• Bulletin of the Korean Chemical Society
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• 제34권11호
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• pp.3307-3311
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• 2013

A new fiber optical sensor was developed for the determination of 2,4-dichlorophenol (DCP). The sensor was based on DCP oxidation by oxygen with the catalysis of iron(III) tetrasulfophthalocyanine (Fe(III)PcTs). The optical oxygen sensing film with $Ru(bpy)_3Cl_2$ as the fluorescence indicator was used to determine the consumption of oxygen in solution. A lock-in amplifier was used for detecting the lifetime of the oxygen sensing film by measuring the phase delay change of the sensor head. The different variables affecting the sensor performance were evaluated and optimized. Under the optimal conditions (i.e. pH 6.0, $25^{\circ}C$, Fe(III)PcTs concentration of 0.62 mg/mL), the linear detection range and response time of the sensor are $1.0{\times}10^{-6}-9.0{\times}10^{-6}$ mol/L and 250 s, respectively. The sensor displays high selectivity, good repeatability and stability, and can be used as an effective tool in analyzing DCP concentration in practical samples.

• Bulletin of the Korean Chemical Society
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• 제27권9호
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• pp.1418-1422
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• 2006

In this work the construction of a novel poly(vinyl chloride) membrane sensor based on 2,2'-dianiline disulfide (DADS) as a neutral carrier, o-nitrophenyloctyl ether (NPOE) as a plasticizer and sodium tetraphenyl borate (NaTPB) as an anionic site with unique selectivity towards Tm(III) ions is reported. The electrode has a linear dynamic range between $1.0\;{\times}\;10^{-6}$ and $1.0\;{\times}\;10^{-2}$ M, with a nice Nernstian slope of 19.5 ${\pm}$ 0.3 mV per decade and a detection limit of $4.0\;{\times}\;10^{-7}$ M at the pH range of 4.8-8.5. It has a very fast response time (<15 s) in the whole concentration range, and can be used for at least 4 weeks without any considerable divergence in the electrode potentials. The proposed sensor revealed comparatively good selectivity with respect to most common metal ions, and especially lanthanide ions. It was used as an indicator electrode in the potentiometric titration of Tm(III) ions with EDTA and in direct determination of concentration of Tm(III) ions in binary mixtures. It was also applied in determination of fluoride ions in mouth wash preparations.

• Bulletin of the Korean Chemical Society
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• 제25권2호
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• pp.172-176
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• 2004

A highly selective membrane electrode based on1,3,5-triphenylpyrylium perchlorate (TPPP) is presented. The proposed electrode shows very good selectivity for sulfate ions over a wide variety of common inorganic and organic anions. The sensor displays a nice Nernstian slope of -29.7 mV per decade. The working concentration ranges of the electrode is 1.0{\times}10^{-1}-6.3{\times}10^{-6} $M with a detection limit of $4.0{\times}10^{-6}$ M (480 ng per mL). The response time of the sensor in whole concentration ranges is very short (< 6 s). The response of the sensor is independent on the pH range of 2.5-9.5. The best performance was obtained with a membrane composition of 32% PVC, 59% benzyl acetate, 5% TPPP and 4% hexadecyltrimethylammonium bromide. It was successfully used as an indicator electrode for titration of sulfate ions with barium ions. The electrode was also applied for determination of salbutamol sulfate and paramomycine sulfate.

• 한국공작기계학회논문집
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• 제17권4호
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• pp.75-80
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• 2008

This paper presents an atomic force probe for triggering coordinate measuring machines(CMMs). A rigorous comparison is made between touch trigger probe and atomic force probe for CMMs. Typical CMMs(touch trigger probe based CMMs) often lead to some errors associated with object curvature and difference in triggering sensitivity. Their applicability is limited only to hard objects. The aim of this work is to develop a trigger sensor for CMMs using atomic force. In order to show the applicability of atomic force as a trigger sensor, a cylindrical shape is measured with a CMM and an atomic force microscope. Three different touch probe heads with different ball sizes are tested. The experiments show that smaller ball provides better results for curved objects. The experimental results also show that the performance of atomic force as a trigger sensor is about that of the smallest ball probe. In addition, experiments are also performed to measure soft objects. Finally, this paper suggests and verifies a trigger sensor using atomic force for CMMs.

• 대한후두음성언어의학회지
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• 제10권1호
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• pp.50-57
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• 1999

A study to get the data of normal stop consonants production as preliminary study for cleft palate patients was performed. Normal Korean native 21 speakers were pronounced $VCV(V=/a/,C=/P/,/{P^1}/,/P^h/,/t/,/{t^1}/,/{t^h}/,/k/,/{k^1}/,/{k^h}/)$ syllables with natural speech rate and intensity. With intrapharyngeal pressure waveforms by pressure sensor in oropharyngeal cavity, amplitude and time duration of intrapharyngeal pressure were analyzed, and with acoustic waveforms and spectrograms, closure duration and VOT were analyzed. As results, the highest amplitude of intrapharyngeal pressure showed in alveolars and heavily aspirated consonants. Velars and unaspirated consonants were higher than bilabials and slightly aspirated ones each, in intrapharyngeal pressure. Bilabilas, alveolars and velars showed similar rise time of intrapharyngeal pressure build-up, but in decay time and total duration time, bilabials were slightly shorter than alveolars and velars, with no statistic significance. In the aspects of tensity, unaspirated consonants showed the longest rise time, heavily aspirated, the second, and slightly aspirated consonants, the shortest, which were also seen in decay time and total duration time. In closure duration, slightly aspirated consonants had the shortest closure duration, and the heavily aspirated ones, the second, and unaspirated consonants showed the longest. In VOT, heavily aspirated consonants showed the longest, slightly aspirated ones, the second and unaspirated ones showed the shortest.

