• Title/Summary/Keyword: polycrystal

Search Result 142, Processing Time 0.031 seconds

Silicidation and Thermal Stability of the So/refreactory Metal Bilayer on the Doped Polycrystalline Si Substrate (Co/내열금속/다결정 Si 구조의 실리사이드화와 열적안정성)

  • 권영재;이종무
    • Journal of the Korean Ceramic Society
    • /
    • v.36 no.6
    • /
    • pp.604-610
    • /
    • 1999
  • Silicide layer structures and morphology degradation of the surface and interface of the silicide layers for he Co/refractory metal bilayer sputter-deposited on the P-doped polycrystalline Si substrate and subjected to rapid thermal annealing were investigated and compared with those on the single Si substrate. The CoSi-CoSi2 phase transition temperature is lower an morphology degradation of the silcide layer occurs more severely for the Co/refractorymetal bilayer on the P-doped polycrystalline Si substrate than on the single Si substrate. Also the final layer structure and the morphology of the films after silicidation annealing was found to depend strongly upon the interlayer metal. The layer structure after silicidation annealing of Co/Hf/doped-poly Si is Co-Hf alloy/polycrystalline CoSi2/poly Si substrate while that of Co/Nb is polycrystalline CoSi2/NbSi2/polycrystalline CoSi2/poly Si.

  • PDF

A Study on the Relationship Between Photovoltaic Module Surface Temperature and Photovoltaic Power Using Real Experiment (실물 실험을 통한 태양광 모듈의 표면온도와 태양광 발전량과의 관계에 대한 연구)

  • Cho, Sung-Woo
    • Journal of the Korean Society for Geothermal and Hydrothermal Energy
    • /
    • v.14 no.3
    • /
    • pp.8-14
    • /
    • 2018
  • PV module power is calculated on PV module surface temperature adjustment by irradiation on the summer and autumn in NOCT(Nominal Operating Cell Temperature) conditions. The summer and autumn periods were selected because of large variation in outdoor air temperature and irradiation. This study was performed to understand relationship between PV module surface temperature and photovoltaic power using field measurement. As a results, it was determined that the amount of irradiation was proportional to the amount of photovoltaic power in the field measurement. However, it was also identified that the PV power generation decreased by increased PV module surface temperatures due to irradiation.

Electrical properties for $ZnIn_2S_4$ epilayers grown by Hot Wall Epitaxy (Hot Wall Epitaxy (HWE)법에 의해 성장된 $ZnIn_2S_4$ 에피레이어의 전기적 특성)

  • Lee, Sang-Youl;Hong, Kwang-Joon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2008.11a
    • /
    • pp.143-144
    • /
    • 2008
  • Single crystal $ZnIn_2S_4$ layers were grown on a thoroughly etched semi-insulating GaAs(100) substrate at $450^{\circ}C$ with the hot wall epitaxy (HWE) system by evaporating the polycrystal source of $ZnIn_2S_4$ at $610^{\circ}C$ prepared from horizontal electric furnace. The crystalline structure of the single crystal thin films was investigated by the photoluminescence and double crystal X-ray diffraction (DCXD). The carrier density and mobility of single crystal $ZnIn_2S_4$ thin films measured with Hall effect by van der Pauw method are $8.51\times10^{17}$ electron/$cm^{-3}$, 291 $cm^2$/v-s at 293 K, respectively.

  • PDF

The Effects of Impurities in Silicon Nitride Substrate on Tribological Behavior between Diamond Film and Silicon Nitride Ball

  • Lim, Dae-Soon;Kim, Jong-Hoon
    • Tribology and Lubricants
    • /
    • v.11 no.5
    • /
    • pp.20-25
    • /
    • 1995
  • Diamond films were prepared by a hot filament vapor deposition onto polycrystal silicon nitride substrates. Different kinds of silicon nitride containing CaO and $Fe_{2}O_{3}$ were manufactured to investigate the impurity effect of substrate on the morphology of diamond films and their wear behaviors. Nucleation rates and morphologies of diamond films deposited on various kinds of silicon nitride were compared. The highest nucleation rate was observed in a substrate containing 1% of CaO. Wear tests were performed with a silicon nitride ball on the disk geometry to investigate the tribological behavior of diamond film against silicon nitride. This study demonstrated that different morphologies of diamond film due to substrate impurities produced different wear behavior against silicon nitride.

Development of Dark Field image Processing Technique for the Investigation of Nanostructures

  • Jeon, Jongchul;Kim, Kyou-Hyun
    • Journal of Powder Materials
    • /
    • v.24 no.4
    • /
    • pp.285-291
    • /
    • 2017
  • We propose a custom analysis technique for the dark field (DF) image based on transmission electron microscopy (TEM). The custom analysis technique is developed based on the $DigitalMicrograph^{(R)}$ (DM) script language embedded in the Gatan digital microscopy software, which is used as the operational software for most TEM instruments. The developed software automatically scans an electron beam across a TEM sample and records a series of electron diffraction patterns. The recorded electron diffraction patterns provide DF and ADF images based on digital image processing. An experimental electron diffraction pattern is recorded from a IrMn polycrystal consisting of fine nanograins in order to test the proposed software. We demonstrate that the developed image processing technique well resolves nanograins of ~ 5 nm in diameter.

