• Title/Summary/Keyword: pH of suspension

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Effect of pH on the Synthesis of Hydroxyapatite (수산화아파타이트 합성시 pH의 영향)

  • 김수룡;이병민;박용갑
    • Journal of the Korean Ceramic Society
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    • v.28 no.11
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    • pp.885-891
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    • 1991
  • Calcium hydroxyapatite have been synthesized by a direct precipitation reaction between 0.05 M calcium hydroxide suspension and 0.3 M orthophosphoric acid solution. 0.01 M calcium hydroxide solution was added during the reaction in order to increase the total Ca/P mol ration and reaction pH of the solution. The stoichiometric hydroxyapatite was synthesized over 1.75 as total Ca/P mol ratio, but the calcium-deficient hydroxyapatite was prepared under 1.725 as total Ca/P mol ratio. The nonstoichiometry of the precipitates were interpreted in terms of the pH change during the reaction.

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Effect of intermittent low-intensity, short duration exercise on Type IImuscle of suspended rats (간헐적인 낮은강도, 짧은기간의 운동부하가 뒷다리 부유쥐의 Type II근육에 미치는 영향)

  • 최명애;지제근;김은희
    • Journal of Korean Academy of Nursing
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    • v.25 no.2
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    • pp.193-209
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    • 1995
  • The purpose of this study was to determine the effect of intermittent low - intensity, short duration exercise during hindlimb suspension on the mass, relative weight, myofibrillar protein content, cross-sectional area of Type I and Type II fibers and SDH activity in Type II(plantaris) muscle. To examine the effectiveness of intermittent low-intensity, short duration exercise on mass, myofibrillar protein content and fiber size, the hindlimbs of adult female Wistar rats were suspended(HS) and half of these rats walked on a treadmill for 45 min/day(9 min every 2h) at 5m /min and a 15$^{\circ}$grade (HS-EX). Plantaris wet weight was 19.67% significantly smaller(p<0.005) and relative plantaris weight was 6.25% smaller compared with those of control rats following seven days of hindlimb suspension. Plantaris wet weight and relative plantaris weight increased by 27.66%, 12.22% each through intermit-tent exercise during hindlimb suspension(p<0.005, p<0.05), moreover, plantaris wet weight and relative plantaris weight of the HS-EX rats were similar to those of control rats. Soleus wet weight and relative soleus weight decreased significantly by 31% and 22.0% in the HS rats(p<0.05). Soleus wet weight and relative soleus weight increased by 10.41%, 25.64% respectively through intermittent ex-ercise during hindlimb suspension, furthermore, soleus wet weight and relative weight of the HS-EX rats were closer to those of control rats. Myofibrillar protein content of plantaris and soleus decreased significantly by 51.49%, 59.65% each, following seven days of hindlimb suspension (p<0.005) Myofibrillar protein content of plantaris and soleus increased by 51.79%, 75.47% each with significance through intermittent exercise during hindlimb suspension(p<0.005). Myofibrillar protein content of plantaris and soleus in HS-EX rats was smaller than that of control rats. No change was observed in fiber type percentage following 1 week of hindlimb suspension or exercise during hindlimb suspension. The type I fiber cross-sectional area of both soleus and plantaris muscle was 18.72% and 41.07% lower in the HS than that of the controls (p<0.05, p<.001), that of both muscles was 6.60% and 29. 3% greater in the HS-EX than that of the HS rats. HS plus intermittent low- intensity short duration exercise resulted in Type I fiber cross-sectional area closer to the controls. Type II fiber cross-sectional area of both plantaris and soleus muscle was 22.45% and 22.58% sl nailer in the HS than in the controls, that of both muschles in the HS-EX was 14.10%, 5.78% greater than HS. Intermittent exercise during hindlimb suspension resulted in Type I, II fiber cross-sectional area closer to the control value. There was no change in SDH activity following 1week of hindlimb suspension or exercise during hindlimb suspension in the plantaris muscle. The results suggest that intermittent low intensity short duration exercise can ameliorate Type II muscular atrophy Induced by hindlimb suspension.

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Synthesis of Resole-type Phenolic Beads via Suspension Polymerization Technique (현탁중합을 이용한 레졸형 구형 페놀입자의 합성)

  • Hahn, Dongseok;Kim, Daejung;Kim, Hongkyeong
    • Korean Chemical Engineering Research
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    • v.51 no.2
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    • pp.279-284
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    • 2013
  • The phenolic beads in macrosize range were obtained by suspension polymerization at $98^{\circ}C$ from phenol and formaldehyde in the presence of basic catalyst with a phenol to formaldehyde (P/F) range of 1:1~1:4, and they were carbonized to spherical carbon beads under nitrogen at $700^{\circ}C$. Thermal analysis on spherical phenolic beads obtained by suspension polymerization showed that the postcuring process is essential. In order to optimize the suspension polymerization, the effects of the P/F molar ratio, the pH of catalyst, and the molecular weight of stabilizer on the size distribution and yield of spherical phenol beads were examined separatively. The particle size was increased whereas the yield was decreased with P/F molar ratio. The increasing basicity of catalyst made the particle size to increase, while the molecular weight of stabilizer had more effect on the yield rather than on the particle size distribution. The thermal stability of the spherical phenolic beads obtained through postcure was also examined by TGA. The phenol beads of high P/F ratio still showed the weight loss at $220^{\circ}C$ even after postcure due to the high possibility of dibenzyl ether, while those of low P/F ratio showed the steady decrease in weight during $220^{\circ}C$ to $400^{\circ}C$, which showed that the optimal P/F ratio was 1:2.