• 대한의용생체공학회:학술대회논문집
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• 대한의용생체공학회 1997년도 추계학술대회
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• pp.395-398
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• 1997

Human pulse represents the physical characteristics of heart and cardiovascular system. Therefore, malfunctions and errors of heart and cardiovascular system can be determined by using an automatic diagnosis system that can detect the pulse signal. Not only will the computerised system preclude the possibilities of observational errors by giving an accurate measurement with great stability, but minimize the possibilities of misinterpretation by using an automated diagnostic logic. A new combinational fiber-optic sensor, which has a detecting part and a transmitting part was used to acquire radial pulse signal noninvasively. The development of P-5 transducer makes it possible to obtain more effective detection and obvious display of pulse signals in the aspect of reliability. Using P-5 transducer in the field of plethysomography and MAC- JIN, one of our diagnoses in Korean traditional medicine, it is expected that we can ontain quantitative and valuable information or the diagnosis of human pulses.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2004년도 춘계학술대회 논문집 전기설비전문위원
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• pp.132-135
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• 2004

In generally, compared with VHF band, electromagnetic waves of UHF band have a low influence for external noise. We can detect the real abnormality with several pC in GIS using UHF method. Recently, it has applied to use the external UHF sensor attached on spacer to GIS of existing substation. In this paper, we firstly described the technique of the partial discharge measurement using frequency analysis and phase analysis in UHF band. Secondly, we presented the results of sensitivity, the relationship of dBm-pC and diagnosis of the reason of PD source by phase analysis. And then, we report the diagnosis result of partial discharge on 800kV GIS in domestic substation. rge diagnosis of GIS.

• 센서학회지
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• 제19권3호
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• pp.214-220
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• 2010

Three-dimensional(3D) structure of specific DNA can be changed between two conformations under an external environmental transition such as pH and salt concentration variations. We have experimentally observed the conformational transitions of i-motif DNA using AFM cantilever bioassay. It is shown that pH change of a solvent induces the bending defleciton change of a cantilever functionalized by i-motif DNA. This indicates that cantilever bioassay enables the label-free detection of DNA structural changes upon pH change. It is implied that cantilever bioassay can be a de novo route to quantitatively understand the conformational transitions of biological molecules under environmental changes.

• Journal of Microbiology and Biotechnology
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• 제33권2호
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• pp.228-234
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• 2023

In this study, the performance of a gold biosensor combined with light microscope imaging system (GB-LMIS) was comparatively evaluated against enzyme-linked immunosorbent assay (ELISA) for detecting Salmonella under simulated chilling condition. The optimum concentration of antiSalmonella polyclonal antibodies (pAbs) was determined to be 12.5 and 100 ㎍/ml for ELISA and GBLMIS, respectively. GB-LMIS exhibited a sufficient and competitive specificity toward three tested Salmonella among only. To mimic a real-world situation, chicken was inoculated with Salmonella cocktail and stored under chilling condition for 48 h. The overall growth of Salmonella under chilling condition was significantly lower than that under non-exposure to the chilling condition (p < 0.05). No significant differences in bacterial growth were observed between brain heart infusion and brilliant green broth during the enrichment period (p > 0.05). Finally, both GB-LMIS and ELISA were employed to detect Salmonella at every 2-h interval. GB-LMIS detected Salmonella with a competitive specificity by the direct observation of bacteria on the sensor using a charge-coupled device camera within a detection time of ~2.5 h. GB-LMIS is a feasible, novel, and rapid method for detecting Salmonella in poultry facilities.

• 한국수자원학회:학술대회논문집
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• 한국수자원학회 2020년도 학술발표회
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• pp.142-142
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• 2020

하천에서의 화학사고는 자연적 및 인위적인 원인으로 인해 발생할 수 있으며, 대량의 화학물질이 하천으로 유입되는 것을 말한다. 이러한 화학사고는 수환경의 변화를 야기해 생태계나 인간에게 악영향을 초래하여 심각한 문제가 발생 될 수 있다. 하천으로 유입된 화학물질의 정량적 평가에 대한 연구는 활발하게 진행되고 있지만, 화학사고 초기 대응을 위한 하천에서의 화학물질 감지에 대한 연구는 미비한 실정이다. 한국 하천의 주요 지점에는 pH 및 EC 등을 실시간으로 측정하는 자동측정망을 운영하고 있기 때문에 이러한 측정항목들을 활용하여 화학물질을 감지하거나 식별 가능성에 대한 평가 연구는 하천 화학사고 대응을 위한 중요한 기초자료로 활용될 수 있다. 또한 분석된 결과를 바탕으로 미지의 화학물질을 다른 용매에 적용 시켰을 때 변화되는 pH 및 EC 결과와 통계적 수치비교를 통해 미지의 화학물질 식별 가능성을 평가하였다. 이를 통해 본 연구에서 선정한 pH 및 EC 항목이 화학물질 감지 및 식별을 위한 대체지표로써의 활용 가능성을 실험적 연구를 통해 평가하고자 하였다. 본 연구의 결과는 현장에서 쉽고, 신속하게 화학물질 감지 및 식별을 위한 정보를 제공할 수 있다는데 의미가 있으며, 화학사고의 신속한 대응을 위한 기초자료로 활용될 수 있을 것으로 판단된다.