• 제목/요약/키워드: official method

검색결과 527건 처리시간 0.027초

열차 속도향상과 다양화를 감안한 선로용량 산정에 관한 연구 (Estimating Line Capacity Considering High-Speeding and Diversification of Trains)

  • 기형서;박동주;최종빈;추준섭
    • 한국철도학회논문집
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    • 제12권5호
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    • pp.623-630
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    • 2009
  • 한국철도시스템은 일반열차(각종 여객열차, 화물열차), 고속열차(KTX), 광역전철 급행열차(EMU) 등 다양한 종류의 열차가 사용되는 대중교통시스템이다. 철도시스템의 특징은 공시된 시간표에 의하여 열차가 운행되며, 안전, 정확, 신속, 쾌적한 서비스를 제곱한다는 것이다. 본 연구의 목적은 기존 열차의 속도향상과 다양화를 반영하여 보다 현실적인 선로용량 산정방식을 제시하고 검증하는 것이다. 본 논문은 이론식에 근거한 선로용량과 철도운영기관의 실용용량과의 차이를 최소화 하는데 역점을 두었다. 이를 위해 노선선형에 대한 TPS 시행, 운전방식과 열차제어방식 및 신호시스템 등을 고려한 새로운 철도용량 개념을 도입하였다. 실용Dia예시를 통해 새로운 선로용량산정방식의 결과를 검증하였다.

소셜 미디어 사회연결성의 팬덤 공동체 형성에 관한 탐색적 연구 : 방탄소년단 사례를 중심으로 (How does the Social Connectivity of Social Media Build a Fandom Community? An Exploratory Study on the BTS Fandom)

  • 이재원
    • 한국콘텐츠학회논문지
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    • 제21권7호
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    • pp.1-12
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    • 2021
  • 본 연구는 방탄소년단의 공식 트위터와 중국 미국 한국인 팬들의 심층 인터뷰를 토대로 스타와 팬이 소셜 미디어의 사회연결성을 토대로 글로벌 팬덤 공동체를 형성해내는 양상을 탐색했다. 스타와 팬은 소셜 미디어의 연결성을 활용해 공과 사를 넘나드는 유사-사적인 관계를 구축한다. 방탄소년단은 자신이 수상했음에도 팬클럽인 아미에게 "축하한다"라며 각 팬 개개인이 주체가 되도록 담화 방식을 구성해낸다. 팬으로서는 자신에게 사적으로 건네는 트윗처럼 여겨지게 되는데, 이는 비단 텍스트 구성 방식에만 적용되는 데 그치지 않는다. 공식적인 활동이나 기념일과 같은 공적인 행사가 없는 날에는 사적인 트윗 혹은 이전의 기억을 끌어올리며 하루도 빠지지 않고 소통하는 장치를 마련했다. 이처럼 끊이지 않고 연결되어 있다는 감각이 팬들이 서로에 대한 공동체 의식을 강화해주는 것으로 나타났다.

건설공사 비탈면 유지관리를 위한 보강공법별 점검항목에 관한 연구 (A Study on the inspection item classified by reinforcement method for the construction slope maintenance)

  • 김용수;장범수;신관영
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2005년도 춘계 학술발표회 논문집
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    • pp.759-764
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    • 2005
  • With the tunnel to case of the construction slope it executes the periodic maintenance due to an objectivity standard. But, the standard connected with construction slope is not integrated with the important public paper organic enemy and it is duplicated and the standards which conflict are being scattered. Also, it is referred to some specifications simply and the feature which is diffuse appears. Therefore, there is a necessity which it investigates the problem point of the maintenance civil official and it improves rationally and it takes a triangular position a confusedly be standard system. In this research which it sees accomplished the fundamental research against the inspection item classified by reinforcement method for the construction slope maintenance.

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Studies of Complex Formation between the Bromophenol Blue and some Important Aminoquinoline Antimalarials

  • Saadia-Mohamed-El-Ashry;Aly, Fatma-Ahmed;Amina-Mohamed-El-Brashy
    • Archives of Pharmacal Research
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    • 제17권6호
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    • pp.415-419
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    • 1994
  • A simple nad rapid colorimetric method for the assay of amodiaquine hydrochloride, chloroquine phosphate and primaquine phosphate is described. The method is based on the interaction of the drug base with bromophenol blue to give a ion-pair complex. The spectra of the complex shows a maxima at 415-420 nm with high apparent molar absorptivities. Beer's law was obeyed in the concentration range 1-8, 2-10 and $2-12{\;}{\mu}{\cdot}ml^{-1}$ for amodiaquine hydrochloride, primaquine phosphate and chloroquine phosphate respectively. The proposed method was applied to the determination of these drugs in certain formulations and the results were favourably comparable to the official methods.

