• 한국추진공학회지
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• 제13권6호
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• pp.41-47
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• 2009

작동 유체에 따른 APU 가스터빈에 적용되는 연료노즐의 분무특성을 확인하였다. 액체연료에 따라 점도, 표면장력 및 비중 등이 상이하여 분무특성이 변화될 수 있다. 본 연구에서는 연료 물성치 변화에 따른 분무특성을 이해하기 위하여 케로신과 유사한 특성을 갖는 보정 유체 2와 일반적으로 연료노즐의 분무특성을 시험하는데 사용하는 물을 이용하여 분무 시험을 수행하였다. 분무가시화와 분무입자 크기 및 분포를 ND-Yag 레이저 및 PDPA(Phase Doppler Particle Analyzer)를 이용하여 측정하였다. 분무시험 결과, 두 작동유체의 분무형태는 유사하게 나타났으며 주 분무영역에서의 SMD 또한 유사하게 분포됨을 확인할 수 있었다.

• 한국추진공학회지
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• 제4권1호
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• pp.36-45
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• 2000

지금까지의 충돌분무에 대한 연구는 제트의 충돌시 형성되는 액막의 분열 과정을 이해하고 이를 모델링하는데 초점을 두어왔기 때문에 실질적으로 연소 효율에 가장 큰 영향을 미치는 연료의 공간분포 특성에 대한 연구가 부족하였다. 따라서 본 연구에서는 like-doublet 충돌분사 노즐을 사용하여 연료 유량 플럭스의 단면분포 특성을 연구하였다. PDPA(Phase Doppler Particle Analyzer)를 통해 액적의 크기를 측정한 기존의 방법은 연료의 평면적인 분포특성을 이해하는데 상당히 제한적이었기 때문에 평면 레이저 유도형광기법(PLE : Planar Laser Induced Fluorescence)을 이용하여 분무의 단면 분포를 측정하였고, 직접사진을 통하여 액적의 크기도 측정하여 PLIF의 결과와 비교하였다.

• 한국세라믹학회지
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• 제44권10호
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• pp.562-567
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• 2007

To precipitate the complex gels of the pH 6, 7, 8, 9 included in a flux and an aluminum hydroxides gel, an aqueous solution of a mixture of $Na_2CO_3\;and\;Na_2PO_4{\cdot}12H_2O$ was added with stirring in an aqueous solution of a mixture of $Al_2(SO_4){_3}{\cdot}18H_2O,\;Na_2SO_4\;and\;K_2SO_4$, and then the complex gels were aged in 20 h at $90^{\circ}C$. As the hydrolysis pH changed, it had an effect on the physical properties such as the crystal structure, crystal morphology and a phase transition temperature of the AlO(OH) gel, and also on the crystal structure, crystal morphology, particle size and particle size distribution of the ${\alpha}-Al_2O_3$ platelets prepared by molten-salt precipitation. Also, in this study, the complex gels were crystallized at $1,200^{\circ}C$ and thereafter dried at $110^{\circ}C$, and then it was investigated to effect of the hydrolysis pH on the crystal structure, morphology and particle size distribution of the ${\alpha}-Al_2O_3$ platelets crystals using XRD, DTA, SEM and particle size analyzer.

• 자원리싸이클링
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• 제14권6호
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• pp.21-27
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• 2005

국내 은 함유 폐자원의 고부가가치 제품화를 위한 연구의 일환으로써 sodium formaldehydesulfoxy와 ascorbic acid를 각각 환원제로 사용한 Ag 나노분발의 제조실험을 수행하였다. Ag수용액은 질산은을 소정 농도로 증류수에 용해시켜 사용하였으며, Ag미립자의 응집방지를 위한 분산제로는 Tamol NN8906, PVP, SDS 및 caprylic acid를 각각 사용하었다. 환원반응을 통하여 제조한 Ag 미립자는 입도분석기 및 TEM측정을 통하여 morphology와 평균입도를 측정하였다. sodium formaldehydesulfoxylate 에 의한 은의 환원을 위해서는 이론치의 1.4배를 첨가해 주어야 하는 것으로 나타났으며, ascorbic acid와는 달리 생성된 Ag 입자가 너무 크게 성장하는 문제점이 있었다. 분산제에 따른 Ag 입자의 특성을 살펴본 결과, Tamol 및 PVP를 사용한 경우에는 bimodal distribution을 보였으나, SDS 와 caprylic acid의 경우에는 수십 nm에서 $100{\mu}m$에 이르는 매우 broad한 입도분포를 보였다.

• 대한기계학회논문집B
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• 제21권8호
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• pp.1056-1067
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• 1997

Present study visualized flow pattern and investigated spray characteristics of twin-fluid atomization with converging-diverging nozzles. Particle sizes were measured by using the Malvern particle analyzer, and the radial size distributions were evaluated by using the tomographic transform technique. The results show that the SMD generally increases in the radial direction at a prescribed liquid flow rate and the increasing rate in the SMD becomes gradual as atomizing gas pressure increases. The SMD decreases as the liquid flow rate increases at a fixed GLR (gas/liquid mass ratio). The atomization performance of the protrusion-type nozzle turned out to be superior to that of the flush-type. However, in the case of the protrusion-type, flow separation occurs outside the liquid delivery tube when the pressure at the gas nozzle chamber is high enough, which may deteriorate the atomization performance.

