• Title/Summary/Keyword: optimum mixture ratio

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Optimization of β-Cyclodextrin Recycling Process for Cholesterol Removal in Cream

  • Kwak, H.S.;Suh, H.M.;Ahn, J.;Kwon, H.J.
    • Asian-Australasian Journal of Animal Sciences
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    • v.14 no.4
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    • pp.548-552
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    • 2001
  • This study was designed to find optimum conditions of four different factors (ratio of solvent to cholesterol-$\beta$-cyclodextrin complex, mixing speed, mixing temperature, and mixing time) for cholesterol dissociation in cream. Using the ratio of 6 to 1 (solvent to the complex) showed the highest cholesterol dissociation rate (82.50%) when mixed at 100 rpm at $50^{\circ}C$ for 1 h. Mixing speed did not significantly affect the cholesterol dissociation. Also, mixing time appeared to be insignificant. The optimum mixing temperature was $50^{\circ}C$ and mixing at $40^{\circ}C$ resulted in a significantly lower rate, compared with that at $50^{\circ}C$. In a subsequent experiment, using recycled $\beta$-cyclodextrin only showed 75.07% of cholesterol removal in cream, while the mixture of recycled to unused $\beta$-CD with the ratio of 6 to 4 increased cholesterol removal to 95.59%, which is highly close to that of 100% unused $\beta$-CD.

Optimization of Makgeolli Manufacture Using Several Sweet Potatoes (다양한 고구마를 이용하여 제조한 막걸리의 최적화)

  • Cheon, Ji-Eun;Baik, Moo-Yeol;Choi, Sung-Won;Kim, Chang-Nam;Kim, Byung-Yong
    • The Korean Journal of Food And Nutrition
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    • v.26 no.1
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    • pp.29-34
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    • 2013
  • The objective of this study was to manufacture three kinds of domestic sweet potato Makgeolli using a mixture design and an optimization technique. The effects of four different manufacture methods, such as simultaneous saccharification and fermentation (SSF) with or without malt and separate hydrolysis and fermentation (SHF) with or without malt were determined. The SSF methods of Makgeolli produced higher alcohol content than that of SHF methods. The sensory score was not influenced by different making methods. Fourteen experimental points were selected, and rice (10~50%), sweet potato (10~50%) and water (40~60%) were chosen as independent variables. The measured responses were sensory preference, total polyphenol content, and DPPH radical scavenging activities. The ratio of the optimum sweet potato Makgeolli mixture formulation was developed as 15.11 (rice): 44.89 (sweet potato): 40 (water) using the optimization technique. The desirability of the optimum mixture formulation was 0.839. Yellow sweet potato Makgeolli using the optimum mixture formulation produced higher soluble sugar content compared to others. Regular sweet potato Makgeolli produced higher pH. The purple sweet potato Makgeolli's total polyphenol content and DPPH radical scavenging activity were measured to be the highest at $771.91{\pm}1.42mg\;GAE/{\ell}$, $131.55{\pm}4.03%$.

Separation of 20(R&S) Prosapogenin Isomers of Ginsenoside-$Rg_2$ and -$Rg_3$ from Ginseng Saponins by Reversed-Phase High Performance Liquid Chromatography (인삼 사포닌에서 Ginsenoside-$Rg_2$와 -$Rg_3$의 이성질체인 20(R&S) Prosapogenin들의 역상 고속 액체 크로마토그래피에 의한 분리)

  • Jeong, Seung-Il;Kim, Cheon-Suk;Lee, Yong-Gu;Lee, Ho-Sup;Kim, Il-Kwang
    • Analytical Science and Technology
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    • v.11 no.5
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    • pp.404-408
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    • 1998
  • Using a reversed-phase high performance liquid chromatography, the separation of 20(S)-, 20(R)-prosapogenin stereo-isomers of ginsenoside-$Rg_2$ and of ginsenoside-$Rg_3$ in ginseng saponins has been carried out with binary solvent system. The optimum conditions for the isomer separation are as following: Nova-$Pak^{(R)}C_{18}$ (Waters, $3.9{\times}150mm$) column, $CH_3CN/CH_3CN$ (100:8, v/v) binary solvent system and the flow rate was 1.7 mL/min. The stereoisomers were separated with change of the mixture ratio of the solvent system, the solvent elution by gradient program, and then detected at 203 nm of UV detector. The simultaneous separation of mixture that were the $Rg_2$, $Rg_3$ isomers was easily performed in nonpolar solvent for $Rg_2$, polar solvent for $Rg_3$ at the same optimum conditions.

