• Nuclear Engineering and Technology
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• v.54 no.3
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• pp.991-996
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• 2022

Microstructures of monolithic high purity SiC and SiC with sintering additives after neutron irradiation to a fluence of 2.0-2.5 × 10²⁴ n/m² (E > 0.1 MeV) at 333-363 K and after post-irradiation annealing up to 1673 K were observed using a transmission electron microscopy. Results showed that no black spot defects or dislocation loops in SiC grains were found after the neutron irradiation for all of the specimens owing to the moderate fluence at low irradiation temperature. Thus, it is confirmed that these specimens were swelled mostly by the formation of point defects. Black spots and small dislocation loops were discovered only after the annealing process in PureBeta-SiC and CVD-SiC, where the swelling almost diminished. Anomalous-shaped YAG grains were found in SiC ceramics containing sintering additives. These grains contained dense black spots defects and might lose crystallinity after the neutron irradiation, while these defects may annihilate by recrystallization during annealing up to 1673 K. Amorphous grain boundary phase was also presented in this ceramic, and a large part of it was crystallized through post-irradiation annealing and could affect their recovery behavior.

• Journal of the Korean Society of Safety
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• v.14 no.3
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• pp.25-32
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• 1999

This study has been performed to investigate the stress distribution around defects that behave as stress concentrators. Besides, the effect of stress interaction effects on the initiation of primary cracks were also investigated by rotary bending fatigue tests which were performed with specimens drilled micro surface defects and the stress distribution was analyzed using Finite Element Method. In addition, the stress interaction effects around defects and cracks were investigated by comparing the results of experiments and F.E.M. The results obtained are summarized as follows ; 1) Area which slip and micro cracks initiated at micro surface defects is between the maximum shear stress points and this area is over than ${\pm}30^{\circ}$ from the maximum stress point along the defect edge. 2) The stress interaction effect for the small size defect is larger than that of large size defect when the interval between them is near 3) Interval which there is no shear stress interaction effect analyzed by F.E.M. is larger than that of experimental results.

• Applied Microscopy
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• v.50
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• pp.27.1-27.6
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• 2020

Transition metal dichalcogenides (TMD), which is composed of a transition metal atom and chalcogen ion atoms, usually form vacancies based on the knock-on threshold of each atom. In particular, when electron beam is irradiated on a monolayer TMD such as MoS₂ and WS₂, S vacancies are formed preferentially, and they are aligned linearly to constitute line defects. And then, a hole is formed at the point where the successively formed line defects collide, and metal clusters are also formed at the edge of the hole. This study reports a process in which the line defects formed in a monolayer WS₂ sheet expends into holes. Here, the process in which the W cluster, which always occurs at the edge of the formed hole, goes through a uniform intermediate phase is explained based on the line defects and the formation behavior of the hole. Further investigation confirms the atomic structure of the intermediate phase using annular dark field scanning transition electron microscopy (ADF-STEM) and image simulation.

• Transactions of Materials Processing
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• v.24 no.4
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• pp.241-247
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• 2015

In order to prevent shape defects such as fluting and stretcher strains during press forming of aged low carbon steel sheets, roller leveling conditions for reducing yield point elongation were studied. Yield point elongations of leveled sheets were determined as a function of leveling, which is defined as the plastic fraction or the ratio of plastically deformed part in sheet thickness section to the whole thickness of the sheet. By adjusting this plastic fraction during leveling to more than 78%, yield point elongation in the leveled sheets was reduced so no fluting occurred during subsequent tangential bending. Stretcher strains can be avoided by leveling the sheet to an 84% plastic fraction condition.

