• Korean Chemical Engineering Research
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• v.46 no.4
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• pp.686-691
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• 2008

There are no many research reports on the preparation of ZnO by electrochemical oxidation since the zinc oxide is very easily dissolved in an acidic or basic environment, even though zinc oxides have attracted many attentions because of their optical/electrical properties. In this paper, we describe the fabrication of self-ordered stripes of ZnO by anodization of Zn in an ethanolic sulfuric acid. The formation of stripes of ZnO originating from Zn is attributed to water-selective dissolution of ZnO during anodization. We study in detail the effects of concentration of $H_2SO_4$, applied potential, anodization time, and addition of a small amount of water on the fabrication of stripes of ZnO. Mechanisms for the fabrication of ZnO stripes are discussed in terms of the above-mentioned effects.

• Journal of Environmental Health Sciences
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• v.45 no.5
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• pp.405-425
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• 2019

Objective: This study aimed to review the methodologies for evaluation of consumer spray products containing engineered nanomaterials (ENM), particularly focusing on inhalation exposure. Method: Literature on the evaluation methods for aerosolized ENM exposure from consumer spray products were collected through academic web searching. Common methodologies used in the literature, including research reports and academic articles, were also introduced. Results: The number of ENM-containing products have shown a considerable increase over recent years, from 54 in 2005 to 1,827 in 2018. Currently there is still discussion over the existing regulations with regard to product safety. Analysis of both ENM suspensions in the products and their aerosols is important for risk assessment. Comparison between the phases suggests how the size and concentration of particles change during the spray process. To analyze the ENM suspensions, dynamic light scattering, electron microscopy techniques, and inductively coupled plasma with mass spectrometry were used. In the aerosol monitoring, direct-reading instruments have been used to monitor the aerosols and conventional active sampling is used together to supplement the lack of real-time monitoring. There are also some models for estimating inhalation exposure. These models may be used to estimate mass exposure to nanomaterials contained in consumer products. Conclusion: Although there is no standardized method to evaluate ENM exposure from consumer products, many concerns about ENM have emerged. Every potential measure to reduce exposure to ENM from spray product use should be implemented through a precautionary recognition.

• Korean Chemical Engineering Research
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• v.59 no.3
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• pp.450-454
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• 2021

Currently, gamma nuclide analysis is mainly used using inorganic scintillators or semiconductor detectors. These detectors have high resolution but there are less economical, limited in size, and low process ability than plastic scintillators. Therefore, quantum dot-based plastic scintillator was developed using the advantages of the quantum dot nanomaterial and the conventional plastic scintillator. In this study, efficient plastic scintillator was fabricated by adding CdS/ZnS based on the most widely used Cd-based nanomaterial in a polystyrene matrix. In addition, the performance of the commercial plastic scintillator was compared and it was analyzed through radiological measurement experiments. The detection efficiency of fabricated plastic scintillator was higher than commercial plastic scintillator, EJ-200. It is believed that this fabricated plastic scintillator can be used as a radioactivity analyzer in the medical and nuclear facility fields.

• Journal of the Korean Society of Industry Convergence
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• v.26 no.6_3
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• pp.1297-1303
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• 2023

Research on enhancing the mechanical strength, lightweight properties, electrical conductivity, and thermal conductivity of composite materials by incorporating nano-materials is actively underway. Thermoplastic resins can change their form under heat, making them highly processable and recyclable. In this study, Polyamide-Nylon 6 (PA6), a thermoplastic resin, was utilized, and as reinforcing agents, fused carbon nano-materials (FCN) formed by structurally combining Carbon Nanotube(CNT) and Graphene were employed. Nano-materials often face challenges related to cohesion and dispersion. To address this issue, Silane functional groups were introduced to enhance the dispersion of FCN in PA6. The manufacturing conditions for the composite materials involved determining the use of a dispersant and varying FCN content at 0.05 wt%, 0.1 wt%, and 0.2 wt%. Tensile strength measurements were conducted, and FE-SEM analysis was performed on fracture surfaces. As a result of the tensile strength test, it was confirmed that compared to pure PA6, the strength of the polymer composite with a content of 0.05 wt% was improved by about 60%, for 0.1 wt%, about 65%, and for 0.2 wt%, the strength was improved by 50%. Also, when compared according to the content of FCN, the best strength value was shown when 0.1 wt% was added. The elastic modulus also showed an improvement of about 15% in the case of surface treatment compared to the case without surface treatment, and an improvement of about 70% compared to pure PA6. Through FE-SEM, it was confirmed that the matrix material and silane-modified nanomaterial improved the dispersibility and bonding strength of the interface, helping to support the load evenly and enabling effective stress transfer.