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Effects of Phosphate Complex the Functional Properties of Fish Meat and Animal Meat of Mixture Pastes -Effect of Properties on the Quality Stability and Technical- (인산성 첨가에 따른 혼합 연육제품에 관한 연구 -품질 및 기능적 성질에 미치는 영향-)

  • 홍종만
    • The Korean Journal of Food And Nutrition
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    • v.3 no.1
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    • pp.39-56
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    • 1990
  • The effects of six kinds of phosphate complex on the water holding capacity (W.H.C) and protein solubility of hair tail, yellow tail runner and dried pollack meat paste were investigated and animal meat(pork, chicken and hare meat complex) The formulation of six kind of phosphate complex employed to this experiment were made by mixing several phosphate such as sodium polyphosphate, sodium pyrophosphate, sodium acid pyrophosphate, potassim pyrophosphate, sodium ultra-meta-phosphate, sodium-tetra-phosphate and monoglyceride at different mixture ratio Among the six kinds of phosphate complex, phosphate B complex which was formulated by mixing sodium polyphosphate 40%, sodium pyrophosphate 30%, sodium tetra mata phosphate 10%, sodium ultra meta phosphate 10% was most effective on enchanging the W H. C, and protein solubility of hair tail, yellow tail runner dried pollack meat past and in case of pork, chicken and hare meat paste. Phosphate C complex which was formulated by mixing sodium polyphosphate 50%. sodium pyrophosphate 30%, sodium tetra meta phosphate 10%, potassium pyrophosphate 10%, was more effective them other phosphate complex, and thief optimum addition level was 0.5% respectively in weight of fish meat paste. Texture characteristics such as hardness, cohesiveness and springiness value of Kamaboko(fish meat and pork, chicken, hare meat complex past meat product) were evaluted as best when 0.5% of Phosphate B complex was added The optimum cooking condition of Kamaboko to get good texture was heating for 20 minutes at 12$0^{\circ}C$.

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Effect of Co-initiator on the Size Distribution of the Stable Poly(Styrene-co-Divinylbenzene) Microspheres in Acetone/Water Mixture

  • Choi, Jin-Young;Lee, Kang-Seok;Lee, Byung-Hyung;Choe, Soon-Ja
    • Macromolecular Research
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    • v.17 no.7
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    • pp.483-490
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    • 2009
  • Stable poly(styrene-co-divinylbenzene) [P(St-co-DVB)] micro spheres with narrow size distribution were synthesized in the presence of 2,2'-azobis(2,4-dimethyl valeronitrile) (V-65) and co-initiator in an acetone/water mixture in the precipitation polymerization at $53^{\circ}C$ for 24 h. Potassium peroxodisulfate (KPS), ammonium peroxodisulfate (APS) and sodium peroxodisulfate (NaPS) were used as co-initiators. The optimum ratio of acetone to water for the formation of a narrow distribution of P(St-co-DVB) particles was 49:11 (g/g). The optimum co-initiator compositions for narrow distribution were 9:1 (g/g) for V-65 to KPS, 11:1 for V-65 to APS and 6:1 for V-65 to NaPS. The yield for these compositions was $54{\sim}57%$ and the largest particle size was obtained with the lowest zeta-potential and CV values. From the XPS measurements, the charge density was increased but the zeta potential decreased with increasing sulfur content, implying that the sulfate group provides the electrostatic stabilization on the particle surface. This suggested that the self-crosslinking between styrene and DVB, the electrostatic stabilization of initiators, and the balanced hydrophobic and hydrophilic properties of the solvents are responsible for the formation of stable P(St-co-DVB) spherical particles with narrow size distribution.

Effects of Fly Ash and Gypsum Mixture on Reducing Phosphorus Loss from Paddy Soil (논 토양에서 석탄회와 석고의 혼합제를 활용한 인산유출 저감)

  • Lee, Yong-Bok;Lee, Seul-Bi;Oh, Ju-Hwan;Lee, Chang-Hoon;Hong, Chang-Oh;Kim, Pil-Joo
    • Korean Journal of Environmental Agriculture
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    • v.27 no.1
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    • pp.66-71
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    • 2008
  • Phosphorus transfer from agricultural soils to surface waters is an important environmental issue. Fly ash and phospho-gypsum which are industrial by-product were investigated as a means of reducing dissolved phosphorus in arable soil. To determine the optimum mixing ratio of fly ash(FA) and phospho-gypsum(PG) for reducing dissolved reactive P(DRP) in soil, various mixture ratio of FA and PG were mixed with two soil. The DRP content and pH in soils were analysed after 3 weeks incubation under flooding condition. Although DRP content in soils was significantly decreased by FA-PG mixture compared with control, there were no significant difference among the FA and PG mixture ratio of 75:25, 50:50, and 25:75. The mixture of 75% FA and 25% PG was selected for field test. A field experiment was carried out to evaluate the reducing DRP content in paddy soil to which 0(NPK), 20(FG 20), 40(FG 40), and 60(FG 60) Mg $ha^{-1}$ of the mixture were applied. The DRP content was reduced by 31% at the application rate of 60 Mg $ha^{-1}$. In contrast to deceasing DRP, Ca-P content increased significantly with the mixture application rate. After rice harvesting, available $SiO_2$, P, and exchangeable Ca content in soil increased significantly with application rate due to high content of Si, P, and Ca in the mixture. Mixtures of fly ash and gypsum should reduce P loss from paddy soil and increase soil fertility.