• Journal of Electrical Engineering and Technology
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• v.5 no.4
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• pp.666-671
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• 2010

Multi-layer perceptron neural networks have been constructed to classify four types of defects in steam generator tubes. Three features are extracted from the signals of the eddy current testing method. These include maximum impedance, phase angle at the point of maximum impedance, and an angle between the point of maximum impedance and the point of half the maximum impedance. Two hundred sets of these features are used for training and assessing the networks. Two approaches are involved to train the networks and to classify the defect type. One is the conjugate gradient method and the other is the Broydon-Fletcher-Goldfarb-Shanno method which is recognized as the most popular algorithm of quasi-Newton methods. It is found from the computation results that the training time of the Broydon-Fletcher-Goldfarb-Shanno method is much faster than that of the conjugate gradient method in most cases. On the other hand, no significant difference of the classification performance between the two methods is observed.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2002.05a
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• pp.58-61
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• 2002

A new concept of dieless sheet forming technology is proposed in this study to overcome the drawback of conventional dieless forming technology. For this purpose, dual points contact of the conventional punch system, which is a primary cause of surface defects, is replaced to single point contact using technology combined with fluid forming. It is expected that the advanced system may lead to easy displacement control of multi-punch elements, reducing surface defects, and increasing decision and forming limits. The reduced number of punch elements also saves the cost of the equipment. In addition, the new technology can be utilized for deep drawing as well as two- or three-dimensional curved surface forming, and thereby become multi-functional and multi-purpose differently from the conventional technology.

• The Transactions of the Korean Institute of Electrical Engineers C
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• v.51 no.5
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• pp.191-195
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• 2002

Chemical mechanical Polishing (CMP) process is widely used for the global planarization of inter-metal dielectric (IMD) layer and inter-layer dielectric (ILD) for deep sub-micron technology. However, as the IMD and ILD layer gets thinner, defects such as micro-scratch lead to severe circuit failure, which affect yield. In this paper, for the improvement of CMP process, deionized water (DIW) pressure, purified $N_2$ ($PN_2$) gas, point of use (POU) slurry filler and high spray bar (HSB) were installed. Our experimental results show that DW pressure and P$N_2$ gas factors were not related with removal rate, but edge hot-spot of patterned wafer had a serious relation. Also, the filter installation in CMP polisher could reduce defects after CMP process, it is shown that slurry filter plays an important role in determining consumable pad lifetime. The filter lifetime is dominated by the defects. However, the slurry filter is impossible to prevent defect-causing particles perfectly. Thus, we suggest that it is necessary to install the high spray bar of de-ionized water (DIW) with high pressure, to overcome the weak-point of slurry filter Finally, we could expect the improvements of throughput, yield and stability in the ULSI fabrication process.

• Progress in Superconductivity
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• v.3 no.1
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• pp.5-12
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• 2001

Our experimental research focuses on manipulating pinning deflects to alter the phase diagram of vortex matter, creating new vortex phases. Vortex matter offers a unique opportunity for creating and studying these novel phase transitions through precise control of thermal, pinning and elastic energies. The vortex melting transition in untwinned YB $a_2$C $u_3$ $O_{7-}$ $\delta$/ crystals is investigated in the presence of disorder induced by particle irradiation. We focus on the low disorder regime, where a glassy state and a lattice state can be realized in the same phase diagram. We follow the evolution of the first order vortex melting transition line into a continuous transition line as disorder is increased by irradiation. The transformation is marked by an upward shift in the lower critical point on the melting line. With columnar deflects induced by heavy ion irradiation, we find a second order Bose glass transition line separating the vortex liquid from a Bose glass below the lower critical point. Furthermore, we find an upper threshold of columnar defect concentration beyond which the lower critical point and the first order melting line disappear together. With point deflect clusters induced by proton irradiation, we find evidence for a continuous thermodynamic transition below the lower critical point..

• Proceedings of the Materials Research Society of Korea Conference
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• 1992.05a
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• pp.104-104
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• 1992

• Journal of the Korean Society for Nondestructive Testing
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• v.35 no.6
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• pp.398-406
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• 2015

This paper explored the results of experimental investigation on carbon fiber reinforced polymer (CFRP) composite sample with thermal wave technique. The thermal wave technique combines the advantages of both conventional thermal wave measurement and thermography using a commercial Infrared camera. The sample comprises the artificial inclusions of foreign material to simulate defects of different shape and size at different depths. Lock-in thermography is employed for the detection of defects. The temperature field of the front surface of sample was observed and analysed at several excitation frequencies ranging from 0.562 Hz down to 0.032 Hz. Four-point methodology was applied to extract the amplitude and phase of thermal wave's harmonic component. The phase images are analyzed to find qualitative and quantitative information about the defects.