• Journal of Korean Society of Environmental Engineers
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• v.37 no.4
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• pp.218-227
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• 2015

A prerequisite for precise quantification of nanomaterials contained in environmental samples is to prepare suitable preservation conditions of samples. This study was initiated to suggest preservation conditions of aqueous samples for analyses of metal nanomaterials. Variation in the size of silver nanomaterial (cit-AgNP) was observed according to change in various conditions, such as pH, electrolyte concentration, temperature, nanomaterial concentration, and time. Aggregation of AgNP was characterized for each environmental condition, and finally proper preservation conditions of samples were proposed based on experimental results on AgNP aggregation. In addition, the preservation period of sample was computed by the doublet time of AgNP. The results indicate that the aggregation rate of cit-AgNP was close to 0 at the conditions of pH of ${\geq}7$, electrolyte ($Ca(NO_3)_2$) concentration of ${\leq}3mM$, temperature of $4^{\circ}C$, and cit-AgNP concentration of ${\leq}2mg/L$. Furthermore, the experimental results on doublet time of cit-AgNP suggest that maximum preservation period was evaluated to be 15.79~17.53 days when the concentration of 100 nm cit-AgNP is assumed to be $1{\mu}g/L$ which is considered as an environmentally-relevant concentration of engineered nanomaterials. Our results suggest that samples should be preserved at $4^{\circ}C$ and analyzed within 2 weeks.

• Electronics and Telecommunications Trends
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• v.33 no.1
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• pp.123-130
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• 2018

Tactile sensors, which are commonly referred to as pressure and strain sensors, have been extensively investigated to meet the demands for attachable and wearable electronics for monitoring the health status or activity of human users. For this purpose, the introduction of two-dimensional (2D) materials such as graphene and transition metal dichalcogenides (TMDs) with high mechanical strength at the atomic scale is very suitable for tactile sensors applicable for use in human-friendly devices. In this paper, we examine a descriptive summary of a tactile sensor and review state-of- the-art research trends of 2D material-based tactile sensors in terms of the material and architecture. Finally, we propose a roadmap for future studies into advanced tactile sensors based on our ongoing research.

• Carbon letters
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• v.12 no.1
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• pp.39-43
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• 2011

Synthesis of carbon fibers from cotton fiber by pyrolysis process has been described. Synthesis parameters are optimized using Taguchi optimization technique. Synthesized carbon fibers are used for studying hydrogen adsorption capacity using Seivert's apparatus. Transmission electron microscopy analysis and X-ray diffraction of carbon fiber from cotton suggested it to be very transparent type material possessing graphitic nature. Carbon synthesized from cotton fibers under the conditions predicted by Taguchi optimization methodology (no treatment of cotton fiber prior to pyrolysis, temperature of pyrolysis $800^{\circ}C$, Argon as carrier gas and paralyzing time for 2 h) exhibited 7.32 wt% hydrogen adsorption capacity.

• Progress in Superconductivity
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• v.9 no.1
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• pp.11-17
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• 2007

Magnetization studies have been carried out on $MgB_2$ polycrystalline samples in the temperature range of 5 - 44 K and in the magnetic field up to 7 Tesla. The critical current density was calculated from hysteresis loops using the Bean's critical state model, and the highest value of $J_c$ at 20 K was $2.7{\times}10^5\;A/cm^2$ at 2 Tesla. The hysteresis loops were carefully examined to determine the temperature and magnetic field range where flux jumps appeared. The first jump occurred typically at 1 Tesla. Due to the strong pinning, we observed the presence of flux jump below H = 1 Tesla at temperature below 30 K.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2014.04a
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• pp.81-82
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• 2014

Recently it is often reported about toxic nanomaterials to organisms. In other words, it is called nanotoxicity, toxic nanomaterials have extremely toxic properties. Zinc oxide is widely used as a promising nanomaterials, but some researchers are warning that nanotype zinc oxide has nanotoxicity. One of typical zinc oxide materials is a zinc oxide nanowire, especially, there is no technique which is detecting a zinc oxide nanowire because of its geometric. In here, we use reduced graphene oxide in order to detect zinc oxide nanowire and use DNA immobilized cantilever sensor, we detect graphene wrapped zinc oxide nanowire. Detection of a zinc oxide nanowire is measured by shifting of cantilever's resonance frequency based on vibration theory. It is proved that cantilever sensor is valid for nanomaterial detection. We showed that detection of a zinc oxide nanowire is successful.

• Journal of Powder Materials
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• v.20 no.1
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• pp.1-6
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• 2013

The key concept of nanopowder agglomerate sintering (NAS) is to enhance material transport by controlling the powder interface volume of nanopowder agglomerates. Using this concept, we developed a new approach to full density processing for the fabrication of pure iron nanomaterial using Fe nanopowder agglomerates from oxide powders. Full density processing of pure iron nanopowders was introduced in which the powder interface volume is manipulated in order to control the densification process and its corresponding microstructures. The full density sintering behavior of Fe nanopowders optimally size-controlled by wet-milling treatment was discussed in terms of densification process and microstructures.