The Effects of Various Hormones on Growth of Carrot Tissue Culture (당근 배양세포의 생육에 미치는 수종 Hormone의 영향)

  • 강영희
    • Journal of Plant Biology
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    • v.20 no.2
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    • pp.63-69
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    • 1977
  • Experiments were conducted to investigate the effects of several hormones on the growth of suspension culture of carrot (Daucus carota L.) cells, where changes in pH and the amount of $NH_4-Nin$ the medium were observed with regard to growth. A treatment with 2,4-D at $10^{-5}M$ resulted in a highest rate of growth; the hormone at this concentration caused an increase in dry weight by about 40 to 50% over the control, measured at a stationary phase. It was thus indicated that 2,4-D at $10^{-5}M$ provided the optimal condition for the suspension culture. Changes in pH of the medium were found to be affected by hormonal treatments during the first 2-3 days following the inoculation, after which the pattern of pH changes in hormone enriched media paralleled that of the control. Subsequent changes of $NH_4-N and NO_3-N$ from the medium by the cells, and also by growth of the cells. The uptake of $NH_4-N$ by the cells did not appear to be influenced by hormonal treatments. At a stationary phase, a considerable amout of $NO_3-N$ played a more important role than $NH_4-N$ in the growth of the carrot cell suspension culture.

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Effects of Synthetic Temperature and Suspension Stability of CeO2 Abrasive on CMP Characteristics (CeO2 연마입자의 합성온도와 수계안정성이 CMP 특성에 미치는 영향)

  • 임건자;김태은;이종호;김주선;이해원;현상훈
    • Journal of the Korean Ceramic Society
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    • v.40 no.2
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    • pp.167-171
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    • 2003
  • CMP(Chemical Mechanical Planarization) slurry for STI process is made by mechanically synthesized$CeO_2$as abrasive. The abrasive can be stabilized by electrostatic or steric stabilization in aqueous slurry and steric stabilization is more effective for long-term stability. Blanket-type$SiO_2$and $Si_3N_4$ wafers are polished with CMP slurry containing$CeO_2$synthesized in 50$0^{\circ}C$ or $700^{\circ}C$. Removal rate and surface uniformity of$SiO_2$and$Si_3N_4$wafer and selectivity are influenced by synthetic condition of abrasive, suspension stability and pH of slurries.

Preparation of Cordierite sols in Aqueous Media and Sintering Behavior of Cordierite Ceramics (수용액 매체로부터 코디어라이트 졸의 제조 및 코디어라이트 세라믹스의 소결거동)

  • Kim, Jae-Won;Kim, Hyeon-Cheol;Kim, Du-Hyeon;Seo, Seong-Mun;Jo, Chang-Yong;Choe, Seung-Ju;Kim, Jae-Cheol
    • Korean Journal of Materials Research
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    • v.10 no.3
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    • pp.233-240
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    • 2000
  • In order to fabricate dense cordierite ceramics without sintering aid, thermal behavior of Mg-Al-Si compounds during sintering was investigated. The dispersibility of cordierite suspension in aqueous media was measured by ESA(electrokinetic sonic amplitude). To prevent aggregation and insufficient dispersion of the cordierite sol, the pH of the suspension was controlled to 1.03 and 8.30 by adding $2N\;HNO_3$ and $2N\;NH_4OH$, respectively. Magnesium-aluminum-silicate complex gel coexisted in the specimen which has been gelled at $150^{\circ}C$ fir 12 hours, however several metastable phase such as ${\mu}-cordierite(Mg_2Al_4Si_5O_{18}),\;spine(MgAl_2O_4)\;and\;mullite(Al_6Si_2O_{13})$ existed below $1300^{\circ}C$ Nucleation rates of the two suspension were similar, but densification of the gel was sensitive to the pH of the sol. Densification of the sol with the pH of 8.3 was more pronounced than that of the sol with pH of 1.63.