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Empirical Evaluation of Indian Tourism Websites

  • Kaur, Anupriya
    • International Journal of Computer Science & Network Security
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    • 제22권9호
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    • pp.63-68
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    • 2022
  • Given the competition between different tourist destinations to attract domestic and international tourists it is absolutely vital to examine their website efficacy on specific attributes. This study employs one of the recently developed multi-criteria decision-making method the Best-Worst Method to assess the state government official tourism website across four Indian states known for their tourism potential- Himachal Pradesh, Uttrakhand, Uttar Pradesh and Rajasthan on specific attributes provided by the widely acknowledged WebQual instrument. Information Fit-to-Task and Trust emerged as the most important criterion. Relative advantage and Innovation the least important. The results of the study are easily interpretable and visual. They offer both an individual and comparative analysis of the perceived website efficacy on specific attributes to facilitate tourism stakeholders and website administrators to strategize and make their digital presence effective and competitive.

액-액 분배법을 활용한 작물 중 pymetrozine의 잔류분석법 확립 (Establishment of Analytical Method for Pymetrozine Residues in Crops Using Liquid-Liquid Extraction(LLE))

  • 윤지영;문혜리;박재훈;한예훈;이규승
    • 농약과학회지
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    • 제17권2호
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    • pp.107-116
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    • 2013
  • 액-액 분배법을 이용한 pymetrozine의 잔류분석방법을 다양한 작물에 적용이 가능하도록 작물의 특성과 대상농약의 물리화학적 특성을 고려하여 간섭물질을 최소화한 방법을 확립하였다. 확립된 분석법의 validation을 진행하였으며 정확성 및 정밀성, 검출한계, 정량한계, 직선성(표준물질의 검량선)을 기준으로 진행하였다. 대표 농산물로 쌀, 현미, 감자, 고추, 배추, 브로콜리, 수박, 쑥갓, 블루베리, 사과 및 체리를 선정하였으며, 농산물 시료에 borax 완충용액과 1N-NaOH 수용액을 가하여 pH를 조절하고 methanol로 추출된 pymetrozine 잔류분은 dichloromethane 액-액 분배법과 silica SPE cartridge를 이용한 silica 흡착크로마토그래피법으로 정제하여 분석대상 시료로 하였다. Pymetrozine의 정량적 분석을 위한 최적 HPLC 분석 조건을 확립하였고, $C_8$ 칼럼을 이용한 HPLC 분석 시 불순물의 간섭은 없었으며, 11종의 대표 농산물 중 pymetrozine의 분석정량한계(MQL)는 0.01 mg/kg이었다. 전체 농산물에 대한 회수율은 83.1~98.5%였으며, 농산물 시료 및 처리수준에 관계없이 반복 간 분석오차는 10% 미만을 나타내어 잔류분석 기준이내를 만족하였다. 검출한계, 회수율 및 분석오차 면에서 국제적 분석기준을 충분히 만족하였으므로, 본 연구에서 확립된 분석법은 기존의 hydromatrix 분배법을 대체하여 농산물 중 pymetrozine의 잔류분석법으로 사용이 가능할 것으로 판단된다.

국내 미등록 유기인계 농약의 수입 농식품에 대한 다성분 잔류분석법 (Multiresidue Analysis Method for Determination of Unregistered Organophosphorus Pesticides in Korea for Imported Agri-Food)

  • 전영환;황정인;안지운;김효영;도정아;오재호;황인균;임무혁;이중근;이영득;김장억
    • 한국환경농학회지
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    • 제31권3호
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    • pp.277-285
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    • 2012
  • 외국으로부터 수입되는 농식품에 대하여 국내에 미등록 된 유기인계 농약 aspon, chlorthion, chlorthiophos, crotoxyphos, demeton-O, demeton-S, demeton-S-methyl, dioxathion, heptenophos, iodofenphos, leptophos, methyl-trithion, propetamphos 및 sulfotep 등 14종에 대한 안전성 평가를 위하여 다성분 잔류분석법을 확립하고자 하였다. 잔류분석법은 식품의약품안전청에서 고시한 다종농약다성분 동시분석법-제2법에 잘 적용되었다. 수입 농산물의 대표 시료로 선정된 현미와 오렌지에 대한 유기인계 농약 14종 대한 잔류분석법의 밸리데이션을 실시한 결과 특이성, 직선성, 정확성, 정밀성 및 정량한계 수준을 만족시키는 것으로 나타났다. 단지 crotoxyphos의 경우는 기기상의 정량한계가 낮아서 저농도에서의 회수율은 좋지 않은 결과를 나타내었다. 따라서 본 연구에서 확립된 다성분 잔류분석법은 수입 농산물 중 crotoxyphos를 제외한 aspon 외 12종의 유기인계 농약에 대해 적용 가능한 것으로 나타났다.