• Korean Chemical Engineering Research
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• 제51권6호
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• pp.685-691
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• 2013

이부프로펜은 비스테로이드성 소염진통제(Non-Steroidal Anti-Inflammatory Drugs; NSAIDs)의 대표적인 성분이다. 이부프로펜은 결정성이 크기 때문에 난용성이며, 따라서 생체이용률(bioavailability)도 낮다. 이와 같은 난용성을 개선하기 위해서는 이부프로펜의 입도를 감소시킬 필요가 있다. 본 연구의 목적은 이부프로펜의 분쇄조건을 최적화하는데 있다. 이부프로펜을 분쇄하기 위하여 유성밀을 사용하였으며, Box-Behnken 방법을 이용하여 분쇄변수들의 최적조건을 구하였다. 이부프로펜 분쇄생성물의 물성을 조사하기 위하여 입도, 결정크기 및 인장강도 측정에는 각각 입도분석기, XRD, tensile/compression tester를 사용하였다. 분쇄 최적조건은 밀회전수는 290 rpm, 시료장입량은 24.6 g, 분쇄시간은 10분이었으며, 이 조건에서 이부프로펜 분쇄생성물의 입도는 $13.5{\mu}m$이었다. 이부프로펜은 분쇄 후 결정크기가 감소하였다. 이부프로펜 분쇄생성물의 정제의 상대밀도가 0.85~0.90인 범위에서 그 정제의 인장강도는 $12{\sim}14Kg_f/cm^2$ 이었다.

• 한국자동차공학회논문집
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• 제4권1호
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• pp.177-186
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• 1996

A convolution alogorithm combined with Fourier transformation is applied to the tomographic reconstruction of the asymmetric spray structure to identify the local drop size and volume concentration. The line of sight intergrated data from Malvern particle analyzer with multiangular scanning form a basic information for the deconvolution. Linear interpolation is tested to obtain the effect of increasing number of scanning angles. This transformation method predicts well the structure of asymmetric spray. The tehnique can be extended to other line of sight combustion diagnostics.

• 한국자동차공학회논문집
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• 제9권5호
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• pp.75-81
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• 2001

This paper presents the atomization characteristics of single hole injector in the direct injection type diesel engine. The spray characteristics of fuel injector such as the droplet size and velocity were measured by phase Doppler particle analyzer. In this paper, the atomization characteristics of fuel spray are investigated for the experimental analysis of the measuring data by the results of mean diameter and mean velocity of droplet. The effect of fuel injection pressure on the droplet size shows that the higher injection pressure results in the decrease of mean droplet diameter in the fuel spray. The minimum size of fuel spray droplet appears on the location of 40mm axial distance from nozzle exit of diesel injector. Based on the experimental results, the correlation between the droplet diameter and mean velocity of the diesel spray due to the change of axial and radial distance from the nozzle tip were investigated.

• 한국신재생에너지학회:학술대회논문집
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• 한국신재생에너지학회 2007년도 춘계학술대회
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• pp.81-85
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• 2007

A fluidized bed reactor is made with quartz. The size of FBR is 0.055 m I.D. and 1.0 m in height. The FBR was employed for the thermocatalytic decomposition of propane to produce hydrogen without $CO_{2}$. The fluidized bed was proposed for the continuous withdraw of product carbons from the reactor. Carbon black DCC-N330 is used to decompose the propane gas. The propane decomposition reaction over carbon black catalyst in a fluidized bed reactor was carried out the temperature range of 600 ${\sim}$ 800 $^{\circ}C$, propane gas velocity of 1.0 ${\sim}$ 4.0$U_{mf}$($1U_{mf}$ = 0.61cm/s) and the catalyst loading of 100 ${\sim}$ 200g. Production of $H_{2}$ such as other reaction temperature, gas velocity, catalytic loading on the reaction rates was investigated. The carbon depositied on the catalyst surface was observed by FE-SEM. The particle size of the carbon black was observed by Particle size analyzer. Resulting production in the experiment was not only hydrogen but also several by-products such as methane, ethylene, ethane, and propylene.

• 한국의류산업학회지
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• 제10권3호
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• pp.371-376
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• 2008

Poly(ethylene-co-vinylacetate) (EVA) microspheres were prepared by thermally induced phase separation (TIPS) in toluene. The microsphere formation occurred by the nucleation and growth mechanism in metastable region. The effects of the concentration and component of the polymer and cooling rate on microsphere formation were investigated. The microsphere formation and growth were followed by the cloud point of the optical microscope measurement. The microsphere size distribution, which was obtained by particle size analyzer, became broader when the polymer concentration was higher, the content of vinyl acetate in EVA copolymer was higher, the cooling rate of EVA copolymer solution were lower. The content of disperse dye in EVA microsphere was obtained by TGA thermal analysis, the dye content of EVA15 and EVA18 were 3.5 and 2.0 wt% respectively.