• Journal of Powder Materials
• /
• v.5 no.4
• /
• pp.241-249
• /
• 1998

Sintering kinetics of ball-milled $MoSi_2$ was studied with the addition of Ni. $MoSi_2$ powder with the average particle size of 1 $\mu\textrm{m}$ was obtained from ball-milling of 10 $\mu\textrm{m}$ powder. Small amount of Ni was added to the ball-milled $MoSi_2$ powder by salt solution and reduction method. The powder was compacted into cylindrical shape at 200 MPa and isothermally sintered in a $H_2$ atmosphere at the temperature range of 1100~$1400^{\circ}C$ for 3~600 minutes. The changes of linear shrinkage and sintered density were monitored as a function of sintering time. The microstructure was observed by using optical microscopy and scanning electron microscopy. Phases were identified by X-ray diffratometer and electro-probe micro analysis. Sintering kinetics of Ni-added powder was compared to as-milled powder and the apparent activation energy was calculated from Arrhenius plot.

• Journal of Powder Materials
• /
• v.8 no.2
• /
• pp.104-109
• /
• 2001

The semiconducting ${\beta}-FeSi_2$ compound has been recognized as a thermoelectric material with excel-lent oxidation resistance and stable characteristics at elevated temperature. In the present work, we applied mechanical alloying(MA) technique to produce ${\beta}-FeSi_2$ compound using a mixture of elemental iron and silicon powders. The mechanical alloying was carried out using a Fritsch P-5 planetary mill under Ar gas atmosphere. The MA powders were characterized by the X-ray diffraction with Cu-K $\alpha$ radiation, thermal analysis and scanning electron microscopy. The single ${\beta}-FeSi_2$ phase has been obtained by mechanical alloying of $Fe_{33}Si_{67}$ mixture powders for 120 hrs or for 70 hrs coupled with the subsequent heat treatment up to $700^{\circ}C$. The grain size of ${\beta}-FeSi_2$ powders analyzed by Hall plot method was 44nm.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2001.07a
• /
• pp.745-748
• /
• 2001

We synthesized polypyrrole (PPy) by electrolysis of the pyrrole monomer solution containing support electrolyte KCl and/or p-toluene sulfonic acid sodium salt (p-TS). The electrochemical behavior was investigated using cyclic voltammetry and AC impedance. In the case of using electrolyte p-TS, the redox potential was about -0.3 V vs. Ag/AgCl reference electrode, while the potential was about 0 V for using electrolyte KCl. It is considered as the backbone forms a queue effectively by doping p-T S. Therefore, it is possible to be arranged regularly. That leads to improvement in the electron hopping. The AC impedance plot gave a hint of betterment of mass transport. PPy doped with p-TS has improved in mass transport, or diffusion. That is because the PPy doped with p-TS has a good orientation, and is more porous than PPy with KCl.

• Water Engineering Research
• /
• v.3 no.4
• /
• pp.269-278
• /
• 2002

A cross sectional analysis for residential water demand was conducted to help understand and explain the spatial and temporal variations in per capita water use in the rapidly growing city of Riyadh, Saudi Arabia. The analysis was based on data previously collected from May 1983 to June 1984. 195 randomly selected households were distributed to three groups according to house condition, household income level, and social and cultural factors. The generated models using stepwise multiple regression indicated that plot size and number of males, females and children are the most significant independent variables. Although, coefficients of determination achieved for most of the developed models were low (0.2-0.5), the independent variables could still explain a part of the variations fur such a complex social and cultural structure.

• Journal of the Korean Society of Tobacco Science
• /
• v.16 no.2
• /
• pp.191-197
• /
• 1994

Relationships between surface structure and adsorption properties of smoke components were investigated in surface-modified and un-modified activated carbon filter cigarettes. Commercially available activated carbon was treated with nitric acid and hydrogen peroxide as oxidant, and their pore volume, surface structure, BET surface area, pore type and size were studied. BET surface area and pore volume were decreased by nitric acid treatment, but median pore diameter was 8.1 $\AA$, which showed better development of pore compared with that of un-modified activated carbon, 6.9 $\AA$. In case of hydrogen peroxide treatment, BET surface area and pore volume were increased. Their pore was found to be a slit type based on V-t plot analysis. Neutralization capacities for bases of different strength (NaHCO3, Na2CO3, NaOEt and NaOH) showed that the majority of the acidic surface groups are of weak acidity. Modification of the activated carbon surface led to a slight change in adsorption properties when analyzing the smoke of triple-filter cigarette with surface-modified activated carbon.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.29 no.4 s.235
• /
• pp.614-623
• /
• 2005