농산물 중 메펜트리플루코나졸 및 트리티코나졸 살균제의 동시 분석법 개발 및 검증 (Development and Validation of a Simultaneous Analytical Method for the Detection of Mefentrifluconazole and Triticonazole Fungicide in Agricultural Crops)

  • 박지수;이한솔;이수정;신혜선;심재한;윤상순;정용현;오재호
    • 한국환경농학회지
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    • 제39권2호
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    • pp.130-137
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    • 2020
  • BACKGROUND: Mefentrifluconazole and triticonazole are the triazole fungicides. The maximum residue levels for agricultural products need to be set up. Therefore, development of the official analytical method for determination of mefentrifluconazole and triticonazole residues from agricultural crops was necessary due to safety management, and then a simultaneous analytical method was developed for the determination of mefentrifluconazole and triticonazole in agricultural crops. METHODS AND RESULTS: Samples were extracted using acetonitrile and purified using dispersive solid phase extraction, and then detected with liquid chromatograph-tandem mass spectrometry (LC-MS/MS). Matrix-matched calibration curves (0.0025-0.25 ㎍/mL) were linear into a sample extract with r2>0.99. For validation, the recovery test was carried out at three fortification levels (LOQ, 10 LOQ and 50 LOQ) from agricultural samples. The results for mefentrifluconazole and triticonazole ranged between 92.3 to 115.3% and 91.4 to 108.5%, respectively and RSD (relative standard deviation) values were also below 6.0%. Furthermore, inter-laboratory was conducted to validate the method. CONCLUSION: All values were corresponded with the criteria ranges requested by both the CODEX (CAC/GL 40-1993, 2003) and MFDS guidelines (2016). Therefore, the proposed method can be used as an official analytical method for determination of mefentrifluconazole and triticonazole (triazole fungicides) in the Republic of Korea.

1,4-Dioxane의 분석방법 연구 (A Study on the Research of Analytical Method for 1,4-Dioxane in Water)

  • 박선구;김태호;임연택;명노일
    • 한국물환경학회지
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    • 제21권6호
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    • pp.549-563
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    • 2005
  • The study was carried out to develop and standardize the analytical method of 1,4-dioxane in water. The National Institute of Environmental Research in Korea has monitored for 1,4-dioxane in water since 1998 and it has been detected in environmental water occasionally. But the environmental pollution and analytical method in water is not well known over the world. The trace analytical method at low-${\mu}/L$ level is prerequisite in order to evaluate the residue of 1,4-dioxane in water. Evaluation of the method was demonstrated by comparing and analyzing with liquid-liquid extraction, solid-phase extraction and purge & trap technique. As a result of experiment by standard solutions and raw samples, the precision and accuracy for three methods were obtained within error rate of about 10%. Therefore, three methods were standardized as official monitoring method in Korea. Also, a convenient and simple liquid-liquid extraction method for the analysis of 1,4-dioxane in water was developed by combined with gas chromatography/mass spectrometry and applied to the water samples in Korea

우유내 잔류물질 검사방법인 TTC-II법 및 Disk assay법의 비교시험 (Comparision of TTC-II and disk assay method for the detection of antibiotic residues in milk)

  • 이정아;이은미;이성해;도재철;박영구
    • 한국동물위생학회지
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    • 제22권1호
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    • pp.93-101
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    • 1999
  • This test process on screening method for the detection of residual antibiotics in milk is simple, economic, sensitive to residual antibiotics and was given approval international organs. Thus, this study was carried out the comparison of Disk assay method and TTC-II method for sensitivity and minimum detectable range of antibiotics in raw milk. The results of this study was summarized as follows ; 1. The number of samples requested for treatment of mastitis was 198 samples. Comparison or analytical results among the methods of TTC-II, disk assay and Delve sp was that TTC-II 37 samples(18.6% ), Disk assay 125samples(63.1%), Delve SP 130 samples(65.7% ) reacted positively. Conformity rate of Delve SP and Disk assay was 70%. 2. Detectable limits of disk assay method in some antibiotics were more sensitive than those of official method(0.05-0.0025ppm in the $\beta$-lactams, 1ppm in two aminoglycoside, 0.2 ppm in one tetracycline, similar in one macrolide) 3. For sensitivity of residual sulfonamides TTC-II was much more sensitive than disk assay. Detectable limits of sulfamethazine and sulfadimethoxine were 30 to 50ppm levels. 4. The best medium preservation period is 1-2 days. 5. Concentration of brome cresol purple related to resistance for B stearothermophilus culture was 24ppm/ml. These results show that disk assay method for screening detection of antibiotics residuces in milk is worthy of use.

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