• Title/Summary/Keyword: pigment solution

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Stability of Pigment Produced by Monascus pilosus (Monascus pilosus가 생성하는 색소의 안정성)

  • Park, Mee-Ja;Yoon, Eun-Kyung;Kim, Soon-Dong
    • Korean Journal of Food Science and Technology
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    • v.34 no.4
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    • pp.541-545
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    • 2002
  • Stability of Monascus pilosus pigment was investigated under various conditions. The concentration of the pigments stored under air and sub-atmosphere (250 mmHg) for 30 days at room temperature decreased by 77.9% and 48.4%, respectively. The pigment solution was stable under temperature ranges of $20-80^{\circ}C$, pH 4-8, darkness and presence of KCl, NaCl, $CaCl_2$, $MgCl_2$, and $ZnCl_2$. In contrast, the pigment solution was relatively unstable, decreasing in concentration by 6.0 and 11.6% at 100 and $121^{\circ}C$, 15.5 and 13.7% at pH 3 and 9, 22.9 and 66.8% under fluorescence and sun light, respectively, and 20.2% in the presence of $AlCl_3$.

Extraction and Characteristics of Purple Sweet Potato Pigment (자색고구마 색소의 추출과 특성)

  • Kim, Seon-Jae;Rhim, Jong-Whan;Lee, Lan-Sook;Lee, Joon-Seol
    • Korean Journal of Food Science and Technology
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    • v.28 no.2
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    • pp.345-351
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    • 1996
  • Studies on extraction and color characteristics of purple sweet potato (PSP) pigment were performed to provide the basic information for the utilization of PSP as a new source of natural food colorant. PSP pigment was extracted well with the polar solvents such as distilled water, ethanol, and methanol. but hardly extracted with the non-polar solvents. Among the tested solvents, 20% ethanol solution containing 0.1% citric acid was found to be the most efficient for extraction of the pigment from PSP. PSP contained high amount of pigment not only in the epidermis but also in the flesh of the potato. The PSP pigment was heat stable even under pretreatments such as autoclaving and blanching of the potato before extraction. The optimum temperature of the extraction for the PSP Pigment was decided to be $30^{\circ}C$ by considering the stability and the rate of extraction. The pigment was markedly influenced by the change of pH. The color of the pigment solution was red at the pH range of $1.0{\sim}3.0$, became blue at $7.0{\sim}8.0$, then turned green at $9.0{\sim}10.0$. A characteristic batho-chromic shift of the pigment solution was observed as the pH of the solution increased.

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Stability of Anthocyanin Pigment Extracted from Mulberry Fruit (오디 색소의 안정성)

  • 강창수;마상조;조원대;김진만
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.32 no.7
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    • pp.960-964
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    • 2003
  • Effects of pH, sugars, organic acids, and metal ions on the stability of anthocyanin pigments extracted from mulberry (Morus alba L) fruit were studied. The pH had marked influences on the color of the anthocyanine pigment: i.e. the lower pH of the anthocyanin solution was, the more stable and intense of the pigment was. Among the sugars, sucrose was the most deleterious followed by fructose, glucose and maltose. Among the organic acids, maleic acid was found to be the most effective in stabilizing the pigment followed by acetic acid, citric acid and tartaric acid. Most metal ions except C $u^{+2}$ and F $e^{+3}$ were found to be effective in stabilizing the pigment.

Determination of the Conditions for Anthocyanin Extraction from Purple-Flashed Sweet Potato (자색고구마 Anthocyanin 색소의 추출조건 결정)

  • 이장욱;이향희;임종환;조재선
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.29 no.5
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    • pp.790-795
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    • 2000
  • To establish the optimum conditions for the extraction of anthocyanin pigment from purple-fleshed sweet potato, a suitable extraction solvent with the optimum citric acid concentration for acidification of the solvent, and the optimum extraction time and temperature were determined. Twenty percent ethanol solution acidified with citric acid was found to be a good solvent for the extraction of the pigment from purple-fleshed sweet potato. About 10 hour extraction at room temperature was appropriate for the extraction. pH of the extract was below 3 when more than 0.7% citric acid was added. The higher the concentration of citric acid added was, the higher the total optical density (TOD) of the extract was. However, the increase in TOD of the extract was insignificant when more than 1% of citric acid was added. Therefore, addition of 1% citric acid was determined for acidification of the extracting solvent. Though the initial rate of the pigment extraction increased as the extracting temperature increased, extraction at higher temperatures of 60 or 8$0^{\circ}C$ for an extended time caused a decrease in the extraction yield due to degradation of the pigment. The optimum extraction temperature for the anthocyanin pigment from purple-fleshed sweet potato with the solvent used was determined as 4$0^{\circ}C$.

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Simultaneous Analysis of the Coloring Compounds in Indigo, Phellodendron bark, and Madder Dye Using HPLC-DAD-MS

  • Ahn, Cheunsoon;Zeng, Xia;Obendorf, S. Kay
    • Journal of the Korean Society of Clothing and Textiles
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    • v.37 no.6
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    • pp.827-836
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    • 2013
  • Indigotin, indirubin, berberine, palmatine, alizarin, and purpurin are major pigments of indigo plant, Phellodendron bark, and madder. The six pigments were examined using the HPLC-DAD-MS instrument for the purpose of the simultaneous detection of the pigments in a single sample run. The HPLC-DAD-MS method examined the individual pigment solutions in DMSO, a solution containing 6 pigments, and the DMSO extract of the silk dyed with a dye solution of 5 pigments excluding indirubin. The retention times of the HPLC chromatograms, ${\lambda}_{max}$ of the uv-vis absorption bands in the DAD analyses, and the molecular ions detected for the compound peaks in the MSD analyses were consistent throughout the analyses of individual pigment solutions, mixed pigment solutions, and dye extracted from silk dyeing. The developed instrumental method of the simultaneous detection of six pigments can identify dye in an exhumed textile if the textile is dyed using any one (or multiple) pigments of indigo, Phellodendron bark, or madder plant.