This study aims to perform the characteristic evaluation of surface grinding for the STD11 material with experimental and analytic techniques based on the response surface model. The grinding force acting on the workpiece and the ground surface roughness were measured according to the change of grain size, table speed and depth of cut. The effect of spark-out on the grinding force and the surface roughness was also characterized. The frictional coefficient between workpiece and grinding wheel could be determined by the analysis of spark-out effect. From the experimental data, the second-order response surface models were developed to predict the grinding force and the surface roughness. Validation of the developed model was examined.

• Journal of Korean Society for Quality Management
• /
• v.25 no.1
• /
• pp.100-115
• /
• 1997

Shewhart control chart is a basic technique to monitor the state of a process. We observe samples of size four or five and plot some statistic(e.g., mean or range) of each sample on the chart. When setting up the chart, we need to obtain u, pp.r and lower control limits. It is common practice that those limits are calculated from the preliminary 20-40 samples presumed to be homogeneous. However, it may ha, pp.n in practice that the samples are contaminated by outlying observations caused by various reasons. The presence of outlying observations make the control limits wider and hence decrease the sensitivity of the charts. In this paper, we introduce robust control charts with tighter control limits when outlying observations are present in the preliminary samples. Examples will be given via simulation study.

• Korean Journal of Agricultural Science
• /
• v.1 no.1
• /
• pp.83-89
• /
• 1974

Georgia lily bulbs from experimental plot of the Chungnam National University, weighting 14.1~18.0gm, were used for this study. These bulbs were treated for the natural cooling at cold frame for 90 days and refrigerating at $8^{\circ}C{\pm}1^{\circ}C$ for 50~90 days. And then, these bulbs were planted in the vinyl house. The results of forcing for each treatments were as follow; 1) The natural cooling treatment gave 3 days ealier flowering than the refrigeratings. 2) In the blooming rate, the height of plant, and the size of flower, all refrigerating treatments were bigger than the natural cooling. 3) Among the refrigerating treatments, the best results were attain in the 50 and 60 days treatments than others. 4) Therefore, it is recommended that Georgia lily, as the next crop after Chrysanthemum ect, can be forced effectively by refrigerating treatment at $8^{\circ}C$ for 50~60 days, if these bulbs can be planted until the end of December.

• Proceedings of the Korean Society of Agricultural Engineers Conference
• /
• 2000.10a
• /
• pp.108-113
• /
• 2000

A field study was performed to investigate the effect of water saving irrigation method on water use efficiency and rice yield. The field plot was 40a (40 ${\times}$ 100m) in size and located at Buryangmyun, Kimjae city, Chonbuk province. Field measurements were made during the growing seasons, May to September of the year 1998 and 1990. Irrigation water volume, drainage water volume, rainfall and ponding depth were measured. Irrigation water management practice employed was such that to keep the ponding depth about 3 to 4cm by intermittent irrigation with drying the soil surface until hair cracks emerge before the next irrigation. The amounts of water volume irrigated and drained were measured by pipe flow meter and ponding depth was observed by using a partly buried 120mm diameter PVC pipe. The results showed that the irrigation water depths, the rainfalls, and the drainage depths were 379mm, 458mm, and 448mm in 1988, and 274mm, 819mm, and 736mm in 1990, respectively. The average yield was 590kg per 10a. The water saving irrigation method saved irrigation water by about 20% with higher yield compared with the traditional method.

• Journal of Magnetics
• /
• v.16 no.3
• /
• pp.216-219
• /
• 2011

Mn doped ZnO films were prepared on Si (100) substrates using sol-gel method. The prepared films were annealed at $550^{\circ}C$ for decomposition and oxidation of the precursors. XRD analysis revealed the presence of ZnMnO hexagonal wurtzite phase along with the presence of small quantity of $ZnMn_2O_3$ secondary phase and poor crystalline nature. The 2D, 3D views of magnetic domains and domain profiles were obtained using magnetic force microscopy at room temperature. Rectangular shaped domains with an average size of 4.16 nm were observed. Magnetic moment measurement as a function of magnetic field was measured using superconducting quantum interference device (SQUID) magnetometry at room temperature. The result showed the ferromagnetic hysteresis loop with a curie temperature higher than 300 K.