The Study of Appropriate Mixture Ratio and Replacement Ratio of Bottom Ash Mixture Compaction Pile in Soft Ground (연약지반에서 저회혼합다짐말뚝의 적정 혼합비 및 치환율 산정에 관한 연구)

  • Do, Jong Nam;Chu, Ick Chan;Chae, Hwi Young;Chun, Byung Sik
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.32 no.4C
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    • pp.139-147
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    • 2012
  • In this study, various laboratory tests using bottom ash, which has similar engineering properties with sand, were conducted in order to solve the problem of clogging in granular compaction pile and to address sand supply and demand. In particular, testing was performed to help reduce clogging and minimize voids in a crushed stone compaction pile constructed in soft ground. Based on compaction tests and large diameter direct shear tests, an optimum mixing ratio was determined to be 80:20 (crushed stone to bottom ash) because an 80:20 mixing ratio showed the highest shear strength. Test results showed that as the bottom ash content increased above 20%, internal friction angle decreased. Another test method showed freezing and thawing had little effect when the replacement ratio was over 40%. Therefore, bottom ash mixed compaction piles in soft ground are most economical at a 40% replacement ratio.

Concrete Optimum Mixture Proportioning Based on a Database Using Convex Hulls (최소 볼록 집합을 이용한 데이터베이스 기반 콘크리트 최적 배합)

  • Lee, Bang-Yeon;Kim, Jae-Hong;Kim, Jin-Keun
    • Journal of the Korea Concrete Institute
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    • v.20 no.5
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    • pp.627-634
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    • 2008
  • This paper presents an optimum mixture design method for proportioning a concrete. In the proposed method, the search space is constrained as the domain defined by the minimal convex region of a database, instead of the available range of each component and the ratio composed of several components. The model for defining the search space which is expressed by the effective region is proposed. The effective region model evaluates whether a mix-proportion is effective on processing for optimization, yielding highly reliable results. Three concepts are adopted to realize the proposed methodology: A genetic algorithm for the optimization; an artificial neural network for predicting material properties; and a convex hull for evaluating the effective region. And then, it was applied to an optimization problem wherein the minimum cost should be obtained under a given strength requirement. Experimental test results show that the mix-proportion obtained from the proposed methodology using convex hulls is found to be more accurate and feasible than that obtained from a general optimum technique that does not consider this aspect.

Least Cost and Optimum Mixing Programming by Yulmu Mixture Noddle (율무국수를 이용한 최소가격/최적배합 프로그래밍)

  • Kim, Sang-Soo;Kim, Byung-Yong;Hahm, Young-Tae;Shin, Dong-Hoon
    • Korean Journal of Food Science and Technology
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    • v.31 no.2
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    • pp.385-390
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    • 1999
  • Noodle was made using a combination of yulmu, wheat and water through mixture design. Statistical models of yulmu noodle were shown by analysing tensile stress and color $(L^{*})$, and sensory evaluation with other constraints. Analysing the linear and non-linear model, the linearity in the values of tensile stress, lightness $(L^{*})$ and sensory evaluation showed that each component worked separately without interactions. In studying the component effect on the response by trace plot, the result indicated that the increase in the amount of yulmu enhanced tensile stress of noodle while degrading $L^{*}$ value and sensory evaluation score. In the range of satisfying the conditions of noodle in every tensile stress, $L^{*}$ value and sensory evaluation point, the optimum mixture ratio of yulmu : wheat : water was 2.27% : 66.28% : 28.45% based on least cost linear programming. In this calculation, the least cost was 9.924 and estimated potential results of the response for tensile stress was 2.234 N and those for $L^{*}$ was 82.39. Finally, the potential response results affected by mixture ratio of yulmu, wheat and water were screened using Excel.

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Optimum Mixture Proportion of Self-Compacting Concrete Considering Packing Factor of Aggregate and Fine Aggregate Volume Ratio (골재 채움율과 잔골재 용적비를 고려한 자기충전형 콘크리트의 최적배합)

  • 최연왕;정문영;정지승;문대중;안성일
    • Proceedings of the Korea Concrete Institute Conference
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    • 2002.10a
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    • pp.549-554
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    • 2002
  • In Powder System, SCC demands high dosage of superplasticizer and a lage amout of powder for suitable fluidity and viscosity. Okamura's method of most representative mixing design method in SCC of Powder-System is unfavorable economically because of using a large amount of powder. In addition, many ready-mixed concrete plants do not use his mix design method and procedure due to complexity for practical application. Therefore, Nan Su proposed more simple mix design method than Okamura's. It had an advantage in simplicity in practical application and required a smaller amount of powders compared with Okamura's method. This paper proposed an optimal mixture proportion of SCC with consideration of Nan Su's method. The new and modified mix design method required a smaller amount of powder than that of Nan Su's. To check the properties of SCC, considered with the requirements specified by the Japanese Society of Civil Engineering.(JSCE)

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