechanical properties, low thermal stability, frequent breakage of strands, and melt cracking of the waste plastics have limited their widespread use. To overcome these disadvantages of waste PVC (W-PVC), recycled PVC powder blend was prepared by adding high-density polyethylene (HDPE) and ethylene vinyl acetate (EVA) as a heat stabilizer and compatibilizer, respectively. An intermeshing co-rotating twin screw extruder was used to prepare the blend, and the characteristics of the blend were analyzed by SEM and TGA, and by using a UTM and Izod impact tester. The impact strength was improved as the EVA content increased for the W-PVC/HDPE (80/20 wt%) blend. As the HDPE and EVA contents increased in the W-PVC/HDPE/EVA blend, the impact strength increased. SEM observations also revealed the improved interfacial adhesion for the EVA-containing blend.

The Study on Implementation of a Semi-Solid Flat Phantom with Equivalent Electrical Properties to Whole Human Body at MICS and ISM Band (MICS 대역과 ISM 대역에서 인체 전기적 상수를 갖는 준(準) 고체형 플랫 팬텀 제작)

  • Lee, Soon-Yong;Seo, Won-Bum;Kwon, Kyeol;Choi, Jea-Hoon
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.23 no.1
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    • pp.101-107
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    • 2012
  • When wireless devises for MICS(Medical Implant Communication Service) or ISM(Industrial Scientific and Medical) bands are designed, it is necessary to verify the performance by using a human body flat phantom. However, most of studies on the phantom are limited to the biological effects of mobile-phone EMF. In this paper, semi-solid phantoms having the electric properties suggested by FCC at MICS and ISM bands are fabricated. The manufactured phantoms satisfy the electric properties($\varepsilon_r=56.7$ and $\sigma=0.94$ at MICS band, $\varepsilon_r=52.7$ and $\sigma=1.95$ at ISM band) at each band. All the composing materials for phantoms are commercially available in domestic market. Two methods using both polyethylene powder and TX-151 and glycerin at each band are proposed for diverse purpose. The electrical properties of the fabricated phantoms are measured by a dielectric probe kit and network analyzer after the lapse of one day (24 hours).

Thermal residues analysis of plastics by FT-near infrared spectroscopy (근적외선분광법을 이용한 플라스틱류의 연소 잔류물 분석)

  • Lee, So Yun;Cho, Won Bo;Kim, Hyo Jin
    • Analytical Science and Technology
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    • v.30 no.5
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    • pp.234-239
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    • 2017
  • Identifying the components of residues that are not completely burned at the sites of fires site can provide valuable information for tracing the causes of fires. In order to clarify the types of plastic combustion residues found at the scenes of fires, we studied the residue formed after the combustion of polyethylene (PE) and acrylonitrile butadiene styrene (ABS). Plastic samples were burned at 200, 300, 350, 400, and $500^{\circ}C$ for 3 min using a cone calorimeter, and the changes in weight and combustion products were observed. The powder products obtained by lyophilization and pulverization of the combustion products obtained at each temperature were analyzed by a Fourier transform-near infrared (FT-NIR) spectrometer. When the PE samples were burned, the weight did not change up to $350^{\circ}C$, however a significant change in the weight could be measured above $400^{\circ}C$. The principal component analysis (PCA) of the FT-NIR spectra of the PE and ABS samples obtained at each temperature confirmed that the combustion residues at each temperature were PE and ABS, respectively. Therefore, the types of unburned plastics found at the sites of fires can be confirmed rapidly by near infrared spectroscopy.

Effect of Solubilizing and Microemulsifying Excipients in Polyethylene Glycol 6000 Solid Dispersion on Enhanced Dissolution and Bioavailability of Ketoconazole