Conversion of Carbon Fiber into Silicon Carbide Fiber by Pack-Cementation

  • Joo, Hyeok-Jong;Kim, Jung-Il;Lee, Jum-Kyun
    • Carbon letters
    • /
    • v.1 no.1
    • /
    • pp.12-16
    • /
    • 2000
  • Carbon fiber was reacted with gaseous silicon monoxide which is produced from pack-powder mixture at elevated temperature. As a result of the reaction, two kinds of SiC fiber were obtained. The first one was SiC fibers which were converted from carbon fiber. The fiber is constituted with polycrystal like fine grains or monolithic crystals that have a size from sub-micron to $10\;{\mu}m$. Their size depends on the temperature during the conversion reaction. The second one was ultra-fine SiC fibers that were found on the surface of the converted SiC fibers. The ultra-fine fibers have diameters from 0.08 to $0.2\;{\mu}m$ and their aspect ratio were larger than 100. The chemical composit ion of the ultra-fine fibers was analyzed using an Auger electron spectroscopy. In result, the fibers consist of 51% silicon, 38% carbon and 11% oxygen by weight.

  • PDF

Direct Observation on the Low Temperature Degradation Due to Surface Treatment in Y-TZP (Y-TZP에서 표면 처리에 따른 저온열화 거동의 직접적 관찰)

  • Chung, Tai-Joo;Kim, Hye-Sung
    • Journal of Powder Materials
    • /
    • v.17 no.3
    • /
    • pp.197-202
    • /
    • 2010
  • Low temperature degradation behavior in yttria stabilized tetragonal zirconia polycrystal (Y-TZP) ceramics was microscopically observed from the phase contrast between monoclinic surface and tetragonal matrix. The degradation behavior was dependent on the surface treatment of sintered Y-TZP, even if the sintering history is same. In the mirror polished specimen, the monoclinic layer appeared in a uniform thickness from the surface. On the contrary, for the specimen with coarse scratch, the thickness of degraded surface was more than double especially from the coarse scratch. Since the scratch results in local deformation, the residual stress should be induced around the scratch. With the transformation from tetragonal to monoclinic, the volume expansion exerts a stress on a neighboring grains and promotes a successive phase transformation. Such a autocatalytic effect can be triggered from the part of coarse scratch.

Sintering and Isothermal Phase Transformation of Calcia Stabilized Tetragonal Zirconia Polycrystals (칼시아 안정화 정방정 지르코니아(Ca-TZP)의 소결 및 등온상전이 거동)

  • 곽효섭;백용혁;이종국
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.3 no.1
    • /
    • pp.37-44
    • /
    • 1993
  • Calcia stabilized zirconia polycrystal (Ca-TZP) powders synthesized by hydrothermal treatment was sintered at a temperature range of $1200^{\circ}C~1400^{\circ}C$ and investigated the properties of sintered body and the behaviors of isothermal phase transformation. The sintered bodies of Ca-TZP were shown the density of about 97% and the average mean tetragonal grain size of about $0.1~0.25{\mu}m$. Also, Ca-TZP specimen was more stable during aging at $250^{\circ}C$ than that of Y-TZP ceramics.

  • PDF

The investigation of plastic spin behavior of body centered polycrystal with simplified accommodatio model (정적 결정수용모델에 의한 체심입방격자 다결정의 소성스핀 거동에 관한 연구)

  • Nam, Y. Y.
    • Journal of Ocean Engineering and Technology
    • /
    • v.10 no.2
    • /
    • pp.42-52
    • /
    • 1996
  • 소성스핀을 취급하기 위한 이론을 살펴보면 개념적으로 현저히 다른 세가지로 압축된다. 또한 재료직조 현상이 소성스핀의 근원이라고 알려져 있지만, 그 지배인자와 발생근원에 대하여 아직 충분히 연구되어 있지 않다. 따라서 앞으로의 연구에 올바른 방향을 제시하기 위하여 소성스핀의 기본적인 거동에 대한 연구가 요구된다. 본 연구에서는 체심입방격자 다결정의 소성스핀 시뮬레이션을 통하여, 소성스핀의 거동을 조사하였는데, 재료직조, 변형경화, 변형속도, 하중역전 등의 영향을 검토하였다. 소성발생원인으로 재료직조현상이 강조되었고, 이에 관련한 주요지배인자를 제시하였다. 무차원 소성스핀은 변형속도, 재료경화에 영향을 받으나 재료직조와 관련한 인자와 비교하여 그 영향이 작게 나타났다.

  • PDF

A Study on the Plastic Spin of Body Centered Crystal (체심입방격자 단결정의 소성스핀에 관한 연구)

  • 남용윤;김사수
    • Journal of Ocean Engineering and Technology
    • /
    • v.10 no.2
    • /
    • pp.53-60
    • /
    • 1996
  • Many studies on the plastic spin have been done, but it is still an opened subject. It is essential for the modelling of plastic spin to understand its origin and governing parameters. For the task, it is helpful to know the hehavior of sigle crystal. This study gives the interpretations for the plastic spin of a B.C.C(body centered cubic crystal) by numerical simulation. It is discussed that the different levels of shear stresses induced on each slip pair in crystallographic slip systems and the nonlinear relationship between shear stress and slip velocity are the fundamental mechanisms of plastic spins. Finally some comments are provided on the plastic spin of polycrystal.

  • PDF