• Title/Summary/Keyword: nickel powder

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Synthesis of Nickel Oxide (NiO) nanoparticles using nickel(II) nitrate hexahydrate as a precursor (Nickel(II) nitrate hexahydrate를 전구체로 사용한 산화니켈(NiO) 나노입자의 합성)

  • Soo-Jong Kim
    • The Journal of the Convergence on Culture Technology
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    • v.9 no.3
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    • pp.593-599
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    • 2023
  • Nickel oxide (NiO) nanoparticles were successfully synthesized by a simple liquid phase process for producing ceramics powder using a precursor impregnated with a nickel(II) nitrate hexahydrate aqueous solution in an industrial pulp. The microfibrile structure of the precursor impregnated with nickel nitrate hexahydrate aqueous solution was confirmed by scanning electron microscope (SEM), and the crystal structure and particle size of nickel oxide (NiO) particles produced as the heat treatment temperature of the precursor were analyzed by X-ray diffraction (XRD) and SEM. As a result, it was confirmed through XRD and SEM analysis that the temperature at which the organic material of the precursor is completely thermally decomposed was 495-500℃, and the size and crystallinity of the nickel oxide particles produced increased as the heat treatment temperature increased. The size of the nickel oxide particles obtained by heat treatment at 500-800℃ for 1 hour was 50-200 nm. It was confirmed by XRD and SEM analysis that a NiO crystal phase was formed at a heat treatment temperature of 380℃, only a single NiO phase existed until 800℃.

Evaluation of Fatigue Crack Propagation Behavior of Nickel-based Powder Metallurgy Superalloy for Aircraft at Elevated Temperature (항공기 터빈 디스크용 니켈기 초내열 분말야금 합금의 고온 피로균열진전 거동 비교 평가)

  • Yoon, Dong Hyun;Na, Seong Hyeon;Kim, Jae Hoon;Kim, Hongkyu;Kim, Donghoon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.41 no.8
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    • pp.751-758
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    • 2017
  • The behavior of fatigue crack growth of nickel-based powder metallurgy superalloy that could be used in aircraft turbine disc is investigated at room temperature, and $650^{\circ}C$ considering real operating conditions. The direct current potential drop(DCPD) method was used to measure the crack length of material in real time according to ASTM E647. Tests were performed with various stress ratios (0.1 and 0.5). Experimental results show that stress ratio, and temperature all affect the behavior of fatigue crack growth. As the stress ratio and temperature increase, the fatigue crack growth rate of nickel-based powder metallurgy superalloy also increases. Results were compared and reviewed with fatigue crack growth rates of other nickel-based superalloy materials (Inconel-100) that were studied in previous papers. Fractography analysis of the fractured specimens was performed using as SEM.

Catalytic Effects and Characteristics of Ni-based Catalysts Supported on TiO2-SiO2 Xerogel

  • Jeong, Jong-Woo;Park, Jong-Hui;Choi, Sung-Woo;Lee, Kyung-Hee;Lee, Chang-Seop
    • Bulletin of the Korean Chemical Society
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    • v.28 no.12
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    • pp.2288-2292
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    • 2007
  • The catalytic activities of nickel-based catalysts were estimated for oxidizing acetaldehyde of VOCs exhausted from industrial facilities. The catalysts were prepared by sol-gel methods of SiO2 and SiO2-TiO2 as a xerogel followed by impregnating Al2O3 powder with the nickel nitrate precursor. The crystalline structure and catalytic properties for the catalysts were investigated by use of BET surface area, X-ray diffraction (XRD), Xray photoelectron spectroscopy (XPS) and temperature programmed reduction (TPR) techniques. These results show that nickel oxide is transformed to NiAl2O4 spinel structure at the calcination temperature of 400 °C in response to the steps with after- and co-impregnation of Al2O3 powder in sol-gel process. The NiAl2O4 could suppress the oxidation reaction of acetaldehyde by catalysts. The NiO is better dispersed on SiO2-TiO2/Al2O3 support than SiO2/Al2O3 and SiO2-TiO2-Al2O3 supports. From the testing results of catalytic activities for oxidation of acetaldehyde, Catalysts showed a big difference in conversion efficiencies with the way of the preparation of catalysts and the loading weight of nickel. The catalyst of 8 wt.% Ni/TiO2-SiO2/Al2O3 showed the best conversion efficiency on acetaldehyde oxidation with 100% conversion efficiency at 350 °C.

Characterization of Nickel Composite Plating with TiO2 Particles for Photolysis of Organic Compound (유기물 광분해용 니켈-TiO2 복합도금 전극 특성에 관한 연구)

  • Choi, Chul-Young;Cho, Seung-Chan;Ryu, Young-Bok;Kim, Young-Seok;Kim, Hyoung-Chan;Kim, Yang-Do
    • Journal of the Korean institute of surface engineering
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    • v.40 no.3
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    • pp.125-130
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    • 2007
  • Many fundamental studies have been carried out regarding waste water and hazardous gas treatment technology using the photolysis effect of $TiO_2$. However, photolysis of both organic and organic-inorganic binders immobilizing $TiO_2$ makes permanent use impossible. In this study we manufactured a catalytic electrode by nickel-$TiO_2$ composite plating in order to immobilize $TiO_2$. The surface properties according to the current density changes of cathode and concentration changes of $TiO_2$ powder in nickel plating bath has been analysed with EDX, XRF, SEM, Raman spectrometer etc. The characterization of the catalytic electrode in decomposition of organic compound has been obtained by using UV-Visible spectrophotometer through analysing concentration changes of methyl orange solution containing the catalytic electrode vs. time with projecting UV-light in the solution. The study shows that a catalytic electrode of nickel-$TiO_2$ composite plating with high-efficiency in decompostion of organic compound has been formed under high concentration of $TiO_2$ powder and low current density of cathode.

Evaluation of the Effect of Nickel Powder on the Piezoresistivity Behavior of Carbon-Fiber/Rubber Composites (탄소섬유/고무 복합재료의 압저항과 니켈입자의 영향)

  • Lim, Dong-Jin
    • Composites Research
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    • v.34 no.6
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    • pp.412-420
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    • 2021
  • In this study, we measure the initial electrical conductivity of SCF/rubber specimens and SCF/rubber specimens with nickel particles respectively. The corresponding electrical conductivity with compressive strain on the specimens is also measured. Through this experiment, we observed the effects of the volume fraction of carbon fiber, nickel particles and external strain on the electrical conductivity. Experiments show that even a small difference in the volume fraction of SCF plays a major role in the change of the electrical conductivity and that the piezoresistivity increases due to fiber reorientation respond to external strain. In addition, the nickel particles contribute to improving the electrical conductivity in specimens with carbon fibers above the threshold volume fraction. It was confirmed that there is an effect of offsetting the increment in the piezoresistivity caused by the reorientation of carbon fibers according to external strain.

Evaluation of Fluidity and Compressive Strength of Mortar by Grading Variation of Ferro-Nickel Slag Sand (페로니켈 슬래그 잔골재의 입도 변화에 따른 모르타르의 유동성 및 압축강도 평가)

  • Kim, Do-Bin;Min, Sang-Hyun;Kim, Jeong-Hyeon;Ban, Jun-Mo;Choi, Se-Jin
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2017.05a
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    • pp.206-207
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    • 2017
  • We investigated the fluidity and compressive strength properties of mortar by Grading Variation of Ferro-Nickel Slag Sand in order to improve the utilization of ferro-nickel which is the by-product produced by making stainless steel, in the construction industry.

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