  • Heo, Min-Young;Piao, Zong-Zhu;Kim, Tae-Wan;Cao, Qing-Ri;Kim, Ae-Ra;Lee, Beom-Jin
    • Archives of Pharmacal Research
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    • v.28 no.5
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    • pp.604-611
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    • 2005
  • Polyethylene glycol (PEG) 6000-based solid dispersions (SDs), by incorporating various pharmaceutical excipients or microemulsion systems, were prepared using a fusion method, t o compare the dissolution rates and bioavailabilities in rats. The amorphous structure of the drug in SDs was also characterized by powder X-ray diffractometry (XRD) and differential scanning calorimetry (DSC). The ketoconazole (KT), as an antifungal agent, was selected as a model drug. The dissolution rate of KT increased when solubilizing excipients were incorporated into the PEG-based SDs. When hydrophilic and lipophilic excipients were combined and incorporated into PEG-based SDs, a remarkable enhancement of the dissolution rate was observed. The PEG-based SDs, incorporating a self microemulsifying drug delivery system (SMEDDS) or microemulsion (ME), were also useful at improving the dissolution rate by forming a microemulsion or dispersible particles within the aqueous medium. However, due to the limited solubilization capacity, these PEG-based SDs showed dissolution rates, below 50% in this study, under sink conditions. The PEG-based SD, with no pharmaceutical excipients incorporated, increased the maximum plasma concentration (C$_{max}$) and area under the plasma concentration curve (AUC$_{0-6h}$) two-fold compared to the drug only. The bioavailability was more pronounced in the cases of solubilizing and microemulsifying PEG-based SDs. The thermograms of the PEG-based SDs showed the characteristic peak of the carrier matrix around 60$^{\circ}C$, without a drug peak, indicating that the drug had changed into an amorphous structure. The diffraction pattern of the pure drug showed the drug to be highly crystalline in nature, as indicated by numerous distinctive peaks. The lack of the numerous distinctive peaks of the drug in the PEG-based SDs demonstrated that a high concentration of the drug molecules was dissolved in the solid-state carrier matrix of the amorphous structure. The utilization of oils, fatty acid and surfactant, or their mixtures, in PEG-based SD could be a useful tool to enhance the dissolution and bioavailability of poorly water-soluble drugs by forming solubilizing and microemulsifying systems when exposed to gastrointestinal fluid.

Freshness Maintenance of Polyethylene Film Containing Surface-modified Zeolite (표면 개질된 제올라이트를 포함한 폴리에틸렌 필름의 선도유지기능)

  • Chun Byoung Chul;Lee Seong Jae;Chung Mi Hwa;Park Jung Hwan;Park Hee Woo;Chung Yong-Chan;Kweon Oh Cheul
    • Food Science and Preservation
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    • v.11 no.4
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    • pp.478-484
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    • 2004
  • Freshness maintenance of polyethylene packaging film containing surface-modified zeolite was investigated depending on the nature of substituted cations and cationic surfactants. Freshness maintenance was designed to work by cation or cationic surfactant adsorbed onto the zeolite surface by ion-exchange method. Cationic surfactants such as DODAB (n-dodecyltrimethylammonium bromide), CTAB (n-cetyltrimethylammonium bromide), and DHAB (n-dihexadecyldime-thylammonium bromide), and cations ($Ce^{3+},\;Al^{3+},\;Mg^{2+},\;Ca^{2+},\;Ag^{3+},\;Na^{1+}\;and\;Cu^{3+}$) were used. Surface-modified zeolite powder was compounded with LDPE to produce $20\;wt\%$ zeolite masterbatch (M/B), and the M/B was again blended with LDPE to get zeolite-containing LDPE films with 3, 5, $10\;wt\%$ of zeolite (width: 40 cm, thickness: $40\;{\mu}m$). Mechanical properties of zeolite-containing LDPE films generally decreased with increasing zeolite content. However, cationic surfactant-modified zeolite film showed the better mechanical properties compared to cation-modified zeolite film. As for the freshness maintenance, the zeolite-containing films modified with cationic surfactants or cations ($Al^{3+},\;Ag^{3+}$) showed the best performance.

Correlation between Acoustic Intensity and Ground Particle Size in Alumina Ball Mill Process

  • Cho, Kyeong-Sik;Kim, Soo-Hyun;Lee, Young Hun
    • Journal of the Korean Ceramic Society
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    • v.55 no.3
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    • pp.275-284
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    • 2018
  • In the ball milling process of ceramic powders, according to economic considerations for industrial applications, it is very important to quickly determine the optimum process condition with the maximum grinding efficiency. However, it is still difficult to determine the optimum condition for a ball mill with respect to the various process parameters, such as the rotational speed and the milling time. Ball milling was carried out at the same starting conditions with given amounts of alumina powders, balls and water, and was conducted slower or faster or a critical rotational speed was just determined by observing the angular position of the slurry in a semi-translucent polyethylene laboratory container. With respect to the different rotational speeds, which were slower or faster than the critical rotational speed, the particle size distribution of the grained powders and the acoustic intensity caused by cascading of the balls led to various behaviors. From the results of the particle size distribution and the acoustic signal analysis in the ball milling, there was one rotational speed that made the finest milled powder with maximum acoustic intensity. As a result, there was a correlation between the ground particle size and the acoustic intensity, which yields the interpretation that it can be possible in-situ to determine the optimum condition of ball milling by acoustic signal without repeated measurement efforts.