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Production of monoterpenoid flavor compounds by suspension culture of peppermint cells (페파민트 세포의 현탁 배양시 생육 및 정유생성 특성)

  • Kim, Jin-Hwan;Lee, Hyong-Joo
    • Applied Biological Chemistry
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    • v.35 no.6
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    • pp.443-448
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    • 1992
  • To investigate the production of monoterpenoids by Mentha pipperita cells in suspension culture, effects of media formulation, plant growth hormones, initial pH of the media, and cold stress on the production of essential oil and menthol were analyzed. Among the media employed, Lin-Staba medium resulted in the best essential oil production. Addition of 100 mg/l of yeast extract to the Lin-Staba medium induced the cells to produce large amount of essential oil and high content of menthol (0.39 g/l and 19.6%, respectively). In the effect of plant growth hormone, auxine were more effective than cytokinins. At initial pH of 4.7, oil production was good but menthol content was low. However at pH 5.7 the trend was reversed. When the culture temperature was lowered from $27^{\circ}$ to $10^{\circ}$ during 6 hour-dark period, growth was not changed much but essential oil production and menthol content was increased and reached to 528 mg/l and 21%, respectively.

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Effect of Periodic Low-intensity Exercise on the Hindlimb Muscles of Hindlimb Suspended Rats (주기적인 운동이 뒷다리 부유에 의해 유발된 쥐의 뒷다리를 위축경감에 미치는 영향)

  • Choe, Myoung-Ae;Shin, Gi-Soo
    • Journal of Korean Biological Nursing Science
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    • v.1 no.1
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    • pp.71-85
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    • 1999
  • The purpose of this study was to determine the effect of periodic low-intensity exercise during hindlimb suspension on the mass, relative weight, myofibrillar protein content in soleus, plantaris and gastrocnemius muscles. To examine the effectiveness of periodic low-intensity exercise on mass, and myofibrillar protein content of hindlimb muscles, adult female Wistar rats were suspended(HS) and half of these rats walked on a treadmill for 45min/day(15 min every 4h) at 5m/min and a $15^{\circ}$ grade(HS-EX). Soleus wet weight was 33.51% significantly smaller(p<0.005) and relative soleus weight of hindlimb suspended rats was 31.96% smaller(p<0.005) compared with those of control rats following seven days of hindlimb suspension. Plantaris wet weight was 7.5% smaller(p<0.01) and relative plantaris weight was 11.83% smaller(p<0.05) compared with those of control rats following seven days of hindlimb suspension. Gastrocnemius wet weight was 11.31% significantly smaller(p<0.005) and relative gastrocnemius weight was 17.13% significantly smaller(p<0.005) compared with those of control rats following seven days of hindlimb suspension. Soleus wet weight while increased by relative soleus weight increased by 25.13%, 27.59% each through periodic low intensity exercise during hindlimb suspension(p<0.05, p<0.05). Plantaris wet weight and relative plantaris weight increased by 1.04%, 10.98%(p<0.05) each, and gastrocnemius wet weight and relative gastrocnemius weight increased by 1.98%, 12.02%(p<0.05) each through periodic low intensity exercise during hindlimb suspension. Wet weight of soleus, plantaris and gastrocnemius in HS-EX rats did not recover to control level. Myofibrillar protein content of soleus, plantaris and gastrocnemius was 48.24%, 40.85% and 37.33% significantly smaller(p<0.005) respectively compared with those of control rats following seven days of hindlimb suspension. Myofibrillar protein content of soleus, plantaris and gastrocnemius increased by 40.68%, 25.07% and 17.93%(p<0.005) each through periodic low intensity exercise during hindlimb suspension. Myofibrillar protein content of soleus, plantaris, and gastrocnemius in HS-EX rats did not recover to control level. The results suggest that periodic low intensity exercise can attenuate hindlimb muscle atrophy induced by hindlimb suspension.

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Effects of Change in Soil pH and Treatment of Gibbsite and Organic Matter on Sulfate Adsorption in Soils (Gibbsite와 유기물(有機物) 처리(處理) 및 pH변화(變化)가 토양(土壤)의 SO4= 흡착(吸着)에 미치는 영향(影響))

  • Yoon, Sun-Kang;Yoo, Sun-Ho
    • Korean Journal of Soil Science and Fertilizer
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    • v.19 no.2
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    • pp.107-113
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    • 1986
  • Laboratory experiments were carried out to investigate the effects of pH, gibbsite, and organic matter on sulfate adsorption by soils. Samples of five soil series (Songjeong, Gopyung, Yeasan, Gyorae, and Namwon), different in physical and chemical properties, were used in this study. The results obtained from sulfate adsorption experiment with sulfate solutions of the concentrations ranging from 50 to 400 ppm were as follows: 1. The adsorption phenomena for five soils were well described by the Freundlich adsorption isotherm over a given range of sulfate concentration. 2. The amounts of sulfate adsorbed and K value of Freundlich adsorption isotherm increased as the initial pH of the suspension decreased. 3. Although the changes in pH of the suspension on the adsorption equilibrium were hardly observed in the soil treated with gibbsite, the sulfate adsorption rates were increased with amount of gibbsite treated. 4. The effects of pH of the suspension on the adsorption rates in the soils treated with gibbsite were remarkable at the level of 0.1% but were little at the level of 1.5%. 5. The adsorption rates of soils, treated with organic matter and incubated for three weeks, were in the order: starch > straw > compost. At the relatively high levels (5 and 10%) of treatments, compost treatment resulted in the sulfate desorption phenomena.

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