Characteristics and Dyeability of Perilla Frutescens L. Britt Extracts with Different Solvents (추출용매에 따른 자소 색소의 염색성 및 기능성)

  • Wang, Qian Wen;Lee, Jung-Soon
    • Textile Coloration and Finishing
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    • v.28 no.3
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    • pp.195-207
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    • 2016
  • In this study, we examined the influence of the pigment characteristic and dyeing condition on dyeing properties and functionality by using Perilla Frutescens L. Britt extracts, in which ethanol, distilled water and NaOH solution were used as 3 different solvents. Changes in dyeing conditions include variations in dye concentration, dyeing temperature, time and pH on dye uptake, and K/S values were compared according to these changes. Additionally, color changes were observed according to the use and types of mordant. Ultraviolet-visible spectrum was utilized to investigate the pigment characteristic, and as a result, chlorophyll was identified in ethanol extract, whereas tannin was identified both in distilled water extract and NaOH solution extract. By using FT-IR analysis, these tannins in distilled-water-extract and NaOH solution extract were verified to be hydrolyzable tannin. When dyeing silk, dye uptake increased as dye concentration, dyeing temperature and time increased, while it decreased as pH of the extract increased. Fabrics dyed without a mordant produced Y-series colors, and fabrics dyed with mordants showed various colors depending on the mordant types. Even though color fastness to washing and light was unsatisfactory, fastness to rubbing and perspiration showed relatively high grade. Moreover, deodorant ability of dyed fabric improved.

Detection of Fake Jindo Hongju Using the pH-dependent Color Change of Gromwell (Lithospermum erythrorhizon) Pigment

  • Kim, Jungho;Bae, Yeong-Hwan;Choi, Kap-Seong
    • Journal of Applied Biological Chemistry
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    • v.42 no.3
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    • pp.151-153
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    • 1999
  • Gromwell (Lithospermum erythrorhizon) pigment solution and Jindo Hongju prepared in the laboratory showed characteristic pH-dependent color changes and a shift in absorption maxima. This phenomenon was not observed in the solution of the artificial food colorant Red No. 2 which was suspected to be used in the manufacture of fake Jindo Hongju. A few fake products could be detected by using the pH-dependent shift in absorption maxima among the Jindo Hongju on market.

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Pigment-dispersing factor induces phase shifts of circadian locomotor rhythm in the cricket Gryllus bimaculatus

  • Singaravel, Muniyandi;Tomioka, Kenji
    • Journal of Photoscience
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    • v.9 no.2
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    • pp.243-245
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    • 2002
  • Pigment-dispersing factor (PDF) is an octadecapeptide distributed in the optic lobe and the brain in a variety of insect species. There are lines of evidence suggesting possible involvement of PDF in the insect circadian system. However, its physiological roles in the circadian time keeping mechanism have not been clearly defined. In this study, we have examined the phase shifting effects of Gryllus-PDF on the circadian locomotor rhythm in the cricket Gryllus bimaculatus of which circadian clock is located in the optic lobe. Phase shifts in the circadian activity rhythm were measured following microinjection of 22nl of vehicle (Ringer's solution) or O.lmM PDF into the optic lobe through the compound eye at various circadian times. The results showed that PDF induced phase shifts of the circadian clock in a phase-dependent manner, suggesting that it may play a role as an input signal for the circadian clock.

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The Novel Preparation of White Pigment by Functionalized Wax Coating of $TiO_2$ for Electrophoretic Display

  • Joung, Meyoung-Ju;Kim, Mi-Kyung;Kim, Chul-Am;Ahn, Seong-Deok;Lee, Yong-Eui;Kang, Seung-Youl;Suh, Kyung-Soo;Kim, Chul-Hwan
    • 한국정보디스플레이학회:학술대회논문집
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    • 2002.08a
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    • pp.828-830
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    • 2002
  • In this study, we have investigated a simple process of preparation of white pigment particles by physical coating with functionalized wax for the electrophoretic display. We will discuss, especially, the implementation of bistable pigment providing high mobility by using unique charge control agent and also optical properties of wax coated $TiO_2$ particles.

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Effect of Solvent on the Dispersion Stability of CaCO3 Pigment (CaCO3 안료의 분산 안정성에 대한 용제의 영향)

  • Lee, Gun Dae;Ryu, Young Cheal;Suh, Cha Soo;Hong, Seong Soo;Ahn, Byung Hyun;Moon, Myung Jun
    • Applied Chemistry for Engineering
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    • v.8 no.2
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    • pp.252-261
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    • 1997
  • The effect of solvent on the dispersion stability of $CaCO_3$ pigment in various solvents and resin solutions has been studied using Dynometer. Dispersion stability can be estimated in a relatively short time by means of Dynometer and the solubility parameter, ${\delta}$, of $CaCO_3$ determined from dispersion stability was 11.62(${\delta}_d=8.04$, ${\delta}_p=5.05$, ${\delta}_h=6.70$). The solvent showing weaker interaction with pigment increased the adsorption of resin on to the pigment, resulting in higher dispersion stability in resin solution. It was found that the rheological properties and dispersion stability of pigmented resin solution were depending strongly on the solvent added in small amount in the formulation.

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