• Korean Journal of Environmental Agriculture
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• v.30 no.1
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• pp.60-67
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• 2011

BACKGROUND: Because dried herbal medicines have many active ingredients, it is not easy to determine the residue amount after extraction, partition and clean up of pesticides from them. Especially, liquid-liquid partition method is consuming many times and solvents. Macroporous diatomaceous earth(MDE) column was used to replace the separatory funnel for liquid-liquid extraction with dichloromethane to analyze the endosulfan and its metabolite. METHODS AND RESULTS: The residue analysis method using MDE column instead of liquid-liquid partition for determining insecticide endosulfan and its metabolite in 4 dried herbal medicines was developed by GC/MS. As a result, the recovery rates of the pesticides in 4 herbal medicines were ranged from 80.3 to 93.5% for ${\alpha}$-endosulfan, from 81.0 to 100.3% for ${\beta}$-endosulfan and from 80.6 to 95.6% for endosulfan sulfate, respectively. The coefficients of variation for triplicate were ranged from 1.1 to 3.4%. CONCLUSION: The improved methods are more ecofriendly, safer, faster and less laborious than conventional method by KFDA.

• Journal of Korean Society for Quality Management
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• v.22 no.2
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• pp.143-153
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• 1994

Cluster analysis is a primitive technique in which no assumptions are made concerning the data structure. And the number of groups is known a priori discriminant analysis provides an information how well N individuals are classified into their own groups. In this study, clustering, which is any partition of a collection of data points, generated by the application of eight hierarchical clustering methods was re-classified by discriminant analysis. Then correct classification ratios were obtained for the application of discriminant analysis through each clustering method and the direct application of discriminant analysis. By comparing the correct classification ratios, the applicability of cluster analysis and discriminant analysis considered.

• Journal of the Korean Chemical Society
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• v.8 no.2
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• pp.47-56
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• 1964

When a developed paper partition chromatogram was irradiated by means of the pneumatic tube system of the Korean research reactor (neutron flux: 1.5 ${\times}10^{12}n/cm^2$sec.) the qualitative confirmation of the developed spot on the chromatogram was possible. In the case of an organic halogen compounds (chloro-acid, chloro-ester, iodide, and fluoride) the spot analysis was possible by the present method whereas the same spot could not give the distinct coloring with a common coloring reagents. Filterpaper thickness calibration and activity calibration induced by irradiation of the components of the filter paper, which were a source of erraneous interpretation of the spot, were searched and an average filterpaper calibration method and filter paper activity were improvised to obtain a good qualitative analysis of the spot. Finally the use and applicability of this method for the analysis identification of an organic halogen compound were evaluated. As the filter paper phase an ordinary phase (Whatmann #1, filter paper) and reversed phase (liquid paraffin impregnated) were used.

• Journal of Pharmaceutical Investigation
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• v.27 no.2
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• pp.119-123
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• 1997

The physicochemical and structural properties of new capsaicin derivative, DA-5018, were examined. The reference standard of this compound was obtained by the recrystallization. A method for the determination of the dissociation constant of the compound is described. pH-solubility and distribution coefficient were determined by chromatographic method. Fundamental properties on thermal behaviors were investigated by TG, DTA and DSC. Structural analysis based on spectroscopic method coincided with the chemical structure of DA-5018. Approximate dissociation constant of the compound determined by UV spectral method was 9.35. Solubilities and partition coefficients in various pH buffer solution appeared pH-dependency. No crystal transition or further transition was found in the thermal analysis. This compound showed good stability, but pH 13 buffer and acetone made some degradative products.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2000.06a
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• pp.251-257
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• 2000

A numerical simulation of the temperature rise for sliding surface in dry contact is based on Jaeger's formula combined with a calculated heat input. A gear tooth temperature analysis was performed. The pressure distribution has the Hertzian pressure distribution on the heat source. The heat partition factor is calculated along line of action. A Temperature distribution of tooth surface is calculated about before and after profile modification. A Temperature of addendum and deddendum in modified gear have reduced.

• Proceedings of the PSK Conference
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• 2003.04a
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• pp.255.3-256
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• 2003

Marine Algae of order Chordariales are rich resources of bioactive metabolites. Methanolic extracts of the brown alga /shige Okamurae exhibited potent antioxidative and butyrylcholinesterase(BChE) inhibitory effects. Bio-guided purification [solvent partition, ODS flash, silica flash, gel-filtration on Sephadex LH 20, ODS HPLC] of them gave a compound 1. Its structure was elucidated by detailed analysis of spectroscopic data of 1 and comparison of literature data. A variety of bioassay for 1 is in progress.

• Proceedings of the PSK Conference
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• 2001.04a
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• pp.238.2-239
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• 2001

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2006.10a
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• pp.107-108
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• 2006

• Proceedings of the Korean Institute of Intelligent Systems Conference
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• 1993.06a
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• pp.985-988
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• 1993

An alternative approach to the design of application-driven fuzzy systems is proposed. A broad class of fuzzy systems applications requires a certain fuzzy partition of the input space while it demands for simple numerical quantities. For this class, a dedicated fuzzy system archictecture is presented and a design strategy is proposed. Both the single-input/single-output and multi-input/multi-output cases are considered. Numerical analysis are complete illustrating several aspects of the proposed framework.

• Proceedings of the PSK Conference
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• 2001.10a
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• pp.308.1-308.1
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• 2001